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    Method for preparing high cure temperature rare earth iron compound magnetic material
    2.
    发明授权
    Method for preparing high cure temperature rare earth iron compound magnetic material 失效
    高固化温度稀土铁复合磁性材料的制备方法

    公开(公告)号：US06383406B1

    公开(公告)日：2002-05-07

    申请号：US09578563

    申请日：2000-05-25

    Applicant: Yuhong Huang ,  Qiang Wei ,  Haixing Zheng

    Inventor： Yuhong Huang ,  Qiang Wei ,  Haixing Zheng

    IPC: H01F100

    CPC classification number: H01F1/059 ,  H01F1/058

    Abstract: Insertion of light elements such as H,C, or N in the R2Fe17 (R=rare earth metal) series has been found to modify the magnetic properties of these compounds, which thus become prospective candidates for high performance permanent magnets. The most spectacular changes are increases of the Curie temperature, Tc, of the magnetization, Ms, and of coercivity, Hc, upon interstitial insertion. A preliminary product having a component R—Fe—C,N phase is produced by a chemical route. Rare earth metal and iron amides are synthesized followed by pyrolysis and sintering in an inert or reduced atmosphere, as a result of which, the R—Fe—C,N phases are formed. Fabrication of sintered rare earth iron nitride and carbonitride bulk magnet is impossible via conventional process due to the limitation of nitridation method.

    Abstract translation: 已经发现在R2Fe17（R =稀土金属）系列中插入诸如H，C或N之类的轻元素可以改变这些化合物的磁性，从而成为高性能永磁体的潜在候选者。 最壮观的变化是间隙插入时磁化强度Ms的居里温度Tc和矫顽力Hc的升高。 通过化学途径制备具有组分R-Fe-C，N相的初级产物。 合成稀土金属和铁酰胺，然后在惰性或还原气氛中进行热解和烧结，结果形成了R-Fe-C，N相。 由于氮化方法的限制，通过常规方法制备烧结稀土氮化铁和碳氮化物块状磁体是不可能的。

    Methods for and products of processing nanostructure nitride, carbonitride and oxycarbonitride electrode power materials by utilizing sol gel technology for supercapacitor applications
    3.
    发明授权
    Methods for and products of processing nanostructure nitride, carbonitride and oxycarbonitride electrode power materials by utilizing sol gel technology for supercapacitor applications 失效
    通过使用溶胶凝胶技术处理超级电容器应用纳米结构氮化物，碳氮化物和碳氮氧化物电极材料的方法和产品

    公开(公告)号：US06168694A

    公开(公告)日：2001-01-02

    申请号：US09244815

    申请日：1999-02-04

    Applicant: Yuhong Huang ,  Oiang Wei ,  Chung-tse Chu ,  Haixing Zheng

    Inventor： Yuhong Huang ,  Oiang Wei ,  Chung-tse Chu ,  Haixing Zheng

    IPC: C25B1100

    CPC classification number: H01G9/155 ,  Y02E60/13

    Abstract: Metal nitride, carbonitride, and oxycarbonitride powder with high surface area (up to 150 m2/g) is prepared by using sol-gel process. The metal organic precursor, alkoxides or amides, is synthesized firstly. The metal organic precursor is modified by using unhydrolyzable organic ligands or templates. A wet gel is formed then by hydrolysis and condensation process. The solvent in the wet gel is then be removed supercritically to form porous amorphous hydroxide. This porous hydroxide materials is sintered to 725° C. under the ammonia flow and porous nitride powder is formed. The other way to obtain high surface area nitride, carbonitride, and oxycarbonitride powder is to pyrolyze polymerized templated metal amides aerogel in an inert atmosphere. The electrochemical capacitors are prepared by using sol-gel prepared nitride, carbonitride, and oxycarbonitride powder. Two methods are used to assemble the capacitors. Electrode is formed either by pressing the mixture of nitride powder and binder to a foil, or by depositing electrode coating onto metal current collector. The binder or coating is converted into a continuous network of electrode material after thermal treatment to provide enhanced energy and power density. Liquid electrolyte is soaked into porous electrode. The electrochemical capacitor assembly further has a porous separator layer between two electrodes/electrolyte and forming a unit cell.

