Preparation of alkynyl aryl compounds
    1.
    发明授权
    Preparation of alkynyl aryl compounds 失效
    烷基芳基化合物的制备

    公开(公告)号:US3758622A

    公开(公告)日:1973-09-11

    申请号:US3758622D

    申请日:1971-05-25

    发明人: WATSON J ALLISON B

    摘要: A process for the conversion of alkyl aryl compounds to alkynyl aryl compounds which comprises subjecting said alkyl aryl compounds to chlorination under conditions suitable for the dichlorination of at least one carbon atom of an alkyl substituent to said alkyl aryl compound or monochlorination of adjacent carbon atoms of said alkyl substituent, subjecting the resulting chlorinated alkyl aryl compound to dehydrochlorination in the presence of a basic medium, and thereafter recovering alkynyl aryl compounds.

    摘要翻译: 一种将烷基芳基化合物转化为炔基芳基化合物的方法,其包括使所述烷基芳基化合物在适合于将所述烷基芳基化合物的至少一个碳原子的烷基取代基二氯化的条件或相邻碳原子的一氯化作用 所述烷基取代基,在碱性介质存在下使所得氯代烷基芳基化合物脱氯化氢,然后回收炔基芳基化合物。

    Titanium dioxide mixing
    2.
    发明授权
    Titanium dioxide mixing 失效
    二氧化钛混合

    公开(公告)号:US3752687A

    公开(公告)日:1973-08-14

    申请号:US3752687D

    申请日:1969-11-10

    发明人: HAHN G

    IPC分类号: B01F15/00 B02C13/28 C09C1/36

    CPC分类号: B01F15/00837 B02C13/2804

    摘要: DISCOLORATION OF WHITE TITANIUM DIOXIDE DURING MIXTURE, MILLING OR BLENDING BY ABRASIVE DISCOLORATION BY METALLIC PARTS OF THE MIXER ARE PREVENTED BY COATING OR PLATING THE MIXING BOWL AND MIXING ELEMENTS WITH VARY HARD MATERIAL EXCEEDING ABOUT WIEGHT MOHS SUCH AS TUNGSTEN CARBIDE OR OTHER HARD CARBIDE MATERIALS.

    Heptyl phenol alkylation
    3.
    发明授权
    Heptyl phenol alkylation 失效
    HEPTYL苯酚烷基化

    公开(公告)号:US3639490A

    公开(公告)日:1972-02-01

    申请号:US3639490D

    申请日:1966-02-25

    IPC分类号: C07C37/14 C07C39/06

    CPC分类号: C07C37/14 C07C39/06

    摘要: A C7 HEART CUT OF CATALYTIC GASOLINE CONTAINING LARGE QUANITIES OF OLEFINES AND CYCLOOLEFINES IS CONVERTED TO A SUBSTANTIALLY SATURATED DEHYDROAROMATIZATION FEEDSTOCK COMPOSED PREDOMINANTLY OF C7 PARAFFINS AND CYCLOALKANES WHILE SIMULTANEOUSLY PRODUCING HIGHLY ECONOMICALLY A MIXTURE OF ALKYL PHENOLS BY USING UP TO OLEFINE AND CYCLOOLEFINE CONTENT FO THE USATURATED C7 HEART CUT IN AN ALKYLATION REACTION UPON PHENOLS.

    Titanium dioxide stabilizing
    4.
    发明授权
    Titanium dioxide stabilizing 失效
    二氧化钛稳定

    公开(公告)号:US3492264A

    公开(公告)日:1970-01-27

    申请号:US3492264D

    申请日:1966-02-08

    发明人: HAHN GRANVILLE J

    IPC分类号: C09C1/36 C08K1/06 C08F45/04

    摘要: 1,181,372. Titanium dioxide compositions. COSDEN OIL & CHEMICAL CO. 7 Feb., 1967 [8 Feb., 1966], No. 5727/67. Heading C3P. The greying of titanium dioxide pigmented compositions imparted during abrasive mixing, i.e. dry mixing in contact with metallic surfaces under conditions where the metal rubs off and discolours the pigment, is reduced by carrying out the mixing in the presence of up to 1% by wt. of a friable, dust-forming, colourless, alkaline inorganic solid containing or producing during the mixing particles having a size of less than 60 mesh U.S. Standard Sieve. The solid may be sodium hydroxide, calcium oxide, barium oxide, strontium oxide, magnesium oxide, calcium hydroxide, sodium bicarbonate, potassium carbonate, or sodium aluminate or borate and may contain an oxidizing agent, e.g. potassium persulphate or hydrogen peroxide. The composition may comprise particles, e.g. beads, of polystyrene.

    Co-extrusion of acrylic ester polymer/polystyrene multiple-layered sheeting
    5.
    发明授权
    Co-extrusion of acrylic ester polymer/polystyrene multiple-layered sheeting 失效
    丙烯酸酯聚合物/聚苯乙烯多层片材的共挤出

    公开(公告)号:US3882219A

    公开(公告)日:1975-05-06

    申请号:US38750673

    申请日:1973-08-10

    发明人: WILEY DONALD F

    摘要: A process is disclosed for producing composite sheeting of polystyrene having a thin protective layer of an acrylic ester polymer. The process comprises joining a molten stream of each polymeric material in a single extruder discharge conduit such that there is produced a single molten stream having a reasonably well defined interface between the two types of polymeric material, and thereafter, passing the resulting single stream of material through a sheet-form extrusion die having its die lips generally aligned with the foregoing interface.

