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    Methods for Controlling Crystal Growth, Crystallization, Structures and Phases in Materials and Systems
    1.
    发明申请
    Methods for Controlling Crystal Growth, Crystallization, Structures and Phases in Materials and Systems 有权
    控制材料和系统中晶体生长，结晶，结构和相的方法

    公开(公告)号：US20120167818A1

    公开(公告)日：2012-07-05

    申请号：US13110456

    申请日：2011-05-18

    申请人： Bentley J. Blum ,  Juliana H. J. Brooks ,  Mark G. Mortenson

    发明人： Bentley J. Blum ,  Juliana H. J. Brooks ,  Mark G. Mortenson

    IPC分类号： C30B7/14

    CPC分类号： C01D3/24 ,  B01D9/005 ,  B01D9/0063 ,  C01B5/00 ,  C01B13/0214 ,  C12N13/00 ,  C30B7/00 ,  C30B29/58

    摘要： This invention relates to novel methods for affecting, controlling and/or directing various crystal formation, structure formation or phase formation/phase change reaction pathways or systems by exposing one or more components in a holoreaction system to at least one spectral energy pattern. In a first aspect of the invention, at least one spectral energy pattern can be applied to a crystallization reaction system. In a second aspect of the invention, at least one spectral energy conditioning pattern can be applied to a conditioning reaction system. The spectral energy conditioning pattern can, for example, be applied at a separate location from the reaction vessel (e.g., in a conditioning reaction vessel) or can be applied in (or to) the reaction vessel, but prior to other (or all) crystallization reaction system participants being introduced into the reaction vessel.

    摘要翻译： 本发明涉及通过将一个或多个组合在一个或多个组合中暴露于至少一个光谱能量图案来影响，控制和/或指导各种晶体形成，结构形成或相形成/相变反应途径或系统的新方法。 在本发明的第一方面中，至少一种光谱能量图案可以应用于结晶反应系统。 在本发明的第二方面，至少一种光谱能量调节模式可以应用于调理反应系统。 例如，光谱能量调节图案可以在与反应容器（例如在调理反应容器中）分开的位置处施加，或者可以应用于反应容器（或反应容器中），但在其它（或全部）之前） 结晶反应系统参与者被引入反应容器。

    Process to make high-purity salt or wet salt, salt SO obtainable, and the use thereof in an electrolysis process
    2.
    发明申请
    Process to make high-purity salt or wet salt, salt SO obtainable, and the use thereof in an electrolysis process 审中-公开
    制备高纯度盐或湿盐，可得到的盐SO的方法及其在电解过程中的用途

    公开(公告)号：US20050076477A1

    公开(公告)日：2005-04-14

    申请号：US10623574

    申请日：2003-07-22

    申请人： Mateo Mayer ,  Robert Geertman ,  Rene Demmer

    发明人： Mateo Mayer ,  Robert Geertman ,  Rene Demmer

    IPC分类号： C01D3/16 ,  C01D3/24 ,  C01D3/26 ,  C30B1/00

    CPC分类号： C01D3/26 ,  C01D3/16 ,  C01D3/24

    摘要： The invention relates to an evaporative crystallisation process to make salt compositions which includes a step wherein a mother liquor containing an effective amount of a crystal growth comprising at least one saccharide or saccharide derivative is formed, to form high-purity salt. The salt can be washed with a reduced amount of washing water while still containing lower amounts of K, Br, SO4 and/or Ca. The high-purity salt can be obtained after drying of the salt crystals formed. A wet salt can be obtained by partially drying said salt crystals.

    摘要翻译： 本发明涉及一种制备盐组合物的蒸发结晶方法，其包括形成含有有效量的包含至少一种糖或糖衍生物的晶体生长的母液以形成高纯度盐的步骤。 盐可以用减少量的洗涤水洗涤，同时仍然含有较少量的K，Br，SO 4和/或Ca。 干燥形成的盐晶后，可以得到高纯度盐。 通过部分干燥所述盐晶体可以获得湿盐。

    Process to make high-purity wet salt, wet salt so obtainable, and the use thereof in an electrolysis process
    3.
    发明申请
    Process to make high-purity wet salt, wet salt so obtainable, and the use thereof in an electrolysis process 失效
    制造高纯度湿盐，如此获得的湿盐的方法及其在电解过程中的应用

