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    3,5-dimethyl-pentenyl-dihydro-2(3H)-furanone isomer mixtures, organoleptic uses thereof, process for preparing same and process intermediates therefor
    1.
    发明授权
    3,5-dimethyl-pentenyl-dihydro-2(3H)-furanone isomer mixtures, organoleptic uses thereof, process for preparing same and process intermediates therefor 失效
    3,5-二甲基 - 戊烯基 - 二氢-2（3H） - 呋喃酮异构体混合物，其感官用途，制备方法及其中间体

    公开(公告)号：US5478803A

    公开(公告)日：1995-12-26

    申请号：US330847

    申请日：1994-10-27

    Applicant: Richard M. Boden ,  William J. Fylak ,  Marie R. Hanna ,  Futoshi Fujioka

    Inventor： Richard M. Boden ,  William J. Fylak ,  Marie R. Hanna ,  Futoshi Fujioka

    IPC: C07C69/587 ,  C11B9/00 ,  C11D3/50 ,  A61K7/46

    CPC classification number: C11D3/50 ,  C11B9/0076

    Abstract: Described are 3,5-dimethyl-pentenyl-dihydro-2(3H)-furanone isomer mixtures defined according to the structure: ##STR1## wherein structure represents mixtures wherein in the mixture in each of the compounds, one of the dashed lines represents a carbon-carbon double bond and the other of the dashed lines represents a carbon-carbon single bond, processes for preparing same and uses thereof in augmenting or enhancing the aroma of consumable materials including perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, hair preparations, fabric softeners, fabric softener articles, cosmetic powders and perfumed polymers). Also described is a process for preparing such 3,5-dimethyl-pentenyl-dihydro-2(3H)-furanone isomer mixtures using as a starting material 2,7-octadienol having the structure: ##STR2## as well as the process intermediates having the structures: ##STR3## wherein R represents C.sub.1 -C.sub.4 alkyl; R.sub.1 and R.sub.2 are the same or different and each represents 2,7-octadienyl or R.

    Abstract translation: 描述的是根据以下结构定义的3,5-二甲基 - 戊烯基 - 二氢-2（3H） - 呋喃酮异构体混合物：其中结构表示混合物，其中在每个化合物的混合物中，虚线之一表示 碳 - 碳双键，虚线中的另一个代表碳 - 碳单键，其制备方法及其用于增强或增强消耗材料的香气，包括香料组合物，古龙水和香料制品（例如固体或液体 阴离子，阳离子，非离子或两性离子洗涤剂，毛发制剂，织物柔软剂，织物柔软剂制品，化妆粉和加香聚合物）。 还描述了使用具有以下结构的起始原料2,7-辛二烯醇制备这种3,5-二甲基 - 戊烯基 - 二氢-2（3H） - 呋喃酮异构体混合物的方法，以及具有 结构： 和其中R表示C1-C4烷基; R1和R2相同或不同，各自表示2,7-辛二烯基或R.

    Tertiary hydroxyl carboxaldehydes, organoleptic uses thereof, and processes for producing same
    4.
    发明授权
    Tertiary hydroxyl carboxaldehydes, organoleptic uses thereof, and processes for producing same 失效
    叔羟基醛，其感官用途及其制备方法

    公开(公告)号：US4554385A

    公开(公告)日：1985-11-19

    申请号：US709916

    申请日：1985-03-08

    Applicant: Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    Inventor： Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    IPC: C07C47/36 ,  C07C47/19

    CPC classification number: C07C47/36

    Abstract: Described are tertiary hydroxyl carboxaldehydes defined according to the generic structure: ##STR1## wherein the lines ##STR2## represent covalent carbon-carbon bonds when m does not=0; and wherein the lines ##STR3## do not represent any bonds when m=0; wherein R represents hydrogen or methyl; wherein p and q each represents 0 or 1 with the proviso that p=1 when q=0 and p=0 when q=1; wherein X and Z each represent one or more carbon atoms required to complete a bicyclo ring with the lines ##STR4## representing carbon-carbon bonds; wherein X and Z complete a phenyl moiety when the line ##STR5## represents no bond; wherein X and Z complete a cycloalkyl ring moiety with the lines ##STR6## represent carbon-carbon bonds and with the line ##STR7## representing no bond; and wherein when m is 0, X represents an alkylene moiety, processes for preparing same by means of reacting carbon monoxide and hydrogen with an unsaturated tertiary alcohol defined according to the structure: ##STR8## by means of an oxo reaction, and uses thereof in augmenting or enhancing the aroma of perfume compositions, colognes and perfumed articles (e.g., cosmetic powders, perfumed polymers, solid or liquid anionic, cationic, nonionic or zwitterionic detergents, fabric softener compositions, fabric softener articles, hair preparations, face creams, and the like).

