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1.发明授权Catalyst demetallization by converting the metal poisons to a sulfur containing metal compound having a defined low amount of sulfur 失效通过将金属毒物转化为具有确定的低量硫的含硫金属化合物来进行催化剂脱金属化
公开(公告)号：US4293403A
公开(公告)日：1981-10-06
申请号：US756581
申请日：1977-01-03
申请人： Emmett H. Burk, Jr. , Jin S. Yoo , John A. Karch , Jui-Yuan Sun
发明人： Emmett H. Burk, Jr. , Jin S. Yoo , John A. Karch , Jui-Yuan Sun
CPC分类号： B01J29/90 , B01J21/20 , B01J37/20 , C10G11/04 , Y10S502/521
摘要： A process for the removal of metal poisons such as nickel, iron and/or vanadium from a hydrocarbon conversion catalyst which includes the step of contacting the catalyst with a sulfur-containing compound to convert at least a portion of the metals on the catalyst to a sulfur-containing metal compound. The weight % sulfur on the thus treated catalyst is controlled to about 40-90%, preferably about 40-75%, of the weight % of the total nickel, vanadium and iron on the catalyst. Preferably, the sulfur-containing compound is hydrogen sulfide in admixture with a reducing gas such as hydrogen and/or carbon monoxide. This step facilitates metal removal in subsequent processing steps.
摘要翻译： 一种用于从烃转化催化剂中除去诸如镍，铁和/或钒的金属毒物的方法，该方法包括使催化剂与含硫化合物接触以将至少一部分催化剂上的金属转化为 含硫金属化合物。 这样处理的催化剂上的重量％硫被控制在催化剂上总镍，钒和铁的重量％的约40-90％，优选约40-75％。 优选地，含硫化合物是与还原气体如氢气和/或一氧化碳混合的硫化氢。 该步骤有助于后续加工步骤中的金属去除。
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公开(公告)号：US4270927A
公开(公告)日：1981-06-02
申请号：US50264
申请日：1979-06-19
摘要： A process for reducing the sulfur and ash content of coal wherein coal particles are treated in an aqueous slurry with a minor amount of hydrocarbon oil to form coal-oil aggregates having modified particle size and density characteristics. The coal-oil aggregates are separated from ash and mineral matter in the slurry by size separation means. Optionally, the coal particles may be treated with a conditioning agent prior to the aggregation step. Recovered coal particles comprise a substantial part of the feed carbon values.
摘要翻译： 一种降低煤的硫和灰分含量的方法，其中煤颗粒在具有少量烃油的含水浆料中处理以形成具有改进的粒径和密度特性的煤 - 油聚集体。 煤油聚集体通过尺寸分离装置与浆料中的灰分和矿物质分离。 任选地，煤颗粒可以在聚集步骤之前用调节剂处理。 回收的煤颗粒占进料碳值的很大一部分。
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公开(公告)号：US4249910A
公开(公告)日：1981-02-10
申请号：US944452
申请日：1978-09-21
CPC分类号： C10L9/00
摘要： A process for reducing the sulfur and ash content of coal comprising the steps of:(1) contacting coal particles containing ash and iron pyrite mineral matter with a promoting amount of at least one conditioning agent capable of modifying or altering the existing surface characteristics of the pyrite under conditions to effectuate alteration or modification of at least a portion of the contained pyritic sulfur;(2) agglomerating the coal particles while said surfaces are altered or modified in an aqueous medium with hydrocarbon oil; and(3) recovering coal hydrocarbon oil agglomerates wherein the coal exhibits reduced sulfur and ash content.
