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    Metallocene compositions
    2.
    发明授权
    Metallocene compositions 有权

    公开(公告)号：US06380120B1

    公开(公告)日：2002-04-30

    申请号：US09619750

    申请日：2000-07-19

    申请人： Terry John Burkhardt ,  William T. Haygood, Jr. ,  Udo M. Stehling ,  James R. Hart ,  Robert Tan Li ,  James Charles Vizzini ,  Matthew Cornyn Kuchta

    发明人： Terry John Burkhardt ,  William T. Haygood, Jr. ,  Udo M. Stehling ,  James R. Hart ,  Robert Tan Li ,  James Charles Vizzini ,  Matthew Cornyn Kuchta

    IPC分类号： B01J3100

    CPC分类号： C07F17/00 ,  C08F4/65908 ,  C08F4/65912 ,  C08F4/65916 ,  C08F10/00 ,  C08F110/02 ,  C08F110/06 ,  C08F210/06 ,  C08F210/16 ,  Y10S526/943 ,  C08F4/65927 ,  C08F2500/12 ,  C08F2500/03 ,  C08F2500/17 ,  C08F2500/15 ,  C08F2500/21

    摘要： This invention relates to metallocene compositions and their use in the preparation of catalyst systems for olefin polymerization, particularly propylene polymerization. The metallocene compositions may be represented by the formula: wherein M1 is selected from the group consisting of titanium, zirconium, hafnium, vanadium, niobium, tantalum, chromium, molybdenum and tungsten; R1 and R2 are identical or different, and are one of a hydrogen atom, a C1-C10 alkyl group, a C1-C10 alkoxy group, a C6-C10 aryl group, a C6-C10 aryloxy group, a C2-C40 alkenyl group, a C7-C40 arylalkyl group, a C7-C40 alkylaryl group, a C8-C40 arylalkenyl group, an OH group or a halogen atom, or a conjugated diene which is optionally substituted with one or more hydrocarbyl, tri(hydrocarbyl)silyl groups or hydrocarbyl, tri(hydrocarbyl)silylhydrocarbyl groups, said diene having up to 30 atoms not counting hydrogen; R3 are identical or different and are each a hydrogen atom, a halogen atom, a C1-C10 alkyl group which may be halogenated, a C6-C10 aryl group which may be halogenated, a C2-C10 alkenyl group, a C7-C40-arylalkyl group, a C7-C40 alkylaryl group, a C8-C40 arylalkenyl group, a —NR′2, —SR′, —OR′, —OSiR′3 or —PR′2 radical, wherein R′ is one of a halogen atom, a C1-C10 alkyl group, or a C6-C10 aryl group; R4 to R7 are identical or different and are hydrogen, as defined for R3 or two or more adjacent radicals R5 to R7 together with the atoms connecting them form one or more rings; —B(R14)—, —Al(R14)—, —Ge—, —Sn—, —O—, S—, —SO—, —SO2—, —N(R14)—, —CO—, —P(R14), or —P(O)(R14)—, or an amidoborane radical; wherein: R14, R15 and R16 are identical or different and are a hydrogen atom, a halogen atom, a C1-C20 allyl group, a C1-C20 fluoroalkyl or silaalkyl group, a C6-C30 aryl group, a C6-C30 fluoroaryl group, a C1-C20 alkoxy group, a C2-C20 alkenyl group, a C7-C40 arylalkyl group, a C8-C40 arylalkenyl group, a C7-C40 alkylaryl group, or R14 and R15, together with the atoms binding them, form a cyclic ring; or, R13 is represented by the formula: wherein R17 to R24 are as defined for R1 and R2, or two or more adjacent radicals R17 to R24, including R20 and R21, together with the atoms connecting them form one or more rings; M2 is one or more carbons, silicon, germanium or tin; R8, R10 and R12 are identical or different and have the meanings stated for R4 to R7; R9 and R11 are identical or different and are a Group 14A radical having from 1 to 20 carbon atoms or are each primary, secondary or tertiary butyl groups, aryl groups, isopropyl groups, fluoroalkyl groups, trialkyl silyl groups, or other groups of similar size.