    公开(公告)号：US20030009857A1

    公开(公告)日：2003-01-16

    申请号：US10174846

    申请日：2002-06-19

    发明人： Mateo Jozef Jacques Mayer ,  Rene Lodewijk Maria Demmer

    IPC分类号： C30B001/00 ,  B01D009/00 ,  C02F001/461 ,  B01D017/06

    CPC分类号： C25B1/26 ,  C01D3/16 ,  C01D3/24

    摘要： The invention relates to an evaporative crystallization process to make salt compositions that includes a step wherein a mother liquor is formed that contains an effective amount of a crystal growth inhibitor that is selected from oligopeptides, polypeptides, and polymers bearing two or more carboxylic acid groups or carboxyalkyl groups and optionally further phosphate, phosphonate, phosphino, sulfate, and/or sulfonate groups, such as carboxymethyl cellulose with phosphate groups, to form salt crystals with a (111 ) face. The salt can be washed with a reduced amount of washing water while still containing lower amounts of K, Br, SO4, and/or Ca. A wet salt can be obtained by partially drying the salt crystals that are formed.

    摘要翻译： 本发明涉及一种制备盐组合物的蒸发结晶方法，其包括其中形成含有有效量的选自寡肽，多肽和带有两个或多个羧酸基团的聚合物的结晶生长抑制剂的母液的步骤，或 羧基烷基和任选的另外的磷酸酯，膦酸酯，膦基，硫酸酯和/或磺酸酯基团，例如具有磷酸酯基团的羧甲基纤维素，以形成具有（111）面的盐晶体。 盐可以用减少量的洗涤水洗涤，同时还含有较少量的K，Br，SO4和/或Ca。 可以通过部分干燥形成的盐晶体来获得湿盐。

    FREE FLOWING SALT COMPOSITION PREPARED BY EVAPORATIVE CRYSTALLIZATION
    6.
    发明申请
    FREE FLOWING SALT COMPOSITION PREPARED BY EVAPORATIVE CRYSTALLIZATION 有权
    通过蒸发结晶制备的自由流动的盐组合物

    公开(公告)号：US20150191361A1

    公开(公告)日：2015-07-09

    申请号：US14412936

    申请日：2013-07-10

    申请人： AKZO NOBEL CHEMICALS INTERNATIONAL B.V.

    发明人： Frits Spijkman ,  Roberot Aloysius Gerardus Maria Bergevoet

    IPC分类号： C01D3/06

    CPC分类号： C01D3/06 ,  C01D3/04 ,  C01D3/24

    摘要： Evaporative crystallization process to make salt compositions which comprises a step wherein a mother liquor is formed containing water and the salt to be crystallized and 1-5 ppm of an additive, based on the weight of the mother liquor, said additive being a water-soluble acrylic polymer, and a further step of evaporating the water to form crystallized salt.

    摘要翻译： 蒸发结晶方法制备盐组合物，其包括其中形成含有水的母液和待结晶的盐和1-5ppm的添加剂的步骤，基于母液的重量，所述添加剂是水溶性的 丙烯酸聚合物，以及蒸发水以形成结晶盐的另一步骤。

    Methods for controlling crystal growth, crystallization, structures and phases in materials and systems
    7.
    发明授权
    Methods for controlling crystal growth, crystallization, structures and phases in materials and systems 有权
    控制材料和系统中晶体生长，结晶，结构和相位的方法

    公开(公告)号：US08734535B2

    公开(公告)日：2014-05-27

    申请号：US13110456

    申请日：2011-05-18

    申请人： Bentley J. Blum ,  Juliana H. J. Brooks ,  Mark G. Mortenson

    发明人： Bentley J. Blum ,  Juliana H. J. Brooks ,  Mark G. Mortenson

    IPC分类号： B01D9/00

    CPC分类号： C01D3/24 ,  B01D9/005 ,  B01D9/0063 ,  C01B5/00 ,  C01B13/0214 ,  C12N13/00 ,  C30B7/00 ,  C30B29/58

    摘要： This invention relates to novel methods for affecting, controlling and/or directing various crystal formation, structure formation or phase formation/phase change reaction pathways or systems by exposing one or more components in a holoreaction system to at least one spectral energy pattern. In a first aspect of the invention, at least one spectral energy pattern can be applied to a crystallization reaction system. In a second aspect of the invention, at least one spectral energy conditioning pattern can be applied to a conditioning reaction system. The spectral energy conditioning pattern can, for example, be applied at a separate location from the reaction vessel (e.g., in a conditioning reaction vessel) or can be applied in (or to) the reaction vessel, but prior to other (or all) crystallization reaction system participants being introduced into the reaction vessel.

