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1.发明授权Binder compositions for making nonwoven fabrics having good hydrophobic rewet properties 失效用于制造具有良好疏水再润湿性能的非织造织物的粘合剂组合物
公开(公告)号：US4447570A
公开(公告)日：1984-05-08
申请号：US353445
申请日：1982-03-01
CPC分类号： A61L15/48 , D04H1/587 , D04H1/64 , Y10T442/671
摘要： A binder composition for nonwoven fabrics which comprises(a) a fugitive base salt of a phosphate ester surfactant or a carboxylate surfactant,(b) a latex comprising a vinyl acetate-ethylene-olefinically unsaturated carboxylic acid interpolymer colloidally suspended in water, the interpolymer containing about 0.5 to 7.0 weight percent olefinically unsaturated carboxylic acid and sufficient ethylene to provide the interpolymer with a glass transition temperature of from about -30.degree. to +20.degree. C., and(c) a polyvalent metal complex compound comprising a polyvalent metal ion and counter ions or ligands which hinder interaction of the polyvalent metal ion with the carboxylate and phosphate groups of the surfactant and interpolymer at room temperature, but at elevated temperature permit such interaction because the counter ions or ligands are expelled or are replaced by the anionic group of the surfactant and interpolymer.Nonwoven fabrics, particularly diaper innerliners, bonded with such binder compositions possess good dry and wet tensile strengths and good low rewet properties.
摘要翻译： 一种无纺布用粘合剂组合物，其包含（a）磷酸酯表面活性剂或羧酸盐表面活性剂的短暂碱盐，（b）包含胶体悬浮在水中的乙酸乙烯酯 - 乙烯 - 烯属不饱和羧酸互聚物的胶乳，含有 约0.5至7.0重量％的烯属不饱和羧酸和足够的乙烯以提供互聚物，其玻璃化转变温度为约-30℃至+ 20℃，和（c）包含多价金属离子的多价金属络合物和 阻止多价金属离子与表面活性剂和互聚物的羧酸盐和磷酸基团在室温下的相互作用的抗衡离子或配体，但在升高的温度下允许这种相互作用，因为反离子或配体被排出或被阴离子基团 表面活性剂和互聚物。 与这种粘合剂组合物粘合的非织造织物，特别是尿布内衬具有良好的干和湿拉伸强度和良好的低再湿润性能。
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公开(公告)号：US06390305B1
公开(公告)日：2002-05-21
申请号：US09574936
申请日：2000-05-19
IPC分类号： B01D7138
CPC分类号： D21H27/08 , D21H17/36 , D21H17/38 , Y10T428/2878
摘要： High performance filters comprise a basestock impregnated with an aqueous based poly(vinyl alcohol) graft emulsion copolymer as binder. The aqueous based poly(vinyl alcohol) graft emulsion copolymer binder is prepared by graft polymerizing one or more ethylenically unsaturated monomer in an aqueous poly(vinyl alcohol) solution in which at least 30% of the total poly(vinyl alcohol) is 70 to 97 mol % hydrolyzed.
摘要翻译： 高性能过滤器包括用基于水的聚（乙烯醇）接枝乳液共聚物作为粘合剂浸渍的基础油料。 水性聚（乙烯醇）接枝乳液共聚物粘合剂通过将一种或多种烯属不饱和单体在聚（乙烯醇）溶液中接枝聚合制备，其中总聚乙烯醇的至少30％为70至97 mol％水解。
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公开(公告)号：US4343133A
公开(公告)日：1982-08-10
申请号：US163240
申请日：1980-06-26
摘要： Nonwoven fibrous sheets impregnated with latices of polyvinyl acetate or its copolymers containing polyvinyl alcohol, intended for use in pre-moistened condition as skin cleansing tissues, are folded and packaged in closed containers or in individual sealed water impervious envelopes; said packaged sheets being maintained in contact with a dilute aqueous solution of a precipitating or gelling agent for polyvinyl alcohol, such as boric acid. The agent imparts improved wet tensile strength to the sheet during storage and use by the consumer but permits the sheet to be safely disposed of, after use, by flushing in plain water without danger of clogging the plumbing system.