    Metallocene compositions
    3.
    发明授权
    Metallocene compositions 有权

    公开(公告)号：US06376411B1

    公开(公告)日：2002-04-23

    申请号：US09620302

    申请日：2000-07-19

    申请人： Terry John Burkhardt ,  William T. Haygood, Jr. ,  Robert Tan Li ,  James Charles Vizzini ,  Matthew Cornyn Kuchta ,  Udo M. Stehling ,  James R. Hart

    发明人： Terry John Burkhardt ,  William T. Haygood, Jr. ,  Robert Tan Li ,  James Charles Vizzini ,  Matthew Cornyn Kuchta ,  Udo M. Stehling ,  James R. Hart

    IPC分类号： B01J3100

    CPC分类号： C07F17/00 ,  C08F4/65908 ,  C08F4/65912 ,  C08F4/65916 ,  C08F10/00 ,  C08F110/02 ,  C08F110/06 ,  C08F210/06 ,  C08F210/16 ,  Y10S526/943 ,  C08F4/65927 ,  C08F2500/12 ,  C08F2500/03 ,  C08F2500/17 ,  C08F2500/15 ,  C08F2500/21

    摘要： This invention relates to metallocene compositions and their use in the preparation of catalyst systems for olefin polymerization, particularly propylene polymerization. The metallocene compositions may be represented by the formula: wherein M1 is selected from the group consisting of titanium, zirconium, hathium, vanadiurm, niobium, tantalum, chromium, molybdenum and tungsten; R1 and R2 are identical or different, and are one of a hydrogen atom, a C1-C10 alkyl group, a C1-C10 alkoxy group, a C6-C10 aryl group, a C6-C10 aryloxy group, a C2-C40 alkenyl group, a C7-C40 arylalkyl group, a C7-C40 alkylaryl group, a C8-C40 arylalkenyl group, an OH group or a halogen atom, or a conjugated diene or tri(hydrocarbyl)silylhydrocarbyl groups, said diene having up to 30 atoms not counting hydrogen; R3 are identical or different and are each a hydrogen atom, a halogen atom, a C1-C10 alkyl group which may be halogenated, a C6-C10 aryl group which may be halogenated, a C2-C10 alkenyl group, a C7-C40-arylalkyl group, a C7-C40 alkylaryl group, a C8-C40 arylalkenyl group, a —NR′2, —SR′, —OR′, —OSiR′3 or —PR′2 radical, wherein R′ is one of a halogen atom, a C1-C10 alkyl group, or a C6-C10 aryl group; R4 to R7 are identical or different and are hydrogen, as defined for R3 or two or more adjacent radicals R5 to R7 together with the atoms connecting them form one or more rings;  —B(R14)—, —Al(R14)—, —Ge—, —Sn—, —O—, —S—, —SO—, —SO2—, —N(R14)—, —CO—, —P(R14)—, or —P(O)(R14)—, or an amidoborane radical; wherein: R14, R15and R16 are identical or different and are a hydrogen atom, a halogen atom, a C1-C20 alkyl group, a C1-C20 fluoroalkyl or silaalkyl group, a C6-C30 aryl group, a C6-C30 fluoroaryl group, a C1-C20 alkoxy group, a C2-C20 alkenyl group, a C7-C40 arylalkyl group, a C8-C40 arylalkenyl group, a C7-C40 alkylaryl group, or R14 and R15, together with the atoms binding them, form a cyclic ring; or, R13 is represented by the formula: wherein R17 to R24 are as defined for R1 and R2, or two or more adjacent radicals R17 to R24, including R20 and R21, together with the atoms connecting them form one or more rings; M2 is one or more carbons, silicon, germanium or tin; R8, R10 and R12 are identical or different and have the meanings stated for R4 to R7; R9 and R11 are identical or different and are a Group 14 radical having from 1 to 20 carbon atoms or are each primary, secondary or tertiary butyl groups, aryl groups, isopropyl groups, fluoroalkyl groups, trialkyl silyl groups, or other groups of similar size.

