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1.发明授权
公开(公告)号：US4994105A
公开(公告)日：1991-02-19
申请号：US364933
申请日：1989-06-12
IPC分类号： A01N37/22 , C07C233/43
CPC分类号： A01N37/22 , C07C233/43
摘要： Compounds corresponding to the formula: ##STR1## wherein: each R.sub.1 is independently selected from H, a straight chain or branched C.sub.1 -C.sub.10 alkyl, C.sub.1 -C.sub.8 alkoxy, C.sub.2 -C.sub.10 alkenyl or C.sub.3 -C.sub.7 cycloalkenyl group;each R.sub.2 is independently selected from--CH.sub.2 (CH.sub.2).sub.m O(CH.sub.2).sub.n CH.sub.3 and ##STR2## wherein m and n are independently selected integers from 0 to 4, inclusive;each R.sub.3 is independently selected from a straight chain or branched C.sub.1 -C.sub.10 alkylene; andeach X is independently selected from F, Cl, Br or I.These compounds demonstrate utility as herbicidal and fungicidal compositions for controlling weeds and grasses in agricultrual crops.
摘要翻译： 对应于下式的化合物：其中：每个R 1独立地选自H，直链或支链C 1 -C 10烷基，C 1 -C 8烷氧基，C 2 -C 10烯基或C 3 -C 7环烯基; 每个R 2独立地选自-CH 2（CH 2）m O（CH 2）n CH 3和其中m和n独立地选自0至4的整数，包括0和4; 每个R 3独立地选自直链或支链C 1 -C 10亚烷基; 并且每个X独立地选自F，Cl，Br或I.这些化合物表现出用作控制农作物中的杂草和草的除草和杀真菌组合物。
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2.发明授权Alkenylated toluenediisocyanates for use in preparing polyurethane urea systems 失效用于制备聚氨酯脲体系的烯基化甲苯二异氰酸酯
公开(公告)号：US4794194A
公开(公告)日：1988-12-27
申请号：US888540
申请日：1986-07-21
CPC分类号： C07C265/12 , C08G18/8125
摘要： This invention relates to a class of alkenylated toluenediisocyanates having at least one alkenyl group ortho to an isocyanate group. More particularly the toluendiisocyanates are represented by the formula: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are hydrogen, C.sub.1-3 aliphatic, phenyl, halogen or alkoxy radicals, or R.sub.2 and R.sub.4 or R.sub.5 are bridged via an alkylene radical --(CH.sub.2).sub.y --wherein y=2 to 5, and x is one or two provided that in said formula at least one of R.sub.1, R.sub.2, R.sub.3, R.sub.4 or R.sub.5 is C.sub.1 or greater.The above described alkenylated toluenediisocyanates have been found to be well suited for preparing crosslinkable condensation polymers by providing pendant unsaturation for post curing and polymerization. They are also well suited for preparing polyurethane and polyurea elastomer systems.
摘要翻译： 本发明涉及一类具有至少一个与异氰酸酯基团邻接的烯基的烯基化甲苯二异氰酸酯。 更具体地，甲苯二异氰酸酯由下式表示：其中R 1，R 2，R 3，R 4和R 5是氢，C 1-3脂族基，苯基，卤素或烷氧基，或者R 2和R 4或R 5经由亚烷基 - （CH 2）y - ，其中y = 2至5，x为1或2，条件是在所述式中，R 1，R 2，R 3，R 4或R 5中的至少一个为C 1或更大。 已经发现上述烯基化甲苯二异氰酸酯通过提供用于后固化和聚合的侧基不饱和度而非常适用于制备可交联缩合聚合物。 它们也非常适合制备聚氨酯和聚脲弹性体体系。
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公开(公告)号：US4745223A
公开(公告)日：1988-05-17
申请号：US768885
申请日：1985-08-23
IPC分类号： C07C211/51 , C08G18/32 , C07C87/58
CPC分类号： C08G18/324 , C08G2120/00
摘要： This invention relates to a class of tertiary-alkyltoluenediamines having alkyl groups ortho to an amine group. More particularly the aromatic diamines are represented by the formulas: ##STR1## wherein R.sub.1, R.sub.2 and R.sub.3 are C.sub.1-3 alkyl groups or R.sub.2 and R.sub.3 are combined to form a C.sub.5-6 membered ring.The above described alkylated aromatic diamines have been found to be well suited for use as a chain extender in forming polyurethane/urea elastomer systems and the mono tert-butyltoluenediamine isomers have been found to be nonmutagenic in the Ames test.
