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    HYDROXYL TERMINATED PRECURSOR AND METHOD OF MAKING THE SAME
    2.
    发明申请
    HYDROXYL TERMINATED PRECURSOR AND METHOD OF MAKING THE SAME 有权
    羟基封端的前体及其制备方法

    公开(公告)号：US20090054611A1

    公开(公告)日：2009-02-26

    申请号：US11842903

    申请日：2007-08-21

    申请人： THOMAS N. JONES ,  Edmund J. Madaj

    发明人： THOMAS N. JONES ,  Edmund J. Madaj

    IPC分类号： C08G71/04

    CPC分类号： C08G18/6696 ,  C08G18/36

    摘要： A method of making a hydroxyl terminated precursor for polyurethane is disclosed. The method comprises heating a vegetable oil-polyol mixture of modified vegetable oil containing about two or more hydroxyl groups per molecule and a polyether polyol having about two or more hydroxyl groups per molecule at a temperature of at least about 25 degrees Celsius and at a pressure of about 1 atmosphere. The mixture has a hydroxyl equivalent ratio of about 1:1 vegetable oil to polyol. The method further comprises mixing for at least about 10 minutes an isocyanate containing about two or more isocyanato groups per molecule at least about 25 degrees Celsius to the vegetable oil-polyol mixture at a molar equivalent ratio of at least 2:1 vegetable oil-polyol mixture to isocyanate to react the isocyanate with the mixture to form the hydroxyl terminated precursor.

    摘要翻译： 公开了制备羟基封​​端的聚氨酯前体的方法。 该方法包括加热每分子含有约两个或更多个羟基的改性植物油的植物油 - 多元醇混合物和每分子具有约两个或多个羟基的聚醚多元醇，其温度为至少约25摄氏度和压力 约1个大气。 该混合物具有约1:1植物油与多元醇的羟基当量比。 该方法还包括将至少约10分钟的异氰酸酯以至少约25℃的至少约25摄氏度的至少约2:1的植物油 - 多元醇混合物的摩尔当量比混合至含有约两个或更多个异氰酸酯基的异氰酸酯基团 与异氰酸酯混合以使异氰酸酯与混合物反应以形成羟基封端的前体。

    Hydroxyl terminated precursor and method of making the same
    4.
    发明授权
    Hydroxyl terminated precursor and method of making the same 有权
    羟基封端的前体及其制备方法

    公开(公告)号：US08722753B2

    公开(公告)日：2014-05-13

    申请号：US11842903

    申请日：2007-08-21

    申请人： Thomas N. Jones ,  Edmund J. Madaj

    发明人： Thomas N. Jones ,  Edmund J. Madaj

    IPC分类号： C08G18/00 ,  C08L91/00

    CPC分类号： C08G18/6696 ,  C08G18/36

    摘要： A method of making a hydroxyl terminated precursor for polyurethane is disclosed. The method comprises heating a vegetable oil-polyol mixture of modified vegetable oil containing about two or more hydroxyl groups per molecule and a polyether polyol having about two or more hydroxyl groups per molecule at a temperature of at least about 25 degrees Celsius and at a pressure of about 1 atmosphere. The mixture has a hydroxyl equivalent ratio of about 1:1 vegetable oil to polyol. The method further comprises mixing for at least about 10 minutes an isocyanate containing about two or more isocyanato groups per molecule at least about 25 degrees Celsius to the vegetable oil-polyol mixture at a molar equivalent ratio of at least 2:1 vegetable oil-polyol mixture to isocyanate to react the isocyanate with the mixture to form the hydroxyl terminated precursor.

