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    Process for the preparation of LiFePO4-carbon composites
    1.
    发明授权
    Process for the preparation of LiFePO4-carbon composites 有权
    制备LiFePO4-碳复合材料的方法

    公开(公告)号：US09209461B2

    公开(公告)日：2015-12-08

    申请号：US13379048

    申请日：2010-06-23

    Applicant: Simon Schroedle ,  Hartmut Hibst ,  Brian Roberts ,  Kirill Bramnik ,  Jordan Keith Lampert

    Inventor： Simon Schroedle ,  Hartmut Hibst ,  Brian Roberts ,  Kirill Bramnik ,  Jordan Keith Lampert

    IPC: H01B1/24 ,  H01M4/525 ,  H01M4/58 ,  C01B25/45 ,  C01B25/455 ,  H01M4/131 ,  H01M4/1315 ,  H01M4/133 ,  H01M4/485 ,  H01M4/505 ,  H01M4/583 ,  H01M10/0525

    CPC classification number: H01M4/5825 ,  C01B25/45 ,  C01B25/455 ,  H01B1/24 ,  H01M4/131 ,  H01M4/1315 ,  H01M4/133 ,  H01M4/485 ,  H01M4/505 ,  H01M4/525 ,  H01M4/583 ,  H01M10/0525 ,  Y02E60/122

    Abstract: The present invention relates to a process for the preparation of particles comprising at least one compound according to general formula (I) M1aM2bM3cOoNnFf (I) wherein M1, M2, M3 O, N, F, a, b, c, o, n and f have the following meanings: M1 at least one alkaline metal, M2 at least one transition metal in oxidation state +2, M3 at least one non-metal chosen form S, Se, P, As, Si, Ge and/or B, O oxygen, N nitrogen, F fluorine, a 0.8-4.2, b 0.8-1.9, c 0.8-2.2, o 1.0-8.4, n 0-2.0 and f 0-2.0, wherein a, b, c, o, n and f are chosen to ensure electroneutrality of the compound according to general formula (I), and carbon, comprising at least the following steps: (A) providing an essentially aqueous mixture comprising at least one compound comprising M1, at least one compound comprising M2 having at least partially an oxidation state higher than +2, optionally at least one compound comprising M3, at least one compound comprising N, if present, and/or at least one compound comprising F, if present, at least one polysaccharide comprising glucose having a molecular weight M of at least 50000 g/mol as carbon precursor and at least one reducing agent, (B) drying the mixture provided in step (A), in order to obtain a solid particle and (C) calcining the solid particle obtained from step (B) at a temperature of 300 to 950° C.

    Abstract translation: 本发明涉及一种制备颗粒的方法，所述颗粒包含至少一种根据通式（I）的M1aM2bM3cOoNnFf（I）的化合物，其中M1，M2，M3O，N，F，a，b，c，o，n和 f具有以下含义：M1至少一种碱金属，M2至少一种氧化态过渡金属+2，M3至少一种非金属选择形式S，Se，P，As，Si，Ge和/或B， O氧，N氮，F氟，0.8-4.2，b 0.8-1.9，c 0.8-2.2，o 1.0-8.4，n 0-2.0和f 0-2.0，其中a，b，c，o，n和 选择f以确保根据通式（I）的化合物和包含至少以下步骤的碳的电中性：（A）提供基本上含水的混合物，其包含至少一种包含M1，至少一种包含M2的化合物，其包含具有 至少部分地高于+2的氧化态，任选地至少一种包含M3的化合物，至少一种包含N的化合物（如果存在）和/或至少一种包含F的化合物 送出至少一种包含分子量M至少为50000g / mol的葡萄糖作为碳前体和至少一种还原剂的至少一种多糖，（B）干燥步骤（A）中提供的混合物，以获得固体颗粒 和（C）在300-950℃的温度下煅烧由步骤（B）得到的固体颗粒。

    Process for the preparation of crystalline lithium-, vanadium-and phosphate-comprising materials
    2.
    发明授权
    Process for the preparation of crystalline lithium-, vanadium-and phosphate-comprising materials 失效
    用于制备结晶的含锂，钒和磷酸盐的材料的方法