摘要翻译： 浸渍在聚乙酸乙烯酯胶乳或其含有聚乙烯醇的共聚物的非织造纤维片材，预先用于预润湿状态作为皮肤清洁组织，被折叠并包装在密闭的容器中或者在密封的不透水的信封中; 所述包装的片材与用于聚乙烯醇如硼酸的沉淀或胶凝剂的稀水溶液保持接触。 在消费者的储存和使用期间，该试剂赋予片材更好的湿拉伸强度，但允许片材在使用后通过在普通水中冲洗而安全地处理，而不会堵塞管道系统的危险。
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4.发明授权Paper wet-strength improvement with cellulose reactive size and amine functional poly(vinyl alcohol) 失效纤维素反应性大小和胺官能聚（乙烯醇）纸张湿强度改善
公开(公告)号：US5397436A
公开(公告)日：1995-03-14
申请号：US207460
申请日：1994-03-07
摘要： The wet strength of cellulosic paper is improved by adding the combination of an amine-functional poly(vinyl alcohol) and a cellulose reactive size which is a 4 or 5 membered cyclic ester or anhydride having alkyl or alkenyl substituents of 4 or more carbon atoms. The amine-functional polymer is preferably a hydrolyzed copolymer of vinyl acetate and N-vinylformamide in which about 1-25 mole % of the monomer units are incorporated N-vinylformamide, and the cellulose reactive size is preferably an alkyl ketene dimer or an alkenyl succinic anhydride. A paper product is provided having improved wet-strength and containing normally 0.05 to 4.0 wt % based on the dry pulp of the additive amine-functional polymer and cellulose reactive size. The particular compounds which represent the polymer and the size cooperate to provide improvements in wet-tensile strength for paper which could not have been foreseen from the effects of either material acting alone.
摘要翻译： 纤维素纸的湿强度通过加入胺官能聚（乙烯醇）和纤维素反应性大小的组合来改善，该组合是具有4个或更多个碳原子的烷基或链烯基取代基的4或5元环状酯或酸酐。 胺官能聚合物优选为乙酸乙烯酯和N-乙烯基甲酰胺的水解共聚物，其中约1-25摩尔％的单体单元加入N-乙烯基甲酰胺，纤维素反应性大小优选为烷基烯酮二聚体或链烯基琥珀酸 酐。 提供了具有改进的湿强度并且基于添加剂胺官能聚合物的干纸浆和纤维素反应尺寸通常含有0.05至4.0重量％的纸产品。 表示聚合物和尺寸的特定化合物相互配合以提供纸张的湿拉伸强度的改进，这不仅是单独使用任一种材料的作用所预见的。
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公开(公告)号：US4245744A
公开(公告)日：1981-01-20
申请号：US870551
申请日：1978-01-18
CPC分类号： D04H1/64 , D04H1/587 , Y10T442/2877
摘要： Nonwoven fibrous sheets impregnated with latices of polyvinyl acetate or its copolymers containing polyvinyl alcohol, intended for use in pre-moistened condition as skin cleansing tissues, are folded and packaged in closed containers or in individual sealed water impervious envelopes; said packaged sheets being maintained in contact with a dilute aqueous solution of a precipitating or gelling agent for polyvinyl alcohol, such as boric acid. The agent imparts improved wet tensile strength to the sheet during storage and use by the consumer but permits the sheet to be safely disposed of, after use, by flushing in plain water without danger of clogging the plumbing system.