摘要翻译： 本发明涉及一类具有与胺基邻位烷基的叔烷基甲苯二胺。 更具体地，芳族二胺由下式表示：其中R 1，R 2和R 3是C 1-3烷基或R 2和R 3结合形成C 5-6元环。 已经发现上述烷基化芳族二胺非常适合用作形成聚氨酯/脲弹性体体系的扩链剂，并且在Ames试验中已经发现单叔丁基甲苯二胺异构体是非引发剂。
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4.发明授权
公开(公告)号：US4714778A
公开(公告)日：1987-12-22
申请号：US837461
申请日：1986-03-07
IPC分类号： C09K15/18 , C07C67/00 , C07C209/00 , C07C209/68 , C07C211/49 , C07C211/50 , C07C213/00 , C07C217/76 , C08G18/32 , C08G18/67 , C08G18/81 , C09K15/20 , C07C87/58
CPC分类号： C08G18/675 , C08G18/676 , C08G18/8125 , C08G2120/00
摘要： This invention relates to a class of alkenylated toluenediamines having at least one alkenyl group ortho to an amine group. More particularly the toluenediamines are represented by the formula: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4 and R.sub.5 are hydrogen, C.sub.1-3 aliphatic, phenyl, halogen or alkoxy radicals, or R.sub.2 and R.sub.4 or R.sub.5 are bridged via an alkylene radical --(CH.sub.2).sub.y -- wherein y=2 to 5, and x is one or two provided that in said formula at least one of R.sub.1, R.sub.2, R.sub.3, R.sub.4 or R.sub.5 is C.sub.1 or greater.The above described alkenylated toluenediamines have been found to be well suited as antioxidants and as tri- and tetra functional chain extenders in forming polyurethane/urea elastomers systems and for providing pendant unsaturation for post curing and polymerization.
摘要翻译： 本发明涉及一类具有至少一个与氨基邻位的烯基的烯基化甲苯二胺。 更具体地，甲苯二胺由下式表示：其中R 1，R 2，R 3，R 4和R 5是氢，C 1-3脂族基，苯基，卤素或烷氧基，或者R 2和R 4或R 5经由亚烷基 - （CH 2）y - ，其中y = 2至5，x为1或2，条件是在所述式中，R 1，R 2，R 3，R 4或R 5中的至少一个为C 1或更大。 已经发现上述烯基化甲苯二胺在形成聚氨酯/尿素弹性体体系中非常适合作为抗氧化剂和作为三官能和四官能的增链剂，并且用于提供用于后固化和聚合的侧基不饱和度。
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5.发明授权N-tert-butyl derivatives of toluenediamine and mixtures as antioxidant for organic materials 失效甲苯二胺的N-叔丁基衍生物和作为有机材料的抗氧化剂的混合物
公开(公告)号：US4711737A
公开(公告)日：1987-12-08
申请号：US946564
申请日：1986-12-24
IPC分类号： C10M133/12 , C08K5/17 , C08L21/00 , C08L91/00 , C09K15/18 , C10L1/22 , C10L1/222 , C10N30/10
CPC分类号： C09K15/18
摘要： This invention relates to the use of tertiary butyl derivatives of toluenediamine and specifically N-tert-butyl-2,6-toluenediamine as an antioxidant material for preventing oxidation of organic materials.
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6.发明授权Polyalkylenecarbonate compositions with improved thermal stability and method for making same 失效具有改进的热稳定性的聚亚烷基碳酸酯组合物及其制备方法
公开(公告)号：US4303759A
公开(公告)日：1981-12-01
申请号：US186935
申请日：1980-09-12
申请人： Dale D. Dixon , Michael E. Ford
发明人： Dale D. Dixon , Michael E. Ford
摘要： Polyalkylene carbonates are stabilized against oxidative degradation by the inclusion therein of 0.2-10%, preferably 1-5%, of peroxyl-reactive sulphur-containing additive. Such compounds, found to be effective, are 3-t-butyl-4-hydroxy-5-methylphenyl sulfide, diphenyl sulfide, diphenyl sulfoxide, diphenyl sulfone, di-(p-tolyl sulfide) and sulphur.