    公开(公告)号：US08506847B2

    公开(公告)日：2013-08-13

    申请号：US12680797

    申请日：2008-09-18

    Applicant: Hartmut Hibst ,  Brian Roberts ,  Jordan Keith Lampert ,  Kirill Bramnik

    Inventor： Hartmut Hibst ,  Brian Roberts ,  Jordan Keith Lampert ,  Kirill Bramnik

    IPC: H01B1/06 ,  H05B7/085 ,  H01M4/88

    CPC classification number: C01B25/45 ,  H01M4/5825 ,  H01M10/0525

    Abstract: The present invention relates to a process for the preparation of compounds of general formula (I) Lia-bM1bV2-cM2c(PO4)x (I) with M1: Na, K, Rb and/or Cs, M2: Ti, Zr, Nb, Cr, Mn, Fe, Co, Ni, Al, Mg and/or Sc, a: 1.5-4.5, b: 0-0.6, c: 0-1.98 and x: number to equalize the charge of Li and V and M1 and/or M2, if present, wherein a−b is >0, by providing an essentially aqueous mixture comprising at least one lithium-comprising compound, at least one vanadium-comprising compound in which vanadium has the oxidation state +5 and/or +4, and at least one M1-comprising compound, if present, and/or at least one M2-comprising compound, if present, and at least one reducing agent which is oxidized to at least one compound comprising at least one phosphorous atom in oxidation state +5, drying and calcining.

    Abstract translation: 本发明涉及制备具有M1：Na，K，Rb和/或Cs，M2：Ti，Zr，Nb的通式（I）Lia-bM1bV2-cM2c（PO4）x（Ⅰ）的化合物的方法 ，Cr，Mn，Fe，Co，Ni，Al，Mg和/或Sc，a：1.5-4.5，b：0-0.6，c：0-1.98和x：等于Li和V和M1的电荷 和/或M2，如果存在，其中ab> 0，通过提供基本上含水的混合物，其包含至少一种含锂化合物，至少一种含钒化合物，其中钒具有+5和/或+4的氧化态 和至少一种含M1化合物（如果存在）和/或至少一种含M2化合物（如果存在）和至少一种还原剂被氧化成至少一种包含至少一个氧化态磷原子的化合物 +5，干燥和煅烧。

    Selective materials separation using modified magnetic particles
    3.
    发明授权
    Selective materials separation using modified magnetic particles 有权
    使用改性磁性颗粒的选择性材料分离

    公开(公告)号：US08377311B2

    公开(公告)日：2013-02-19

    申请号：US13054713

    申请日：2009-07-15

    Applicant: Imme Domke ,  Alexej Michailovski ,  Norbert Mronga ,  Hartmut Hibst ,  Juergen Tropsch ,  Susanne Stutz

    Inventor： Imme Domke ,  Alexej Michailovski ,  Norbert Mronga ,  Hartmut Hibst ,  Juergen Tropsch ,  Susanne Stutz

    IPC: B03C1/005

    CPC classification number: H01F1/44 ,  B03C1/015 ,  B82Y25/00 ,  H01F1/0045

    Abstract: The present invention relates to a process of the invention for separating at least one first material from a mixture comprising this at least one first material and at least one second material, which comprises the steps: (A) Contacting of at least one magnetic particle and at least one bifunctional molecule or an adduct of the two with the mixture comprising the at least one first material and at least one second material so that an adduct is formed from the at least one magnetic particle, the bifunctional compound of the general formula (I) and the at least one first material, (B) suspension of the adduct obtained in step (A) in a suitable suspension medium, (C) separation of the adduct present in the suspension from step (B) from the suspension by application of a magnetic field, (D) if appropriate, dissociation of the adduct separated off in step (C) in order to obtain the at least one first material. a corresponding adduct and the use of such an adduct for the separation of mixtures of materials.