摘要翻译： 浸渍在聚乙酸乙烯酯胶乳或其含有聚乙烯醇的共聚物的非织造纤维片材，预先用于预润湿状态作为皮肤清洁组织，被折叠并包装在密闭的容器中或者在密封的不透水的信封中; 所述包装的片材与用于聚乙烯醇如硼酸的沉淀或胶凝剂的稀水溶液保持接触。 在消费者的储存和使用期间，该试剂赋予片材更好的湿拉伸强度，但允许片材在使用后通过在普通水中冲洗而安全地处理，而不会堵塞管道系统的危险。
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6.发明授权
公开(公告)号：US5244695A
公开(公告)日：1993-09-14
申请号：US852600
申请日：1992-03-17
IPC分类号： D04H1/64 , D06M15/227 , D06M15/248 , D06M15/29 , D06M15/333
CPC分类号： D06M15/248 , D04H1/587 , D04H1/64 , D06M15/227 , D06M15/29 , D06M15/333 , Y10T442/2861
摘要： A method for making a nonwoven filter which comprises impregnating a nonwoven filter substrate with a curable binder composition, the binder composition consisting essentially of(a) 10 to 100 wt% fully hydrolyzed PVOH which has a DPn of 100 to 2300; and(b) 0 to 90 wt% aqueous polymer emulsion, on a solids basis.The preferred aqueous polymer emulsion is an ethylene-vinyl chloride (EVCl) copolymer emulsion or a vinyl acetate/-N-methylolacrylamide (VAc/NMA) copolymer emulsion, or both.
摘要翻译： 一种制造无纺过滤器的方法，其包括用可固化粘合剂组合物浸渍非织造过滤器基材，所述粘合剂组合物基本上由（a）10至100重量％的完全水解的PVOH组成，其具有100至2300的DPn; 和（b）0至90重量％的聚合物水乳液，基于固体。 优选的水性聚合物乳液是乙烯 - 氯乙烯（EVCl）共聚物乳液或乙酸乙烯酯/ N-羟甲基丙烯酰胺（VAc / NMA）共聚物乳液，或两者。
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公开(公告)号：US4343134A
公开(公告)日：1982-08-10
申请号：US163243
申请日：1980-06-26
摘要： Nonwoven fibrous sheets bonded with polyvinyl alcohol, intended for use in pre-moistened condition as skin cleansing tissues, are folded and packaged in closed containers or in individual sealed water impervious envelopes; said packaged sheets being maintained in contact with a dilute aqueous solution of boric acid. The boric acid imparts improved wet tensile strength to the sheet during storage and use by the consumer but may be safely disposed of, after use, by flushing in plain water without danger of clogging the plumbing system. Instead of boric acid solution, one may employ for the indicated purpose a non-alkaline aqueous solution of a salt which acts as a precipitating or gelling agent for polyvinyl alcohol, said salt being one having an acid to neutral pH on hydrolysis.
摘要翻译： 用于预浸湿条件下用作皮肤清洁组织的聚乙烯醇粘合的非织造纤维片材被折叠并包装在密闭的容器中或者在密封的不透水的信封中; 所述包装的片材保持与稀硼酸水溶液接触。 硼酸在消费者的储存和使用期间赋予片材更好的湿拉伸强度，但是在使用后可以通过在普通水中冲洗而安全地处理，而不会堵塞管道系统的危险。 代替硼酸溶液，可以为指定目的使用非碱性盐水溶液，其作为聚乙烯醇的沉淀剂或胶凝剂，所述盐是在水解时具有酸至中性pH的盐。
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8.发明授权
公开(公告)号：US5281307A
公开(公告)日：1994-01-25
申请号：US3760
申请日：1993-01-13
IPC分类号： D21H17/34 , D21H17/06 , D21H17/15 , D21H17/36 , D21H17/47 , D21H17/49 , D21H17/52 , D21H21/18 , D21H23/76 , D21H17/33
摘要： An improved papermaking process has been developed to enhance the properties of the resultant paper or paper-type products. The process involves adding a polyvinyl alcohol/vinylamine copolymer along with a crosslinking agent at the dry end step of a conventional papermaking process. Improvements in the properties of the resultant paper products are observed, especially at low levels of copolymer addition.
