公开(公告)号：US07832619B2

公开(公告)日：2010-11-16

申请号：US11062777

申请日：2005-02-22

申请人： Greg A. Butzer ,  Robert H. Huizenga ,  Steven D. Mussman

发明人： Greg A. Butzer ,  Robert H. Huizenga ,  Steven D. Mussman

IPC分类号： B23K20/00

CPC分类号： C23C14/3414 ,  B23K20/021

摘要： A method of making a large Mo billet or bar for a sputtering target wherein two or more bodies comprising Mo are placed adjacent one another (e.g. stacked one on the other) with Mo powder metal present at gaps or joints between the adjacent bodies. The adjacent bodies are hot isostatically pressed to form a diffusion bond at each of the metal-to-Mo powder layer-to-metal joint between adjacent bodies to form a billet or bar that can be machined or otherwise formed to provide a large sputtering target. The number and dimensions of the Mo bodies placed adjacent one another are selected to yield a desired large size the billet or bar suitable for the sputtering target. The billet or bar for the sputtering target exhibits a microstructure comprising equiaxed grains of less than 30 microns grain size and exhibits a low oxygen content of less than about 100 ppm by weight.

摘要翻译： 制造用于溅射靶的大的Mo钢坯或棒的方法，其中包含Mo的两个或更多个本体彼此相邻放置（例如，彼此堆叠）的Mo粉末金属存在于相邻体之间的间隙或接缝处。 相邻的主体被热等静压以在相邻体之间的每个金属至钼粉末层与金属接头之间形成扩散结合，以形成可被加工或以其它方式形成以提供大的溅射靶的坯料或棒 。 选择彼此相邻放置的Mo体的数量和尺寸以产生适合于溅射靶的坯料或棒的期望的大尺寸。 用于溅射靶的坯料或棒材显示出包含小于30微米晶粒尺寸的等轴晶粒的显微组织，并且具有低于约100重量ppm的低氧含量。

公开(公告)号：US20070199676A1

公开(公告)日：2007-08-30

申请号：US11363518

申请日：2006-02-27

申请人： George Wolter

发明人： George Wolter

IPC分类号： B22C9/04

CPC分类号： B22D17/10

摘要： Composite mold for use in casting a metal or alloy includes an inner mold region that includes a mold cavity and a fugitive metallic outer backup mold region residing on the inner mold region, wherein the metallic material of the backup mold region has such a melting temperature that the backup mold region melts from the inner mold region after the molten metal or alloy is cast and at least partially solidified in the mold. The inner mold region can comprise a non-metallic refractory or ceramic shell mold, while the backup mold region can comprise tin or other relatively low melting point metal or alloy.

摘要翻译： 用于铸造金属或合金的复合模具包括内模区域，其包括模内腔和位于内模区域上的短暂的金属外支撑模具区域，其中备模区域的金属材料具有这样的熔化温度： 在铸造熔融金属或合金并在模具中至少部分地固化之后，备用模具区域从内部模具区域熔化。 内模区域可以包括非金属耐火材料或陶瓷壳模具，而后模具区域可以包括锡或其它相对低熔点的金属或合金。

公开(公告)号：US20060222922A1

公开(公告)日：2006-10-05

申请号：US11099416

申请日：2005-04-05

申请人： Kenneth Murphy

发明人： Kenneth Murphy

IPC分类号： H01M8/12 ,  H01M2/08 ,  B05D5/12

CPC分类号： H01M8/1246 ,  C23C14/02 ,  C23C14/083 ,  H01M8/0258 ,  H01M8/0271 ,  H01M2008/1293 ,  Y02E60/525 ,  Y02P70/56

摘要： A method of making a solid oxide fuel cell electrolyte includes preheating a substrate on which an oxide electrolyte layer is to be deposited to a substrate temperature of about 1100° C. and above, impinging a surface of a source comprising the oxide with an electron beam in an evacuated chamber at a pressure of about 10−3 or less mm of Hg devoid of process gas, such as oxygen, to evaporate the oxide in the chamber, and placing the preheated substrate in the chamber where the oxide deposits on the preheated substrate. The oxide fuel cell electrolyte is deposited having a columnar oxide microstructure.