摘要翻译： 聚碳酸亚烷基酯通过其中包含0.2-10％，优选1-5％的过氧化物反应性含硫添加剂来稳定，防止氧化降解。 发现有效的这些化合物是3-叔丁基-4-羟基-5-甲基苯基硫醚，二苯基硫醚，二苯基亚砜，二苯基砜，二（对甲苯基硫醚）和硫。
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7.发明授权Wet adhesion emulsions of polymer resins systems employed in water-based paint and coating compositions comprising as a component thereof monomer containing an ethylenic double bond and a ureido group polymerized therein 失效用于水性涂料和涂料组合物中的聚合物树脂体系的湿粘合乳液，其包含其中聚合有烯键式双键和脲基的作为其组分的组分
公开(公告)号：US4151142A
公开(公告)日：1979-04-24
申请号：US873813
申请日：1978-01-31
申请人： Frederick L. Herman , Dale D. Dixon
发明人： Frederick L. Herman , Dale D. Dixon
IPC分类号： C09K3/16 , A61K47/32 , C07D233/36 , C07D239/06 , C07D239/10 , C08F16/00 , C08F18/00 , C08F18/02 , C08F18/10 , C08F218/00 , C08F218/02 , C08F263/00 , C08L31/00 , C08L31/04 , C09D131/02 , D06M13/02 , D06M13/322 , D06M13/402 , D06M13/425 , D06M13/432 , D21H17/34 , D21H19/20 , C08L35/00
CPC分类号： D06M13/432 , C07D233/36 , C07D239/10 , C08F18/10 , C08K5/34 , C09D131/02 , D06M13/425
摘要： Improved wet adhesion properties of water-based paints and coating compositions are obtained by incorporating into the polymeric resin emulsion systems employed in the formulation of such paints or coating compositions a monomeric compound having a terminal ureido group at one end thereof and a vinyl terminal group at the opposite end. Such incorporated monomeric compounds correspond to the general formula ##STR1## wherein R is H or CH.sub.3, U designates a cyclic or acyclic ureido or thioureido group and L designates a selected linking structure. In the simplest of such monomeric compounds, L is --CH.sub.2 --, as specifically represented by allyl urea. In other representative compounds the linking group L may be a polymethylene group - (CH.sub.2).sub.n --or the chain may contain one or more oxy (ether), amino, amido or carbonyl groups, provided that any carbonyl group (CO) present is not directly attached to U or to an ethylenic carbon atom nor is such ethylenic carbon directly attached to a nitrogen atom. Among preferred monomeric compounds imparting such improved wet adhesion are: N-Beta-allylaminoethyl ethylene urea, allyloxy-N-B-(1-ethylene ureido) ethyl acetamide, and allyl ester of N-ethyl-B-(1-ethylene ureido)-N-methyl carbamate. The polymer resin in the emulsion is one formed from one or more ethylenically unsaturated monomer compounds, such as acrylates and methacrylates, vinyl esters, vinyl chloride, mono- or di-ethylenic hydrocarbons; or copolymers, interpolymers or blends of these.
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公开(公告)号：US4137280A
公开(公告)日：1979-01-30
申请号：US897627
申请日：1978-04-19
申请人： Dale D. Dixon , Michael E. Ford
发明人： Dale D. Dixon , Michael E. Ford
摘要： This invention relates to a polyvinyl chloride composition having blended therein from about 5-60% of a polyalkylene carbonate formed by reacting an alkylene oxide and carbon dioxide. The polyalkylene carbonate is added to improve the melt flow indices and oxygen barrier characteristics of the polyvinyl chloride.
摘要翻译： 本发明涉及一种聚氯乙烯组合物，其中约5-60％由烯化氧与二氧化碳反应形成的聚亚烷基碳酸酯混合。 加入聚碳酸亚烷基酯以改善聚氯乙烯的熔体流动指数和氧阻隔特性。
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9.发明授权
公开(公告)号：US4066630A
公开(公告)日：1978-01-03
申请号：US757909
申请日：1977-01-10
CPC分类号： C08G64/0208 , C08G63/64 , C08G64/34
摘要： Polycarbonates, of the type formed by reacting an aliphatic or cycloaliphatic 1,2-monoepoxide with carbon dioxide and having substantially alternating units of epoxide and carbon dioxide, are improved in thermal stability by reacting the free hydroxyl groups thereon with a hydroxyl reactive organic compound.
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公开(公告)号：US3940520A
公开(公告)日：1976-02-24
申请号：US443460
申请日：1974-02-19
申请人： Dale D. Dixon , Larry J. Hayes
发明人： Dale D. Dixon , Larry J. Hayes
摘要： This invention relates to a process for improving the water wicking and moisture transport properties of synthetic resins, e.g., fiber form polyamides, polyesters, polyolefins, and polyacrylonitriles, which comprises sulfofluorinating said resins in a self-activating gaseous reaction medium containing from about 0.1-20% by volume elemental fluorine, 0.1-50% by volume of sulfur dioxide, 0-21% by volume oxygen, and the balance inert for providing from 1 .times. 10.sup.-.sup.9 to 1 .times. 10.sup.-.sup.3 milligrams fluorine and sulfur per square centimeter of resin surface.
摘要翻译： 本发明涉及一种改善合成树脂（例如纤维形式聚酰胺，聚酯，聚烯烃和聚丙烯腈）的吸水性和湿气输送性能的方法，该方法包括在含有约0.1-约0.1重量份的自激活气态反应介质中使所述树脂磺化氟化， 20体积％的元素氟，0.1〜50体积％的二氧化硫，0〜21体积％的氧，余量为1×10 -9〜1×10 -3毫克的氟和 硫磺每平方厘米的树脂表面。
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