摘要翻译： 一种改进的造纸工艺已被开发，以提高所得的纸或纸产品类型的性能。 该方法涉及与常规造纸过程的干燥结束步骤交联剂沿添加聚乙烯醇/乙烯胺共聚物。 在所得纸产品的性能改进中观察到，尤其是在共聚物加入低水平。
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9.发明授权Ethylene-vinyl chloride copolymer emulsions containing tetramethylol glycoluril for use as binder compositions 失效含有四羟甲基甘脲的乙烯 - 氯乙烯共聚物乳液用作粘合剂组合物
公开(公告)号：US4999239A
公开(公告)日：1991-03-12
申请号：US531974
申请日：1990-05-31
IPC分类号： C08F14/06 , C08K5/3445 , B01D39/18 , B32B27/26 , B32B27/30
CPC分类号： C08F14/06 , C08K5/3445 , Y10T428/31906 , Y10T442/2262 , Y10T442/2721
摘要： Aqueous emulsions containing an ethylene-vinyl chloride (EVCl) copolymer and tetramethylol glycoluril are described for use as binder compositions suitable for application onto nonbonded filter paper. The emulsions are prepared by incorporating 4 to 10 wt % tetramethylol glycoluril, based on the total weight of the emulsion copolymer, into an aqueous dispersion of a copolymer consisting essentially of 65 to 90 wt % vinyl chloride, 5 to 35 wt % ethylene and optionally, up to 10 wt % of a hydroxyalkyl- or carboxylic acid-containing functional comonomer. The polymerization is conducted in the presence of a stabilizing system consisting essentially of 3 to 15 wt % polyvinyl alcohol. Filter paper impregnated with these emulsions maintain tensile strength and flexibility upon being subjected to hot oil.
摘要翻译： 描述含有乙烯 - 氯乙烯（EVCl）共聚物和四羟甲基甘脲的含水乳液用作适用于非粘结滤纸上的粘合剂组合物。 乳液通过将基于乳液共聚物的总重量的4至10重量％的四羟甲基甘脲包含在基本上由65至90重量％的氯乙烯，5至35重量％的乙烯和任选地 ，至多10重量％的含羟烷基或羧酸的官能共聚单体。 在基本上由3至15重量％的聚乙烯醇组成的稳定体系的存在下进行聚合。 用这些乳液浸渍的滤纸在经受热油后保持拉伸强度和柔软性。
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10.发明授权Ethylene-vinyl chloride copolymer emulsions containing tetramethylol glycoluril for use as binder compositions 失效含有四羟甲基甘脲的乙烯 - 氯乙烯共聚物乳液用作粘合剂组合物
公开(公告)号：US4962141A
公开(公告)日：1990-10-09
申请号：US326144
申请日：1989-03-20
IPC分类号： C08F14/06 , C08K5/3445
CPC分类号： C08F14/06 , C08K5/3445
摘要： Aqueous emulsions containing an ethylene-vinyl chloride (EVCl) copolymer and tetramethylol glycoluril are described for use as binder compositions suitable for application onto nonbonded filter paper. The emulsions are prepared by incorporating 4 to 10 wt % tetramethylol glycoluril, based on the total weight of the emulsion copolymer, into an aqueous disperson of a copolymer consisting essentially of 65 to 90 wt % vinyl chloride 5 to 35 wt % ethylene and optionally, up to 10 wt % of a hydroxyalkyl- or carboxylic acid-containing functional comonomer. The polymerization is conducted in the presence of a stabilizing system consisting essentially of 3 to 15 wt % polyvinyl alcohol. Filter paper impregnated with these emulsions maintain tensile strength and flexibility upon being subjected to hot oil.
摘要翻译： 描述含有乙烯 - 氯乙烯（EVCl）共聚物和四羟甲基甘脲的含水乳液用作适用于非粘结滤纸上的粘合剂组合物。 乳液通过将基于乳液共聚物的总重量的4至10重量％的四羟甲基甘脲包含在基本上由65至90重量％的氯乙烯5-35重量％的乙烯组成的共聚物的水性分散体中， 至多10重量％的含羟基烷基或羧酸的官能共聚单体。 在基本上由3至15重量％的聚乙烯醇组成的稳定体系的存在下进行聚合。 用这些乳液浸渍的滤纸在经受热油后保持拉伸强度和柔软性。
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