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    Adducts of mid-range vinylidene content polyisobutylene polymer products and methods for making the same
    4.
    发明授权
    Adducts of mid-range vinylidene content polyisobutylene polymer products and methods for making the same 有权
    中等偏二氯乙烯含量聚异丁烯聚合物产品的加合物及其制备方法

    公开(公告)号：US07091285B2

    公开(公告)日：2006-08-15

    申请号：US10896792

    申请日：2004-07-22

    申请人： C. Edward Baxter, Jr. ,  Christopher Lobue ,  Gilbert Valdez ,  Daniel Herndon ,  Timothy Lowry

    发明人： C. Edward Baxter, Jr. ,  Christopher Lobue ,  Gilbert Valdez ,  Daniel Herndon ,  Timothy Lowry

    IPC分类号： C08F8/46

    CPC分类号： C08F110/10 ,  C08F10/00 ,  C08F10/10 ,  C08F110/14 ,  C08F210/10 ,  Y10S525/911 ,  C08F2/14 ,  C08F4/14 ,  C08F2500/08 ,  C08F2500/20 ,  C08F2500/02 ,  C08F210/08 ,  C08F2/01

    摘要： A reaction product comprising an adduct of a mid-range vinylidene content PIB polymer composition and maleic anhydride, a phenolic compound or a compound having a reactive site for subsequent amination. The PIB composition comprises a relatively low molecular weight, mid-range vinylidene content PIB polymer product wherein at least about 90% of the PIB molecules present in the product comprise alpha or beta position isomers. The vinylidene (alpha) isomer content of the product may range from 20% to 70% thereof and the content of tetra-substituted internal double bonds is very low, preferably less than about 5% and ideally less than about 1–2%. The mid-range vinylidene content PIB polymer products may be prepared employing a liquid phase polymerization process conducted in a loop reactor at a temperature of at least 60° F. using a BF3/methanol catalyst complex and a contact time of no more than 4 minutes.

    摘要翻译： 一种反应产物，其包含中等偏
    二氯乙烯含量的PIB聚合物组合物和马来酸酐的加合物，酚类化合物或具有用于随后胺化的反应性位点的化合物。 PIB组合物包含相对低分子量的中程偏二氟乙烯含量的PIB聚合物产物，其中存在于产物中的至少约90％的PIB分子包含α或β位异构体。 产物的亚乙烯基（α）异构体含量可以在20％至70％的范围内，四取代的内部双键的含量非常低，优选小于约5％，理想地小于约1-2％。 中等范围的亚乙烯基含量的PIB聚合物产物可以使用在环流反应器中在至少60°F的温度下进行的液相聚合方法制备，使用BF 3 /甲醇催化剂络合物和 接触时间不超过4分钟。

    Apparatus for preparing polyolefin products and methodology for using the same
    7.
    发明授权
    Apparatus for preparing polyolefin products and methodology for using the same 有权
    用于制备聚烯烃产品的设备及其使用方法

    公开(公告)号：US06844401B2

    公开(公告)日：2005-01-18

    申请号：US10758499

    申请日：2004-01-15

    申请人： C. Edward Baxter, Jr. ,  Daniel Herndon ,  James G. Wakeland ,  Russel E. Reid, Sr. ,  Gilbert Valdez

    发明人： C. Edward Baxter, Jr. ,  Daniel Herndon ,  James G. Wakeland ,  Russel E. Reid, Sr. ,  Gilbert Valdez

    IPC分类号： B01J8/00 ,  B01J8/20 ,  B01J19/24 ,  C08F2/00 ,  C08F2/40 ,  C08F6/02 ,  C08F10/00

    CPC分类号： B01J19/2425 ,  B01J8/007 ,  B01J8/20 ,  B01J19/2405 ,  B01J19/2465 ,  B01J2208/00212 ,  B01J2208/00283 ,  B01J2219/00006 ,  B01J2219/00038 ,  B01J2219/00085 ,  B01J2219/0011 ,  B01J2219/00272 ,  C08F6/02 ,  C08F10/00 ,  C08L23/00

    摘要： Apparatus for olefin polymerization includes a plurality of shell and tube olefin polymerization reactors, each of which has an olefin polymerization reaction mixture inlet connection and a crude polyolefin product outlet connection. Each reactor is equipped with a recirculation system including a pump arranged to circulate a reaction mixture through the tube side of the reactor independently of the introduction of olefin polymerization reaction mixture into the reactor. The apparatus also includes an inlet reaction mixture distribution manifold and an outlet polymerization reaction mixture collection manifold interconnecting the reactors for operation in parallel. The apparatus also includes catalyst composition and catalyst modifier inlets for each reactor arranged such that a catalyst modifier to may be introduced into each reactor at a rate which is independent of the introduction of catalyst composition. The apparatus further incorporates a crude polyolefin product catalyst removal and wash system including a plurality of settler vessels, associated piping and an inlet for a catalyst killing agent. This crude polyolefin product catalyst removal and wash system operates to receive crude polyolefin product from the crude polyolefin product outlet and remove residual catalyst therefrom.

    摘要翻译： 用于烯烃聚合的设备包括多个壳和管烯烃聚合反应器，每个反应器具有烯烃聚合反应混合物入口连接和粗聚烯烃产物出口连接。 每个反应器配备有循环系统，其包括泵，其被布置成使反应混合物循环通过反应器的管侧，而与将烯烃聚合反应混合物引入反应器中无关。 该装置还包括入口反应混合物分配歧管和出口聚合反应混合物收集歧管，其将反应器互连以并行操作。 该装置还包括用于每个反应器的催化剂组合物和催化剂改性剂入口，其布置成使催化剂改性剂以不同于引入催化剂组合物的速率引入每个反应器中。 该装置还包括粗聚烯烃产物催化剂去除和洗涤系统，其包括多个沉降器容器，相关联的管道和用于催化剂杀伤剂的入口。 该粗聚烯烃产物催化剂去除和洗涤系统用于从粗聚烯烃产物出口接收粗聚烯烃产物并从其中除去残留的催化剂。