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8 条记录 (耗时 0.01 秒)

    Device for preparing dissolved substances for mass-spectrometric analysis
    1.
    发明授权
    Device for preparing dissolved substances for mass-spectrometric analysis 失效
    制备用于质谱分析的溶解物质的装置

    公开(公告)号：US4376391A

    公开(公告)日：1983-03-15

    申请号：US238280

    申请日：1981-02-25

    申请人： Curt Brunnee

    发明人： Curt Brunnee

    IPC分类号： G01N1/40 ,  G01N35/02

    CPC分类号： G01N1/40 ,  G01N2001/4027

    摘要： A fraction obtained from a liquid chromatograph column is introduced into a cup-shaped collecting vessel 12 having a centrally apertured funnel-shaped bottom surface 14. A sample holder 13 is removably accommodated in the aperture, and after the evaporation of the fraction solvent the remaining residue 11 collects on or in the holder, which may then be removed and directly introduced into the ionization chamber of a mass spectrometer for further analysis.

    摘要翻译： 将从液相色谱柱获得的级分引入具有中心孔漏斗形底表面14的杯形收集容器12中。样品保持器13可移除地容纳在孔中，并且在蒸馏馏分溶剂后，剩余的 残留物11收集在载体上或载体中，然后将其除去并直接引入质谱仪的电离室用于进一步分析。

    Separating device for mixtures of gaseous or vaporous substances, especially for separating a carrier gas from a fraction to be analyzed in a combined gaschromatograph and mass-spectrometer
    2.
    发明授权
    Separating device for mixtures of gaseous or vaporous substances, especially for separating a carrier gas from a fraction to be analyzed in a combined gaschromatograph and mass-spectrometer 失效
    用于分离气相或蒸气物质混合物的分离装置，特别用于分离载体气体，分析在组合的气相色谱和质谱仪中

    公开(公告)号：US3678656A

    公开(公告)日：1972-07-25

    申请号：US3678656D

    申请日：1970-04-06

    申请人： CURT BRUNNEE ,  HANS JOACHIM BULTEMANN

    发明人： BRUNNEE CURT ,  BULTEMANN HANS-JOACHIM

    IPC分类号： G01N30/72 ,  G01N30/84 ,  B01D53/02

    CPC分类号： G01N30/84 ,  G01N30/7293

    摘要： This invention relates to a device for separating mixtures of gasses or vapors. The device utilizes a separating chamber having an inlet for admitting the mixture by viscous flow. The chamber has two outlets, one of which permits molecular flow and the other of which permits viscous flow. Separation occurs when the lower molecular weight fraction of the mixture predominantly leaves the chamber through the outlet permitting molecular flow while the higher molecular weight fraction leaves through the viscous flow outlet. The device may be employed, for example, to separate the helium carrier gas from a hydrocarbon where the mixture is eluted from a gas chromatograph and it is desired to concentrate the hydrocarbon for analysis by mass spectrometry.

    摘要翻译： 本发明涉及用于分离气体或蒸汽混合物的装置。 该装置使用具有用于通过粘性流来允许混合物的入口的分离室。 该室具有两个出口，其中一个允许分子流动，另一个允许粘性流动。 当混合物的较低分子量级分主要通过允许分子流出口的出口离开室，而较高分子量级分离开粘性流出口时，就发生分离。 该装置可以用于例如将氦载气与烃混合从气相色谱仪中洗脱出来，并且期望通过质谱法浓缩烃进行分析。

    Device for adjusting slit widths in spectrometers
    4.
    发明授权
    Device for adjusting slit widths in spectrometers 失效
    用于调整光谱仪中狭缝宽度的装置

    公开(公告)号：US4612440A

    公开(公告)日：1986-09-16

    申请号：US648891

    申请日：1984-09-10

    申请人： Curt Brunnee ,  Peter Dobberstein ,  Gunter Kappus

    发明人： Curt Brunnee ,  Peter Dobberstein ,  Gunter Kappus

    IPC分类号： G01J3/04 ,  G21K1/04 ,  H01J49/02 ,  G01J3/02

    CPC分类号： H01J49/067 ,  G01J3/04 ,  G21K1/04 ,  H01J49/02

    摘要： Slit means in spectrometers for the analysis of organic and inorganic substances, in particular in mass spectrometers, have hitherto been controlled for varying the slit widths by connecting them in a suitable manner to a metallic wire, through which an electric current flowed, under the influence of which the wire heats up and changes its length. The slit or diaphragm means connected to the wire were then displaced relative to the beam path. It is a great disadvantage that the diaphragms follow a change of the current for controlling the slit widths with a relatively long time delay, which is unacceptable for various types of measuring operation, in particular types of measuring operation under data system control. To eliminate this disadvantage, a device (11) is proposed which has at least one movable slit jaw (12) which is movable to and fro, substantially perpendicular to the beam path (16) and without delay, by a piezo-electric element (14).