摘要翻译： 一种减少煤的硫和灰分含量的方法，包括以下步骤：（1）使含有灰分和铁黄铁矿矿物质的煤颗粒与促进量的至少一种调节剂接触，所述调节剂能够改变或改变现有的表面特性 黄铁矿在条件下进行至少部分含硫黄硫的改变或改性; （2）在具有烃油的水性介质中改变或改性所述表面时，使煤颗粒凝聚; 和（3）回收煤炭烃油附聚物，其中煤表现出降低的硫和灰分含量。
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公开(公告)号：US4204840A
公开(公告)日：1980-05-27
申请号：US916667
申请日：1978-06-19
申请人： Jin S. Yoo , Emmett H. Burk, Jr. , John A. Karch
发明人： Jin S. Yoo , Emmett H. Burk, Jr. , John A. Karch
CPC分类号： C10L9/02
摘要： A process for reducing the pyritic sulfur content of coal comprising the steps of:(1) contacting an aqueous slurry of water, an alkaline earth metal base and pyrite-containing coal at elevated temperature with oxygen, said alkaline earth metal base being present in an amount at least equal to the stoichiometric amount of pyrite, and said aqueous slurry being maintained at a pH of from about 5.0 to about 12.0; and(2) recovering coal particles of reduced pyritic sulfur content.
摘要翻译： 一种降低煤的黄铁矿硫含量的方法，包括以下步骤：（1）在升高的温度下将水，碱土金属碱和含黄铁矿的煤的含水浆料与氧接触，所述碱土金属碱存在于 至少等于黄铁矿的化学计量量，并且所述含水浆料保持在约5.0至约12.0的pH; 和（2）回收硫化黄硫含量降低的煤颗粒。
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5.发明授权Process for removing sulfur from coal employing aqueous solutions of sulfites and bisulfites 失效使用亚硫酸盐和亚硫酸氢盐的水溶液从煤中除去硫的方法
公开(公告)号：US4155717A
公开(公告)日：1979-05-22
申请号：US866592
申请日：1978-01-03
申请人： Jui-Yuan Sun , Jin S. Yoo , Emmett H. Burk, Jr.
发明人： Jui-Yuan Sun , Jin S. Yoo , Emmett H. Burk, Jr.
CPC分类号： C10L9/02
摘要： A process for reducing the sulfur content of coal comprising the steps of:(1) contacting coal particles with an aqueous solution of compositions selected from the group comprising alkali metal and alkaline earth metal sulfites and bisulfites to reduce the sulfur content of the coal; and(2) recovering coal particles of reduced sulfur content.
摘要翻译： 一种降低煤的硫含量的方法，包括以下步骤：
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6.发明授权Polyfunctional aliphatic and cycloaliphatic cyclic nitrile sulfites and carbonates 失效多官能脂族和脂环族腈亚硫酸盐和碳酸盐
公开(公告)号：US3979401A
公开(公告)日：1976-09-07
申请号：US442706
申请日：1974-02-27
IPC分类号： C07D273/00 , C07D291/04 , C08G18/70
CPC分类号： C07D291/04 , C07D273/00 , C08G18/701
摘要： The disclosure is of compounds of the formula: ##EQU1## WHEREIN R is aliphatic hydrocarbon, X is sulfur (S) or carbon (C) and n is an integer of 1 to 3. The compounds are useful as easily-storable, polyisocyanate generators, especially the essentially-chlorine free compounds.
摘要翻译： 本公开是下式的化合物：OO PARALLEL PARALLEY XX ANGLE ANGLE OOOO |||| N = C-R-C = N n WHEREIN R是脂族烃，X是硫（S）或碳（C）和 n为1〜3的整数。该化合物可用作容易储存的多异氰酸酯发生剂，特别是基本上不含氯的化合物。
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7.发明授权
公开(公告)号：US4735705A
公开(公告)日：1988-04-05
申请号：US048623
申请日：1987-05-11
CPC分类号： C10G11/04 , C10G11/05 , Y10S502/524
摘要： An improved process for converting hydrocarbons using a catalyst which is periodically regenerated to remove carbonaceous deposits, the catalyst being comprised of a mixture containing, as a major component, solid particles capable of promoting hydrocarbon conversion at hydrocarbon conversion conditions, and, as a minor component, discrete entities comprising at least one spinel, preferably alkaline earth metal-containing spinel, and a minor amount of at least one added component selected from the group consisting of alkali metal components, calcium components, barium components, strontium components, beryllium components and mixtures thereof.