    摘要翻译： 公开了制备羟基封​​端的聚氨酯前体的方法。 该方法包括加热每分子含有约两个或更多个羟基的改性植物油的植物油 - 多元醇混合物和每分子具有约两个或多个羟基的聚醚多元醇，其温度为至少约25摄氏度和压力 约1个大气。 该混合物具有约1:1植物油与多元醇的羟基当量比。 该方法还包括将至少约10分钟的异氰酸酯以至少约25℃的至少约25摄氏度的至少约2:1的植物油 - 多元醇混合物的摩尔当量比混合至约2或更多个异氰酸酯基团 与异氰酸酯混合以使异氰酸酯与混合物反应以形成羟基封端的前体。

    Isocyanato terminated precursor and method of making the same
    5.
    发明授权
    Isocyanato terminated precursor and method of making the same 有权
    异氰酸酯封端的前体及其制备方法

    公开(公告)号：US07678936B2

    公开(公告)日：2010-03-16

    申请号：US11842889

    申请日：2007-08-21

    申请人： Thomas N. Jones ,  Edmund J. Madaj

    发明人： Thomas N. Jones ,  Edmund J. Madaj

    IPC分类号： C08G18/12 ,  C08G18/66 ,  C08G18/36 ,  C08G18/76

    CPC分类号： C08G18/7671 ,  C08G18/36 ,  C08G2101/00

    摘要： A method of making an isocyanato terminated precursor for polyurethane is disclosed. The method comprises heating an isocyanate containing about two or more isocyanato groups per molecule at a temperature of up to 80 degrees Celsius and at a pressure of about 1 atmosphere. The method further comprises mixing a modified vegetable oil comprising about two or more hydroxyl groups per molecule with the isocyanate at a molar equivalent ratio of at least 2:1 isocyanate to vegetable oil for a predetermined time period to form the isocyanato terminated precursor.

    摘要翻译： 公开了一种制备用于聚氨酯的异氰酸酯酯封端的前体的方法。 该方法包括在高达80摄氏度的温度和约1大气压的压力下加热每分子含有大约两个或更多个异氰酸酯基的异氰酸酯。 该方法还包括将每分子含有约两个或多个羟基的改性植物油与异氰酸酯以至少2:1异氰酸酯的摩尔当量比与植物油混合预定时间以形成异氰酸酯酯基封端的前体。

    Flexible, combustion-modified, polyurethane foams
    7.
    发明授权
    Flexible, combustion-modified, polyurethane foams 失效
    柔性，燃烧改性的聚氨酯泡沫

    公开(公告)号：US5229427A

    公开(公告)日：1993-07-20

    申请号：US893472

    申请日：1992-06-02

    申请人： Edmund J. Madaj

    发明人： Edmund J. Madaj

    IPC分类号： C08L75/00 ,  C08G18/38 ,  C08G18/48 ,  C08G18/76 ,  C08K5/3492 ,  C08K5/51

    CPC分类号： C08K5/34922 ,  C08G18/3851 ,  C08G18/4816 ,  C08G18/7664 ,  C08K5/51 ,  C08G2101/0008 ,  C08G2101/0058 ,  C08G2101/0083 ,  Y10S521/906

    摘要： Polyurethane foams of excellent properties are produced by reacting a) one or more polyether polyols, b) a polymethylene poly(phenyl isocyanate) having a methylene-bis(phenyl isocyanate) content of from 70 to 77% by weight, c) melamine, d) a phosphorous containing compound and d) water as the blowing agent. The isocyanate must have a specific 4,4' to 2,4'-isomer ratio and the amounts of melamine and phosphorous must be within narrowly defined limits.

    摘要翻译： 具有优异性能的聚氨酯泡沫体通过使a）一种或多种聚醚多元醇，b）具有70至77重量％亚甲基 - 双（苯基异氰酸酯）含量的多亚甲基聚（苯基异氰酸酯）反应，c）三聚氰胺，d ）含磷化合物和d）水作为发泡剂。 异氰酸酯必须具有特定的4,4'至2,4'异构体比例，三聚氰胺和磷的量必须在限定范围内。

    ISOCYANATO TERMINATED PRECURSOR AND METHOD OF MAKING THE SAME
    8.
    发明申请
    ISOCYANATO TERMINATED PRECURSOR AND METHOD OF MAKING THE SAME 审中-公开
    ISOCYANATO终止前身及其制造方法