    摘要翻译： 本发明涉及通过将一个或多个组合在一个或多个组合中暴露于至少一个光谱能量图案来影响，控制和/或指导各种晶体形成，结构形成或相形成/相变反应途径或系统的新方法。 在本发明的第一方面中，至少一种光谱能量图案可以应用于结晶反应系统。 在本发明的第二方面，至少一种光谱能量调节模式可以应用于调理反应系统。 例如，光谱能量调节图案可以在与反应容器（例如在调理反应容器中）分开的位置处施加，或者可以施加在反应容器中（或到其中），但在其它（或全部）之前） 结晶反应系统参与者被引入反应容器。

    Hydrodynamic cavitation crystallization device and process
    9.
    发明申请
    Hydrodynamic cavitation crystallization device and process 审中-公开
    流体动力学空化结晶装置及工艺

    公开(公告)号：US20060118034A1

    公开(公告)日：2006-06-08

    申请号：US11330473

    申请日：2006-01-12

    申请人： Oleg Kozyuk

    发明人： Oleg Kozyuk

    IPC分类号： H01L21/322

    CPC分类号： C30B35/00 ,  B01D9/005 ,  B01D9/0054 ,  B01D9/0063 ,  B01D9/0081 ,  B01F5/0656 ,  C01D3/16 ,  C01D3/24 ,  C30B7/00 ,  C30B7/10 ,  C30B29/60

    摘要： A device and process for crystallizing a compound using hydrodynamic cavitation comprising the steps of mixing at least one stream of a solution of such compound to be crystallized with at least one stream of an anti-solvent and passing the mixed streams at an elevated pressure through a local constriction of flow to create hydrodynamic cavitation thereby causing nucleation and the direct production of crystals.

    摘要翻译： 一种用于使用流体动力空化使化合物结晶的装置和方法，包括以下步骤：将待结晶的这种化合物的溶液的至少一种流与至少一种抗溶剂流混合，并在高压下通过混合物流 流动的局部收缩以产生流体动力空化，从而引起成核并直接产生晶体。

    Process for the crystallization of an inorganic substance
    10.
    发明授权
    Process for the crystallization of an inorganic substance 失效
    无机物质结晶的方法

    公开(公告)号：US06478828B1

    公开(公告)日：2002-11-12

    申请号：US08358974

    申请日：1994-12-19

    申请人： Léon Ninane ,  Léopold Detry

    发明人： Léon Ninane ,  Léopold Detry

    IPC分类号： B01D902

    CPC分类号： C01D3/24 ,  B01D9/0022 ,  B01D9/0031 ,  B01D9/0036 ,  C30B7/00

    摘要： A process for crystallization of an inorganic substance includes preparing a supersaturated solution of the inorganic substance to be crystallized in a solvent which is a liquid; forcing a stream of the supersaturated solution upwardly through successively a fluidized bed distributor of a fluidized bed reactor and a bed of crystals arranged above the fluidized bed distributor with a pressure effective to cause fluidization of the bed of crystals, the fluidized bed distributor dividing the stream of supersaturated solution into thin, substantially parallel and vertical jets; maintaining the fluidized bed distributor at a temperature which is uniform and at which the inorganic substance to be crystallized from the supersaturated solution is lower than or equal to the concentration corresponding to saturation; and controlling the temperature of the fluidized bed distributor to cause the stream of supersaturated solution in the fluidized bed distributor to undergo a temperature change which is insufficient to desupersaturate it completely.

    摘要翻译： 无机物质的结晶方法包括在液态的溶剂中制备待结晶的无机物质的过饱和溶液; 将过饱和溶液的流向上通过流化床反应器的流化床分布器和布置在流化床分布器上方的晶体床，其压力有效地引起晶体床的流化，流化床分配器将流 的过饱和溶液变成薄的，基本上平行的和垂直的喷嘴; 将流化床分布器维持在均匀的温度下，从过饱和溶液中待结晶的无机物质低于或等于对应于饱和浓度的浓度; 并且控制流化床分布器的温度使得流化床分配器中的过饱和溶液流经历不足以使其完全过饱和的温度变化。