摘要翻译： 制备固体氧化物燃料电池电解质的方法包括将其上沉积有氧化物电解质层的基板预热到约1100℃及更高的基板温度，用电子束撞击包含氧化物的源的表面 在真空室中，在大约10 -3 -3mm或更小mm的没有工艺气体（例如氧）的Hg的压力下蒸发室中的氧化物，并将预热的衬底放置在室中， 氧化物沉积在预热的基底上。 沉积具有柱状氧化物微结构的氧化物燃料电池电解质。

公开(公告)号：US06916387B2

公开(公告)日：2005-07-12

申请号：US10140004

申请日：2002-05-06

申请人： James B. Lulofs

发明人： James B. Lulofs

IPC分类号： B23K9/167 ,  B23K9/04 ,  B23K9/23 ,  B23K31/00 ,  B23P6/00 ,  B23P6/04 ,  F01D5/00 ,  C21D10/00

CPC分类号： B23P6/007 ,  B23K9/04 ,  B23K9/044 ,  B23K2101/001 ,  B23K2103/08 ,  B23K2103/26 ,  F01D5/005 ,  F05D2230/30 ,  F05D2230/80

摘要： A method of repairing a void on a nickel or cobalt base superalloy investment casting by vibrating the casting for a time before repairing the void, vibrating the casting while filling the void wherein the void is filled by repeatedly making incremental weld deposits of a superalloy filler material in the void using pulsed gas tungsten arc welding, and impinging each incremental deposit with a cooling gas after each incremental weld deposit is made and before the next incremental weld deposit is made, and vibrating the casting for a time after the void is filled.

摘要翻译： 一种修复镍或钴基超级合金熔模铸造件上的空隙的方法，该方法是在修复空隙之前振动铸件一段时间，同时在填充空隙的同时振动铸件，其中通过反复制造超合金填充材料的增量焊接沉积来填充空隙 在使用脉冲气体钨电弧焊接的空隙中，并且在进行每次增量焊接沉积之后并且在进行下一个增量焊接沉积之前，用冷却气体冲击每个增量沉积物，并在填充空隙之后振动一段时间。

公开(公告)号：US06896030B2

公开(公告)日：2005-05-24

申请号：US10630224

申请日：2003-07-30

申请人： Mark L. Soderstrom ,  Bradley Donaldson ,  John R. Brinegar

发明人： Mark L. Soderstrom ,  Bradley Donaldson ,  John R. Brinegar

IPC分类号： B22D27/04 ,  B22D25/00

CPC分类号： B22D27/045

摘要： Apparatus and method for DS casting using one or more thermal baffle members positionable at a lower open end of a directional solidification casting furnace by movement of a ram on which a mold to be cast is moved relative to the casting furnace. A unique thermal baffle member can be used for each particular series or run of molds to be cast.

摘要翻译： 一种用于DS浇铸的装置和方法，其使用一个或多个热定挡件，其可定位在定向凝固铸造炉的较低开口端，通过其上待铸造的模具相对于铸造炉移动的冲头。 可以为每个特定的系列或模具铸造使用独特的热障板构件。

公开(公告)号：US5335717A

公开(公告)日：1994-08-09

申请号：US828206

申请日：1992-01-30

申请人： Stephen Chin ,  Donald R. Parille ,  Paul R. Aimone ,  Robert L. McCormick ,  Paul R. Johnson ,  Bart M. Kilinski

发明人： Stephen Chin ,  Donald R. Parille ,  Paul R. Aimone ,  Robert L. McCormick ,  Paul R. Johnson ,  Bart M. Kilinski

IPC分类号： B22C3/00 ,  B22D27/20 ,  C22C1/02 ,  B22C1/02

CPC分类号： C22C1/02 ,  B22C3/00 ,  B22D27/20

摘要： The oxidation resistance of a superalloy casting such as an equiaxed, directionally solidified, or single crystal casting, is improved by melting, pouring, or casting the alloy so as to react with a magnesium or calcium-bearing ceramic material. Magnesium or calcium is introduced into the alloy through a controlled reaction between the alloy and the magnesium or calcium-bearing ceramic material.