    Abstract translation: 本发明涉及一种本发明的方法，用于从包含该至少一种第一材料和至少一种第二材料的混合物中分离至少一种第一材料，其包括以下步骤：（A）接触至少一种磁性颗粒和 至少一种双功能分子或两者的加合物与混合物包含至少一种第一材料和至少一种第二材料，使得加合物由至少一个磁性颗粒形成，通式（I）的双官能化合物 ）和所述至少一种第一材料，（B）步骤（A）中获得的加合物的悬浮液在合适的悬浮介质中，（C）通过施用将来自步骤（B）的悬浮液中存在的加合物与悬浮液 （D）如果合适，在步骤（C）中分离的加合物的解离以获得至少一种第一材料。 相应的加合物和这种加合物用于分离材料混合物的用途。

    ELECTRO-OPTICALLY SWITCHABLE SYSTEM
    4.
    发明申请
    ELECTRO-OPTICALLY SWITCHABLE SYSTEM 审中-公开
    电光开关系统

    公开(公告)号：US20120106139A1

    公开(公告)日：2012-05-03

    申请号：US13382583

    申请日：2010-07-06

    Applicant: Bastian Ewald ,  Dirk Gerhard ,  Hartmut Hibst

    Inventor： Bastian Ewald ,  Dirk Gerhard ,  Hartmut Hibst

    IPC: F21V33/00 ,  G02F1/163 ,  G02F1/1347 ,  G02F1/1334 ,  G02F1/01 ,  G02F1/13

    CPC classification number: B65D65/16 ,  B65D81/30 ,  B65D2201/00

    Abstract: An electro-optically switchable system that includes an optically active element and a momentary switch, a container that includes such an electro-optically switchable system and use of such an electro-optically switchable system for providing containers that allow increased light to pass through into the interior thereof only for the duration of a control intervention.

    Abstract translation: 一种电光可切换系统，其包括光学有源元件和瞬时开关，容器包括这种电光可切换系统，并且使用这种电光可切换系统来提供允许增加的光通过的容器 其内部仅在控制干预的持续时间内。

    PROCESS FOR THE PREPARATION OF CRYSTALLINE LITHIUM-, IRON- AND PHOSPHATE-COMPRISING MATERIALS
    6.
    发明申请
    PROCESS FOR THE PREPARATION OF CRYSTALLINE LITHIUM-, IRON- AND PHOSPHATE-COMPRISING MATERIALS 审中-公开
    制备结晶锂，铁和磷酸盐包覆材料的方法

    公开(公告)号：US20110049443A1

    公开(公告)日：2011-03-03

    申请号：US12988418

    申请日：2009-04-16

    Applicant: Hartmut Hibst ,  Brian Roberts ,  Jordan Keith Lampert ,  Kirill Bramnik

    Inventor： Hartmut Hibst ,  Brian Roberts ,  Jordan Keith Lampert ,  Kirill Bramnik

    IPC: H01B1/08 ,  H01B1/10

    CPC classification number: H01M4/48 ,  C01B25/30 ,  C01B25/45 ,  C01P2006/40 ,  H01B1/02 ,  H01B1/08 ,  H01M4/525 ,  H01M4/5825 ,  H01M4/625 ,  H01M10/0525

    Abstract: The present application relates to a process for the preparation of compounds of general formula (I) Lia-bM1bFe1-cM2cPd-eM3eOx (I), wherein M1, M2, M3, a, b, c, d, e and x: M1: Na, K, Rb and/or Cs, M2: Mn, Mg, Ca, Ti, Co, Ni, Cr, V, M3: Si, S, a: 0.8-1.9, b: 0-0.3, c: 0-0.9, d: 0.8-1.9, e: 0-0.5, x: 1.0-8, depending on the amount and oxidation state of L1, M1, Fe, M2, P, M3, wherein compounds of general formula (I) are neutrally charged, comprising the following steps (A) providing an essentially aqueous mixture comprising at least one lithium-comprising compound, FeOOH as iron-comprising compound and at least one M1-comprising compound, if present, and/or at least one M2-comprising compound, if present, and/or least one M3-comprising compound, if present, at least one compound comprising at least one phosphorous atom and at least one reducing agent, (B) drying the mixture provided in step (A), in order to obtain a solid compound and (C) calcining the solid compound obtained from step (A) or (B) at a temperature of 300 to 950° C.