    Abstract translation: 描述的是根据通用结构定义的叔羟基醛：其中当m不为0时，线和 - - - - 和/或+ + + + +代表共价碳 - 碳键; 并且当m = 0时，线+ + + + +和 - - - - - 不表示任何键; 其中R表示氢或甲基; 其中p和q各自表示0或1，条件是当q = 0时p = 1，q = 1时p = 0; 其中X和Z各自表示一个或多个用代表碳 - 碳键的+ + + + +和 - 当线 - - - - 表示无键时，X和Z完全为苯基部分; 其中X和Z与所述线完成环烷基环部分，并且+ + + + +代表碳 - 碳键，并且具有不代表键的线 - - - - - 。 并且其中当m为0时，X表示亚烷基部分，通过使一氧化碳和氢与根据以下结构定义的不饱和叔醇反应制备其方法：通过氧代反应，其用途在 增加或增强香水组合物，古龙水和香水制品（例如，化妆品粉末，加香聚合物，固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，织物柔软剂组合物，织物柔软剂制品，头发制剂，面霜和 喜欢）。

    Ether carbinols and process for preparing same
    7.
    发明授权
    Ether carbinols and process for preparing same 失效
    醚甲醇及其制备方法

    公开(公告)号：US4521634A

    公开(公告)日：1985-06-04

    申请号：US574150

    申请日：1984-01-26

    Applicant: Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    Inventor： Futoshi Fujioka ,  Richard M. Boden ,  William L. Schreiber

    IPC: A24B15/34 ,  C07C43/178 ,  C07C43/196 ,  C07C43/23 ,  C07C45/49 ,  C07C47/198 ,  C07C47/277 ,  C11B9/00 ,  C07C43/188 ,  C07C41/06

    CPC classification number: C11B9/0046 ,  A24B15/345 ,  C07C43/178 ,  C07C43/196 ,  C07C43/23 ,  C07C45/49 ,  C07C47/198 ,  C07C47/277 ,  C07C2102/42

    Abstract: Described are ether carbinols defined according to the generic structure: ##STR1## wherein X.sub.1 represents a moiety selected from the group consisting of: ##STR2## and wherein Y.sub.1 represents C.sub.4 or C.sub.5 alkylene or C.sub.4 or C.sub.5 alkenylene or C.sub.4 or C.sub.5 alkynylene; processes for preparing such ether carbinols by means of first reacting allyl ethers with a mixture of carbon monoxide and hydrogen by means of an oxoreaction to produce ether carboxaldehydes and then reducing the thus formed ether carboxaldehydes to ether carbinols; or reacting camphene with appropriate diols; as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; and smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carbinols.Also described are two ether carboxaldehydes having one of the structures: ##STR3## processes for preparing such ether carboxaldehydes by means of reacting out an appropriate allyl ether with a mixture of carbon monoxide and hydrogen by means of an oxo-reaction as well as methods for augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes and perfumed articles; foodstuffs, chewing gums, chewing tobaccos, medicinal products and toothpastes; smoking tobaccos and smoking tobacco articles by adding thereto an aroma or taste augmenting or enhancing quantity of the thus produced ether carboxaldehydes.

    Abstract translation: 描述根据通用结构定义的醚甲醇：其中X 1表示选自下列的部分：其中Y 1表示C 4或C 5亚烷基或C 4或C 5亚链烯基或C 4或C 4 C5亚炔基; 通过首先使烯丙基醚与一氧化碳和氢气的混合物通过氧化反应制备这种醚甲醇的方法，以产生醚甲醛，然后将由此形成的醚甲醛还原成醚甲醇; 或使camp烯与适当的二醇反应; 以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 并通过向其中加入香烟或味道来增加或增加如此生产的醚甲醇，从而吸烟烟草和烟草制品。 还描述了具有以下结构之一的两种醚甲醛：通过使一种合适的烯丙基醚与一氧化碳和氢气的混合物通过氧代反应制备这种醚甲醛的方法 以及用于增强或增强消耗材料（包括香水，古龙水和香水制品）的香味或味道的方法; 食品，口香糖，咀嚼烟草，药用产品和牙膏; 通过向其中加入香味或味道增加或增加如此制备的醚甲醛的量来吸烟烟草和烟草制品。

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