摘要翻译： 通过熔融，浇注或铸造合金以与含镁或钙的陶瓷材料发生反应，提高了诸如等轴，定向凝固或单晶铸件的超级合金铸件的抗氧化性能。 通过合金和含镁或钙的陶瓷材料之间的受控反应将镁或钙引入合金中。

公开(公告)号：US5332022A

公开(公告)日：1994-07-26

申请号：US942020

申请日：1992-09-08

申请人： Gregory N. Colvin

发明人： Gregory N. Colvin

IPC分类号： B22D19/02 ,  B22D31/00

CPC分类号： B22D31/005 ,  B22D19/02

摘要： A method of making a composite casting wherein a casting mold is provided having a melt-receiving mold cavity and a preformed metallic or intermetallic insert located in a predetermined position in the mold cavity. A melt is introduced into the mold cavity about the insert and is solidified to provide a composite casting having one or more interfaces between the insert, or an insert positioning member, and cast/solidified metal about the insert. The interface is exposed on or communicates with an exterior surface of the composite casting. After separation from the mold, the composite casting is subjected to a sealing operation to gas-tight seal the interface(s) at the exterior casting surface. For example, the interface can be sealed by providing fused material at the interface. After the interface(s) is (are) sealed, the composite casting is subjected to elevated temperature and isostatic gas pressure conditions effective to produce a sound, void-free, contamination-free metallurgical bond between the insert and the cast melt thereabout. The previously sealed interface(s) prevent the pressurizing gas from entering and migrating between the insert and the cast melt so as to enable formation of the sound, void-free, contamination-free bond.

摘要翻译： 一种制备复合铸造的方法，其中提供具有熔体接收模具腔的铸模和位于模腔中的预定位置的预成型金属或金属间插入件。 将熔体引入到模具腔内，并且固化，以提供在插入件或插入件定位构件之间具有一个或多个界面的复合铸件和围绕插入件的铸造/固化金属。 该界面暴露在复合铸件的外表面上或与复合铸件的外表面连通。 在与模具分离之后，对复合铸件进行密封操作，以在外部铸造表面上气密地密封界面。 例如，可以通过在界面处提供熔融材料来密封界面。 在密封界面之后，复合铸件经受高温和等静压气体压力条件，有效地在插入件和铸造熔体之间产生声音，无空隙，无污染的冶金结合。 先前密封的界面防止加压气体进入和移动插入件和铸造熔体之间，以便形成声音，无空隙的无污染的粘合。

公开(公告)号：US5287910A

公开(公告)日：1994-02-22

申请号：US943704

申请日：1992-09-11

申请人： Gregory N. Colvin ,  Leonard L. Ervin ,  Robert F. Johnson

发明人： Gregory N. Colvin ,  Leonard L. Ervin ,  Robert F. Johnson

IPC分类号： B22D18/06 ,  B22C9/06 ,  B22C9/08 ,  B22D18/04 ,  B22D21/00 ,  B22D21/02

CPC分类号： B22C9/061 ,  B22D18/04 ,  B22D18/06 ,  B22D21/005 ,  B22D21/025

摘要： Titanium based and nickel based castings are made by casting a suitable melt having a relatively low melt superheat into a mold cavity defined by one or more low carbon steel or titanium mold members where the melt solidifies to form the desired casting. The melt super-heat is limited so as not to exceed about 150.degree. F. above the liquidus temperature of the particular melt being cast. For a steel mold, one or more titanium melt inlet-forming members are provided for cooperating with the steel mold members to form an melt ingate that communicates to the mold cavity for supplying the melt thereto in a manner to avoid harmful iron contamination of the melt during casting. The mold body-to-mold cavity volume ratio is controlled between 10:1 to 0.5:1 to minimize casting surface defects and mold wear/damage.