    Abstract translation: 通过使用溶胶 - 凝胶法制备具有高表面积（高达150m 2 / g）的金属氮化物，碳氮化物和碳氮氧化物粉末。 首先合成金属有机前体，醇盐或酰胺。 通过使用不可水解的有机配体或模板来修饰金属有机前体。 然后通过水解和缩合过程形成湿凝胶。 然后将湿凝胶中的溶剂超临界除去以形成多孔无定形氢氧化物。 将该多孔氢氧化物材料在氨流下烧结至725℃，形成多孔氮化物粉末。 获得高表面积氮化物，碳氮化物和碳氮氧化物粉末的另一种方法是在惰性气氛中热解聚合的模板化金属酰胺气凝胶。 通过使用溶胶 - 凝胶制备的氮化物，碳氮化物和碳氮氧化物粉末制备电化学电容器。 使用两种方法来组装电容器。 电极通过将氮化物粉末和粘合剂的混合物压制成箔，或者通过在金属集电体上沉积电极涂层而形成。 在热处理后，粘合剂或涂层被转化成电极材料的连续网络，以提供增强的能量和功率密度。 将液体电解质浸入多孔电极中。 电化学电容器组件还在两个电极/电解质之间具有多孔隔离层，并形成单电池。

    Method and composition useful treating metal surfaces
    5.
    发明授权
    Method and composition useful treating metal surfaces 失效
    用于处理金属表面的方法和组合物

    公开(公告)号：US5807430A

    公开(公告)日：1998-09-15

    申请号：US521915

    申请日：1995-11-06

    Applicant: Haixing Zheng ,  Su-Jen Ting ,  Cheng-Jye Chu

    Inventor： Haixing Zheng ,  Su-Jen Ting ,  Cheng-Jye Chu

    IPC: C09D183/14 ,  C09D183/06 ,  C09D183/07 ,  C09D183/08

    CPC classification number: C09D183/14

    Abstract: A composition suitable for treating metal surfaces prior to bonding of the surfaces to materials including metals, rubber, glass, polymers, sealants, coatings, and in particular polymeric adhesives, to enhance the strength of the bond and to prolong useful life in corrosive environments, is described. The composition comprises: (a) water; (b) metal alkoxide comprising M(OR).sub.x, where M is a metal and R is an alkyl group; and (c) organoalkoxysilane comprising silane coupling functional groups capable of bonding with the material to be bonded to the metal surface; and (d) acid to promote hydrolysis and crosslinking of the metal alkoxide and organoalkoxysilane, wherein the molar ratio of metal alkoxide:organoalkoxysilane:acid is selected such that the composition is characterized by: (i) an extended shelf life, and (ii) is capable of crosslinking when applied to the metal surface to form a adherent coating having a substantially uniform distribution of metal, silicon, and oxygen species through the thickness of the coating, (iii) is capable of bonding with the material to be bonded to the metal surface to form a strong adherent bond between the metal surface and the material to be bonded to the metal surface. Also described is a method of using the composition to bond metal surfaces to one another.

    Abstract translation: 在将表面粘合到包括金属，橡胶，玻璃，聚合物，密封剂，涂层，特别是聚合物粘合剂的材料之前，适于处理金属表面的组合物，以增强粘结强度并延长腐蚀环境的使用寿命， 被描述。 组合物包括：（a）水; （b）包含M（OR）x的金属醇盐，其中M是金属，R是烷基; 和（c）有机烷氧基硅烷，其包含能够与待结合的材料与金属表面结合的硅烷偶联官能团; 和（d）酸以促进金属醇盐和有机烷氧基硅烷的水解和交联，其中选择金属醇盐：有机烷氧基硅烷：酸的摩尔比，使得组合物的特征在于：（i）延长的保质期，和（ii） 当施加到金属表面上时能够交联以形成通过涂层的厚度具有金属，硅和氧物质的基本上均匀分布的粘附涂层，（iii）能够与待粘合的材料结合 金属表面以在金属表面和待结合到金属表面的材料之间形成牢固的粘结。 还描述了使用组合物将金属表面彼此粘合的方法。

    Radiation-curable anti-reflective coating system
    7.
    发明授权
    Radiation-curable anti-reflective coating system 失效
    可辐射固化的抗反射涂层系统