    摘要翻译: 公开了一种制备具有薄丙烯酸酯聚合物保护层的聚苯乙烯复合片材的方法。 该方法包括将单个挤出机排出导管中的每种聚合物材料的熔融流接合,使得产生具有在两种类型的聚合物材料之间具有相当明确界定的界面的单一熔融流,然后使得到的单一物料流 通过具有通常与前述界面对准的模唇的片状挤出模具。

    Thermolysis of styrene oxide
    6.
    发明授权
    Thermolysis of styrene oxide 失效
    苯乙烯氧化物的热解

    公开(公告)号:US3860614A

    公开(公告)日:1975-01-14

    申请号:US33545673

    申请日:1973-02-26

    发明人: WATSON JAMES M

    摘要: Styrene oxide is heated under relatively mild temperature conditions to cause thermolysis. Such thermolysis produces substantial quantities of phenylacetaldehyde in the reaction product. Substantially pure phenylacetaldehyde may be recovered from the crude reaction product by distillation procedure, or other separation means, or, if desired, the phenylacetaldehyde may be directly converted in the crude reaction product to produce its acetals. The process of thermolysis of styrene oxide may be conducted with the styrene oxide in liquid phase, in vapor phase, or in solution within an inert solvent. The conditions of reaction are maintained to achieve a mild decomposition, described as thermolysis, as contrasted to a drastic decomposition, a so-called pyrolysis.

    摘要翻译: 在相对温和的温度条件下加热氧化苯乙烯以引起热解。 这种热解在反应产物中产生大量苯乙醛。 可以通过蒸馏程序或其他分离方法从粗反应产物中回收基本上纯的苯基乙醛,或者如果需要,可以将苯乙醛直接转化成粗反应产物以产生其缩醛。 氧化苯乙烯的热解过程可以用苯乙烯氧化物在液相中,气相或在惰性溶剂中的溶液中进行。 保持反应的条件以达到轻度分解,被描述为热解,与剧烈的分解(所谓的热解)相反。

    Method of forming foamed polystyrene articles from polystyrene beads
    8.
    发明授权
    Method of forming foamed polystyrene articles from polystyrene beads 失效
    从聚苯乙烯珠形成泡沫聚苯乙烯制品的方法

    公开(公告)号:US3814779A

    公开(公告)日:1974-06-04

    申请号:US13025871

    申请日:1971-04-01

    发明人: WILEY D

    IPC分类号: B29C44/34 B29D27/00 B29F3/06

    摘要: A SCREW EXTRUDER FOR CONVERTING POLYSTYRENE BEADS INTO FOAM INCLUDING AN EXTRUDER SCREW HAVING A FIRST SCREW STAGE FOR RECEIVING POLYESTERS BEADS AND FOR COMPRISING AND MELTING THE BEADS TO FORM MELTED POLYSTRENE AND A SECOND SCREW STAGE FORRECEIVING MELTED POLYSTRENE FROM THE FIRST STAGE AND FOR DISTRUBING A BOWLING AGENT THROUGHOUT THE MELTED POLYRENE; AND A RING VALVE FOR CONTROLLING THE FLOW OF MELTED POLYSTYRENE FROM THE FIRST

    STAGE TO THE SECOND STAGE AND THEREBY PREVENTING BACKFLOE OF THE BOWLING AGENT FROM THE SECOND STAGE INTO THE FIRST STAGE. THE FIRST SCREW STAGE OF THE EXTRUDER SCREW HAS A COMPRESSION RATIO OF ABOUT 3.5:1, AND COMPRISES A METERING SECTION, A TRANSITION SECTION THAT IS ABOUT 1.5 TIMES AS LONG AS THE METERING SECTION, AND A FEED SECTION THAT IS ABOUT 2 TIMES AS LONG AS THE METERING SECTION.

    Synthesis of dialkaryl sulfone
    10.
    发明授权
    Synthesis of dialkaryl sulfone 失效
    DIALKARYL SULFONE的合成

    公开(公告)号:US3729517A

    公开(公告)日:1973-04-24

    申请号:US3729517D

    申请日:1970-11-09

    发明人: BRACKE W

    IPC分类号: C07C315/06 C07C317/14

    CPC分类号: C07C315/06 C07C317/14

    摘要: DIALKARYL SULFONES ARE FORMED BY TREATING THE FIRST STAGE ALKARYL SULFONIC ACID WITH MORE ALKARYL HYDROCARBON IN A SECOND STAGE, THE SECOND STAGE REACTION BEING INITIATED BY P2O5, REMOVING THE WATER FORMED IN THE REACTION BY AZEOTROPIC DISTILLATION OF SOME OF HE EXCESS HYDROCARBON FROM THE REACTION MIXTURE AS THE SULFONIC IS FORMED.