摘要翻译： 钛基和镍基铸件通过将具有相对低的熔体过热的合适的熔体浇铸到由一个或多个低碳钢或钛模具构件限定的模腔中而制成，其中熔体固化以形成所需的铸件。 熔体超热受到限制，以便不超过要浇注的特定熔体的液相线温度以上约150华氏度。 对于钢模具，设置一个或多个钛熔体入口形成构件以与钢模具构件配合以形成熔融浇口，其与模腔连通以将熔体供应到其中以避免熔体的有害铁污染 铸造时。 模具体对模腔体积比控制在10：1至0.5：1之间，以最大限度地减少铸件表面缺陷和模具磨损/损坏。

公开(公告)号：US5273204A

公开(公告)日：1993-12-28

申请号：US173468

申请日：1988-03-25

申请人： Ranes P. Dalal ,  John M. McFadden ,  Mark J. Straszheim ,  Louis E. Dardi

发明人： Ranes P. Dalal ,  John M. McFadden ,  Mark J. Straszheim ,  Louis E. Dardi

IPC分类号： B23K28/00 ,  B23K1/00 ,  C23C4/02 ,  C23C4/08 ,  C23C4/12 ,  C23C4/18 ,  B23K10/02

CPC分类号： B23K1/0008 ,  B23K2203/26

摘要： A method of joining metal materials by spraying molten metal into a cavity between the articles to be joined. Prior to deposition of the metal, the surface of the cavity is cleaned and the articles to be joined are preheated. Subsequent to deposition of the metal within the cavity, the joined articles are cooled at a rate that precludes damage due to thermal effects and the deposited metal is consolidated in the cavity by hot pressing.

摘要翻译： 通过将熔融金属喷射到待接合制品之间的空腔中来连接金属材料的方法。 在沉积金属之前，清洁空腔的表面并且待接合的物品被预热。 在将金属沉积在空腔内之后，连接的制品以不会由于热效应造成损坏的速度被冷却，并且沉积的金属通过热压固结在空腔中。

公开(公告)号：US5241738A

公开(公告)日：1993-09-07

申请号：US2104

申请日：1993-01-08

申请人： Gregory N. Colvin

发明人： Gregory N. Colvin

IPC分类号： B22D19/02

CPC分类号： B22D19/02 ,  Y10T29/49972 ,  Y10T29/49988

摘要： A casting mold includes a melt-receiving mold cavity having a preformed metallic or intermetallic insert suspended therein by at least one elongated, slender suspension member fixed at one end to the insert and at another end to the mold. A melt of metallic or intermetallic material is introduced into the mold cavity about the suspended insert and the suspension member and is solidified to form a composite casting The casting is subjected to elevated temperature/elevated isostatic gas pressure conditions wherein the interface between the suspension member and the cast melt is effective to inhibit gas penetration between the insert and cast melt, thereby allowing a sound, void-free, contamination-free metallurgical bond to be produced between the insert and the cast melt.

摘要翻译： 铸造模具包括熔体接收模具腔，其具有通过至少一个细长的细长悬挂构件悬挂在其中的预成型金属或金属间插入件，该悬挂构件的一端固定在插入件上，另一端固定在模具上。 金属或金属间材料的熔体围绕悬挂的嵌件和悬挂构件被引入模腔中并被固化以形成复合铸件。铸件经受高温/升高的等静压气体压力条件，其中悬架构件和 铸造熔体有效地抑制插入件和铸造熔体之间的气体渗透，从而允许在插入件和铸造熔体之间产生无声无空隙的无污染冶金结合。