    公开(公告)号：US20100160593A1

    公开(公告)日：2010-06-24

    申请号：US12719892

    申请日：2010-03-09

    申请人： Thomas N. Jones ,  Edmund J. Madaj

    发明人： Thomas N. Jones ,  Edmund J. Madaj

    IPC分类号： C08G18/34

    CPC分类号： C08G18/7671 ,  C08G18/36 ,  C08G2101/00

    摘要： A method of making an isocyanato terminated precursor for polyurethane is disclosed. The method comprises heating an isocyanate containing about two or more isocyanato groups per molecule at a temperature of up to 80 degrees Celsius and at a pressure of about 1 atmosphere. The method further comprises mixing a modified vegetable oil comprising about two or more hydroxyl groups per molecule with the isocyanate at a molar equivalent ratio of at least 2:1 isocyanate to vegetable oil for a predetermined time period to form the isocyanato terminated precursor.

    摘要翻译： 公开了一种制备用于聚氨酯的异氰酸酯酯封端的前体的方法。 该方法包括在高达80摄氏度的温度和约1大气压的压力下加热每分子含有大约两个或更多个异氰酸酯基的异氰酸酯。 该方法还包括将每分子含有约两个或多个羟基的改性植物油与异氰酸酯以至少2:1异氰酸酯的摩尔当量比与植物油混合预定时间以形成异氰酸酯酯基封端的前体。

    Allophanate-modified diphenylmethane diisocyanates and processes for their production and use
    10.
    发明授权
    Allophanate-modified diphenylmethane diisocyanates and processes for their production and use 失效
    脲基甲酸酯改性二苯基甲烷二异氰酸酯及其生产和使用的方法

    公开(公告)号：US5663272A

    公开(公告)日：1997-09-02

    申请号：US577580

    申请日：1995-12-22

    申请人： William E. Slack ,  Edmund J. Madaj ,  David D. Steppan

    发明人： William E. Slack ,  Edmund J. Madaj ,  David D. Steppan

    IPC分类号： C08G18/78 ,  C08G18/71

    CPC分类号： C08G18/7837 ,  C08G2120/00

    摘要： Allophanate-modified MDI which is a storage stable liquid at 25.degree. C. is produced by reacting a monoisocyanate and an organic material having at least two hydroxyl groups and a molecular weight of from about 60 to about 6,000 to form a urethane. The urethane is then reacted with and isomeric mixture of MDI in an amount such that the product isocyanate will have an NCO content of from about 12 to about 30%. The isomeric mixture of MDI is composed of 4,4'-diphenylmethane diisocyanate containing from 0 to about 60% by weight 2,4'-MDI and less than 6% by weight of the 2,2'-MDI. This allophanate-modified MDI is further reacted with an organic isocyanate-reactive material to produce an allophanate-modified MDI prepolymer containing urethane, urea and/or biuret groups having an NCO content which is generally from about 5 to about 29% by weight. The prepolymers of this invention are particularly useful in reaction injection molding processes because they give molded articles having improved flex modulus.

    摘要翻译： 通过使单异氰酸酯和具有至少两个羟基并且分子量为约60至约6,000的有机材料反应形成氨基甲酸酯来制备作为25℃储存稳定液体的脲基甲酸酯改性MDI。 然后将氨基甲酸酯与MDI的异构体混合物反应，其量使得产物异氰酸酯的NCO含量为约12至约30％。 MDI的异构体混合物由含有0至约60重量％的2,4'-MDI和小于6重量％的2,2'-MDI的4,4'-二苯基甲烷二异氰酸酯组成。 该脲基甲酸酯改性的MDI进一步与有机异氰酸酯反应性材料反应以产生含有通常为约5至约29重量％的NCO含量的氨基甲酸酯，脲和/或缩二脲基团的脲基甲酸酯改性的MDI预聚物。 本发明的预聚物在反应注射成型工艺中特别有用，因为它们具有改进的挠曲模量的模塑制品。