    摘要翻译： 狭缝意味着用于分析有机和无机物质，特别是在质谱仪中的分光计，迄今为止已经通过将它们以合适的方式连接到金属丝来控制以改变狭缝宽度，电流在影响下通过其流过电流 其中电线加热并改变其长度。 连接到电线的狭缝或隔膜装置然后相对于光束路径移位。 隔膜具有相当长的时间延迟来控制狭缝宽度的电​​流的变化是非常大的缺点，对于各种类型的测量操作，特别是在数据系统控制下的测量操作类型是不可接受的。 为了消除这个缺点，提出了一种装置（11），其具有至少一个可移动的狭缝钳口（12），其可移动地来回移动，基本上垂直于光束路径（16）并且无延迟地通过压电元件（ 14）。

    Ion detector with bipolar accelerating electrode
    5.
    发明授权
    Ion detector with bipolar accelerating electrode 失效
    带双极加速电极的离子探测器

    公开(公告)号：US4267448A

    公开(公告)日：1981-05-12

    申请号：US45144

    申请日：1979-06-04

    申请人： Karl Feser ,  Curt Brunnee

    发明人： Karl Feser ,  Curt Brunnee

    IPC分类号： G01T1/28 ,  H01J49/02 ,  B01D59/44

    CPC分类号： G01T1/28 ,  H01J49/025

    摘要： The ion detector of a mass spectrometer includes an accelerating electrode 10, 34, 38 disposed between the spectrometer discharge shutter 6 and a secondary electron multiplier 18. The electrode 10 is selectively energized by a high positive or negative voltage opposite the initial polarity of the ions by a source 16. Thus, a positively energized electrode draws in and accelerates negative ions, and strips away their electrons to leave them positively charged for further acceleration into the first dynode of the secondary electron multiplier.

    摘要翻译： 质谱仪的离子检测器包括设置在分光计放电快门6和二次电子倍增器18之间的加速电极10,34,38。电极10选择性地通过与离子的初始极性相反的高正或负电压 因此，带正电的电极吸引并加速负离子，并剥离其电子，以使它们带正电，以进一步加速到二次电子倍增器的第一倍增电极。

    Mass spectrometer having an ICP source
    6.
    发明授权
    Mass spectrometer having an ICP source 失效
    质谱仪具有ICP源

    公开(公告)号：US5552599A

    公开(公告)日：1996-09-03

    申请号：US315569

    申请日：1994-09-30

    申请人： Ulrich Giessmann ,  Gerhard Jung ,  Curt Brunnee

    发明人： Ulrich Giessmann ,  Gerhard Jung ,  Curt Brunnee

    IPC分类号： H01J49/02 ,  H01J49/10 ,  H01J49/32

    CPC分类号： H01J49/32 ,  H01J49/105

    摘要： A mass spectrometer includes an inductive coupled plasma source whose flame is near ground potential, an interface, a flight tube, and an analyzer that includes magnetic and electric sectors, and an ion detector, which detector is operated at high voltage for ion acceleration. The magnetic sector includes a magnet and pole pieces that are insulated electrically relative to the flight tube. The pressure within the interface preferably does not exceed 10.sup.-3 mbar. By varying the magnetic field and the acceleration potential, identification of a specified mass over defined time intervals is carried out. The disclosed mass spectrometer provides improved coupling between the plasma ion source and a double-focussing analyzer, while advantageously providing a low voltage regime for the plasma source.

    摘要翻译： 质谱仪包括其火焰接近地电位的感应耦合等离子体源，界面，飞行管和包括磁性和电气部分的分析仪，以及离子检测器，该检测器以高电压操作用于离子加速。 磁性部件包括相对于飞行管电绝缘的磁体和极片。 界面内的压力优选不超过10-3毫巴。 通过改变磁场和加速电位，执行在规定的时间间隔内确定指定的质量。 所公开的质谱仪提供等离子体离子源和双重聚焦分析仪之间的改进的耦合，同时有利地为等离子体源提供低电压状态。

    Automatically controllable loading apparatus for mass spectrometers or the like
    7.
    发明授权
    Automatically controllable loading apparatus for mass spectrometers or the like 失效
    用于质谱仪等的自动控制加载装置

    公开(公告)号：US4405860A

    公开(公告)日：1983-09-20

    申请号：US225828

    申请日：1981-01-19

    申请人： Curt Brunnee ,  Lothar Delgmann ,  Gunter Marten

    发明人： Curt Brunnee ,  Lothar Delgmann ,  Gunter Marten

    IPC分类号： H01J49/04 ,  H01J49/26

    CPC分类号： H01J49/0413

    摘要： Automatically controllable loading apparatus for a mass spectrometer or like equipment comprises a rotatable disc for holding a plurality of sample carriers for successive movement into a transfer position. A push rod transfers successive sample carriers from the transfer position to a loading position. Guide means guide the push rod during its transfer movement. The guide means include a shut-off valve adjacent the loading position. Sealing means define in a fixed position between the valve and the transfer position at least one vacuum chamber adapted to be exhausted for the purpose of equalizing the pressure at opposite sides of said valve.

    摘要翻译： 用于质谱仪或类似设备的自动控制加载装置包括用于保持多个样品载体以用于连续移动到转移位置的可旋转盘。 推杆将连续的样品载体从转印位置传送到装载位置。 导向装置在传送运动期间引导推杆。 引导装置包括与装载位置相邻的截止阀。 密封装置在阀和转移位置之间的固定位置限定适于排出的至少一个真空室，用于均衡所述阀的相对侧的压力。