    公开(公告)号：US06942924B2

    公开(公告)日：2005-09-13

    申请号：US10001639

    申请日：2001-10-31

    Applicant: Liu He ,  Sung-Soon Park ,  Haixing Zheng ,  Grace Tang ,  Aylin Vance

    Inventor： Liu He ,  Sung-Soon Park ,  Haixing Zheng ,  Grace Tang ,  Aylin Vance

    IPC: C08F2/46 ,  G02B1/11 ,  B32B9/00

    CPC classification number: G02B1/111 ,  Y10T428/31507 ,  Y10T428/31612 ,  Y10T428/31645

    Abstract: A radiation-curable anti-reflective coating is disclosed. The coating may be deposited on a substrate by spinning, dipping or rolling. The anti-reflective coating may have two layers in which case the anti-reflective coating has a V-shaped reflectance pattern in the visible wavelength spectrum. The anti-reflective coating may have three layers in which case the anti-reflective coating has a broadband reflectance pattern in the visible wavelength spectrum.

    Abstract translation: 公开了一种可辐射固化的抗反射涂层。 可以通过旋转，浸渍或滚压将涂层沉积在基底上。 抗反射涂层可以具有两层，在这种情况下，抗反射涂层在可见波长光谱中具有V形反射率图案。 抗反射涂层可以具有三层，在这种情况下，抗反射涂层在可见波长光谱中具有宽带反射图案。

    Composition useful for treating metal surfaces
    9.
    发明授权
    Composition useful for treating metal surfaces 失效
    用于处理金属表面的组合物

    公开(公告)号：US06391465B1

    公开(公告)日：2002-05-21

    申请号：US09087227

    申请日：1998-05-29

    Applicant: Haixing Zheng ,  Su-Jen Ting ,  Cheng-Jye Chu

    Inventor： Haixing Zheng ,  Su-Jen Ting ,  Cheng-Jye Chu

    IPC: B32B1508

    CPC classification number: C09D183/14

    Abstract: A composition suitable for treating metal surfaces prior to bonding of the surfaces to materials including metals, rubber, glass, polymers, sealants, coatings, and in particular polymeric adhesives, to enhance the strength of the bond and to prolong useful life in corrosive environments, is described. The composition comprises: (a) water; (b) metal alkoxide comprising M(OR)x, where M is a metal and R is an alkyl group; and (c) organoalkoxysilane comprising silane coupling functional groups capable of bonding with the material to be bonded to the metal surface; and (d) acid to promote hydrolysis and cross-linking of the metal alkoxide and organoalkoxysilane, wherein the molar ratio of metal alkoxide:organoalkoxysilane:acid is selected such that the composition is characterized by: (i) an extended shelf life, and (ii) is capable of cross-linking when applied to the metal surface to form an adherent coating having a substantially uniform distribution of metal, silicon, and oxygen species through the thickness of the coating, (iii) is capable of bonding with the material to be bonded to the metal surface to form a strong adherent bond between the metal surface and the material to be bonded to the metal surface. Also described is a method of using the composition to bond metal surfaces to one another.

    Abstract translation: 在将表面粘合到包括金属，橡胶，玻璃，聚合物，密封剂，涂层，特别是聚合物粘合剂的材料之前，适于处理金属表面的组合物，以增强粘结强度并延长腐蚀环境的使用寿命， 被描述。 组合物包括：（a）水; （b）包含M（OR）x的金属醇盐，其中M是金属，R是烷基; 和（c）有机烷氧基硅烷，其包含能够与待结合的材料与金属表面结合的硅烷偶联官能团; 和（d）酸以促进金属醇盐和有机烷氧基硅烷的水解和交联，其中选择金属醇盐：有机烷氧基硅烷：酸的摩尔比，使得组合物的特征在于：（i）延长的保质期和（ ii）当应用于金属表面时能够交联以形成通过涂层厚度具有金属，硅和氧物质的基本均匀分布的粘附涂层，（iii）能够与材料粘合 结合到金属表面以在金属表面和待结合到金属表面的材料之间形成牢固的粘结。 还描述了使用组合物将金属表面彼此粘合的方法。

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