摘要翻译： 一种使用周期性再生以除去含碳沉积物的催化剂转化烃的改进方法，该催化剂由含有作为主要组分的能够在烃转化条件下促进烃转化的固体颗粒和作为次要组分的混合物 ，包含至少一种尖晶石，优选含碱土金属的尖晶石和少量至少一种选自碱金属组分，钙组分，钡组分，锶组分，铍组分和混合物的至少一种添加组分的离散实体 其中。
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公开(公告)号：US4295858A
公开(公告)日：1981-10-20
申请号：US126248
申请日：1980-03-03
摘要： A process for reducing the sulfur and ash content of coal comprising the steps of: (1) contacting coal particles containing ash and iron pyrite mineral matter with a promoting amount of at least one conditioning agent, said conditioning agent having a ferrous component maintained at a pH of from about 5.5 to 11.0 and being capable of modifying or altering the existing surface characteristics of the pyrite under conditions to effectuate alteration of modification of at least a portion of the contained pyritic sulfur; (2) agglomerating the coal particles while said pyrite surfaces are altered or modified in an aqueous medium with hydrocarbon oil to form coal-hydrocarbon oil agglomerates; (3) separating said coal-hydrocarbon oil agglomerates from pyrite mineral matter and ash to recover coal-hydrocarbon oil agglomerates wherein the coal exhibits reduced sulfur and ash content.
摘要翻译： 一种减少煤的硫和灰分含量的方法，包括以下步骤：（1）使含有灰分和铁黄铁矿矿物质的煤颗粒与促进量的至少一种调节剂接触，所述调理剂具有维持在 pH为约5.5至11.0，并且在条件下能够改变或改变黄铁矿的现有表面特性，以实现至少部分含硫黄硫的改性改性; （2）在含烃油的含水介质中改变或改性所述黄铁矿表面的同时使煤颗粒凝聚，形成煤 - 烃油附聚物; （3）将煤 - 烃油附聚物与黄铁矿矿物和灰分离，以回收煤 - 烃油附聚物，其中煤表现出降低的硫和灰分含量。
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公开(公告)号：US4270926A
公开(公告)日：1981-06-02
申请号：US50262
申请日：1979-06-19
CPC分类号： B03D1/02 , B03D1/1431 , C10L9/00
摘要： A process for reducing the sulfur and ash content of coal wherein coal particles are treated in an aqueous slurry with a minor amount of hydrocarbon oil to form coal-oil aggregates. The coal-oil aggregates are separated from ash and mineral matter in the slurry by dissolved gas flotation. Optionally, the coal particles may be treated with a conditioning agent prior to the aggregation step. Recovered coal particles comprise a substantial part of the feed carbon values.
摘要翻译： 一种降低煤的硫和灰分含量的方法，其中煤颗粒在具有少量烃油的含水浆料中处理以形成煤 - 油聚集体。 煤油聚集体通过溶解气体浮选与浆料中的灰分和矿物质分离。 任选地，煤颗粒可以在聚集步骤之前用调节剂处理。 回收的煤颗粒占进料碳值的很大一部分。
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公开(公告)号：US4234452A
公开(公告)日：1980-11-18
申请号：US23559
申请日：1979-03-26
申请人： Emmett H. Burk, Jr. , Jin S. Yoo , Jui-Yuan Sun , John A. Karch
发明人： Emmett H. Burk, Jr. , Jin S. Yoo , Jui-Yuan Sun , John A. Karch
IPC分类号： B01J21/20 , B01J29/90 , C10G11/02 , C10G35/06 , C10G49/02 , B01J29/38 , C10G11/04 , C10G11/05
摘要： An improved demetallization process is disclosed comprising high pressure aqueous phase oxidation of a catalyst contaminated with a metal such as nickel, vanadium, copper and/or iron. The metal-contaminated catalyst can be oxidized in an aqueous phase at high pressure either before regeneration or subsequent to regeneration. Optionally, an oxidative and reductive wash can also be employed.
摘要翻译： 公开了一种改进的脱金属工艺，其包括被金属如镍，钒，铜和/或铁污染的催化剂的高压水相氧化。 金属污染的催化剂可以在再生之前或再生之后在高压下在水相中氧化。 任选地，还可以使用氧化还原洗涤。
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