    Abstract translation: 本申请涉及制备通式（I）Lia-bM1bFe1-cM2cPd-eM3eOx（Ⅰ）的化合物的方法，其中M1，M2，M3，a，b，c，d，e和x：M1： Na，K，Rb和/或Cs，M2：Mn，Mg，Ca，Ti，Co，Ni，Cr，V，M3：Si，S，a：0.8-1.9，b：0-0.3，c： 0.9，d：0.8-1.9，e：0-0.5，x：1.0-8，取决于L1，M1，Fe，M2，P，M3的量和氧化态，其中通式（I）的化合物是中性的 包括以下步骤（A），其提供基本上含水的混合物，其包含至少一种含锂化合物，作为含铁化合物的FeOOH和至少一种含M1化合物（如果存在）和/或至少一种含M2的化合物 化合物（如果存在）和/或至少一种含M3化合物（如果存在）至少一种包含至少一个磷原子和至少一种还原剂的化合物，（B）按顺序干燥步骤（A）中提供的混合物 得到固体化合物，（C）煅烧由步骤获得的固体化合物 （A）或（B）在300〜950℃的温度下进行。

    ELECTRICALLY CONDUCTIVE, MAGNETIC COMPOSITE MATERIAL, PROCESS FOR ITS PRODUCTION, AND ITS USE
    10.
    发明申请
    ELECTRICALLY CONDUCTIVE, MAGNETIC COMPOSITE MATERIAL, PROCESS FOR ITS PRODUCTION, AND ITS USE 审中-公开
    电导体，磁性复合材料，其生产工艺及其使用

    公开(公告)号：US20090045374A1

    公开(公告)日：2009-02-19

    申请号：US12192610

    申请日：2008-08-15

    Applicant: Dirk LAWRENZ ,  Ingolf Hennig ,  Andrey Karpov ,  Stefan Kirsch ,  Hartmut Hibst ,  Juergen Kaczun ,  Uta Holzenkamp ,  Stephen Ems ,  Harry Thomas Mills ,  Paul Edwin Gloor

    Inventor： Dirk LAWRENZ ,  Ingolf Hennig ,  Andrey Karpov ,  Stefan Kirsch ,  Hartmut Hibst ,  Juergen Kaczun ,  Uta Holzenkamp ,  Stephen Ems ,  Harry Thomas Mills ,  Paul Edwin Gloor

    IPC: H01F1/00 ,  C01G49/08

    CPC classification number: H05B6/64

    Abstract: Electrically conductive, magnetic composite material, comprising (A) pulverulent, inorganic, magnetic material which is electrically not or only poorly conductive, and (B) an electrically conductive material, selected from the group consisting of pulverulent and liquid carbon-comprising organic materials and pulverulent carbon allotropes, in a ratio by weight of (A):(B)=from 1:100 to 100:1; a process for its production, and its use, and also ferrimagnetic mixed oxide (A) of the general formula I: M″M′″O4  (I), in which M″ is a first metal component which comprises divalent metal cations; and M′″ is a second metal component which comprises trivalent metal cations; capable of production by reacting, in a quantitative ratio such that the resultant ferromagnetic mixed oxide (A) is electrically neutral, divalent metal cations M″ and trivalent metal cations M′″ in aqueous solution and/or dispersion, comprising at least one electrically conductive material (B) and/or at least one material which differs therefrom and which is a binder (C) which dries physically or else is crosslinkable thermally and/or by actinic radiation.

    Abstract translation: 导电性磁性复合材料，其包含（A）不具有导电性或导电性差的粉状，无机，磁性材料，和（B）导电材料，其选自由含有粉状和液态碳的有机材料和 粉末碳同素异形体，以（A）:( B）的重量比= 1:100至100:1; 其制备方法及其用途，以及通式I的亚铁磁性混合氧化物（A）：<？in-line-formula description =“In-line formula”end =“lead”？> M'M ''O4（I），<？in-line-formula description =“In-line Formulas”end =“tail”？>其中M“是包含二价金属阳离子的第一金属成分; M“是包含三价金属阳离子的第二金属组分; 能够通过使得所得铁磁混合氧化物（A）电中性的数量比使水溶液和/或分散体中的二价金属阳离子M“和三价金属阳离子M”反应而制备，包含至少一种 导电材料（B）和/或与其不同的至少一种材料，其是物理上干燥的或者是通过光化辐射可交联的粘合剂（C）。

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