    Analysis method
    4.
    发明授权
    Analysis method 失效
    分析方法

    公开(公告)号：US07456021B2

    公开(公告)日：2008-11-25

    申请号：US10758900

    申请日：2004-01-16

    申请人： Patrick Brant ,  Burkhard Endeward ,  Hans Thomann ,  Yuan-Ju Chen ,  Terry John Burkhardt

    发明人： Patrick Brant ,  Burkhard Endeward ,  Hans Thomann ,  Yuan-Ju Chen ,  Terry John Burkhardt

    IPC分类号： G01N31/10

    CPC分类号： G01N21/6408 ,  C08F4/65908 ,  C08F4/65912 ,  C08F4/65916 ,  C08F10/00 ,  G01N21/274 ,  G01N2201/127 ,  Y10S502/522 ,  C08F4/65927

    摘要： Disclosed herein is a method for determining the presence of an activated catalyst site in a catalyst system comprising a catalyst precursor and an activator, wherein the catalyst system is capable of providing a luminescence, the method comprising: performing a time resolved luminescence analysis on a reference analyte comprising the catalyst precursor that is not in combination with the activator, and performing a time resolved luminescence analysis on a sample analyte comprising the catalyst precursor in combination with the activator, determining a reference emission energy and a reference lifetime each associated with a maximum emission intensity in the reference output values; determining a sample emission energy and a sample lifetime each associated with a maximum emission intensity in the sample output values; and comparing the values to determine if the sample comprises an activated catalyst site. Use of the above method in relation to an activation index is also disclosed.

    摘要翻译： 本文公开了一种用于确定催化剂体系中活化催化剂位点的存在的方法，其包括催化剂前体和活化剂，其中所述催化剂体系能够提供发光，所述方法包括：对参考物进行时间分辨发光分析 分析物，其包含不与活化剂组合的催化剂前体，并且对包含催化剂前体的样品分析物与活化剂组合进行时间分辨发光分析，确定参考发射能量和参考寿命，每个与最大发射相关联 参考输出值的强度; 确定每个与样本输出值中的最大发射强度相关联的样本发射能量和采样寿命; 并比较这些值以确定样品是否包含活化的催化剂位点。 还公开了关于活化指数的上述方法的使用。

    Metallocene compositions
    7.
    发明授权
    Metallocene compositions 有权

    公开(公告)号：US06414095B1

    公开(公告)日：2002-07-02

    申请号：US09620303

    申请日：2000-07-19

    申请人： Terry John Burkhardt ,  William T. Haygood, Jr. ,  Robert Tan Li ,  James Charles Vizzini ,  Matthew Cornyn Kuchta ,  Udo M. Stehling ,  James R. Hart

    发明人： Terry John Burkhardt ,  William T. Haygood, Jr. ,  Robert Tan Li ,  James Charles Vizzini ,  Matthew Cornyn Kuchta ,  Udo M. Stehling ,  James R. Hart

    IPC分类号： C08F494

    CPC分类号： C07F17/00 ,  C08F4/65908 ,  C08F4/65912 ,  C08F4/65916 ,  C08F10/00 ,  C08F110/02 ,  C08F110/06 ,  C08F210/06 ,  C08F210/16 ,  Y10S526/943 ,  C08F4/65927 ,  C08F2500/12 ,  C08F2500/03 ,  C08F2500/17 ,  C08F2500/15 ,  C08F2500/21

    摘要： This invention relates to metallocene compositions and their use in the preparation of catalyst systems for olefin polymerization, particularly propylene polymerization The metallocene compositions may be represented by the formula: wherein M1 is selected from the group consisting of titanium, zirconium, hafnium, vanadium, niobium, tantalum, chromium, molybdenum and tungsten; R1 and R2 are identical or different, and are one of a hydrogen atom, a C1-C10 alkyl group, a C1-C10 alkoxy group, a C6-C10 aryl group, a C6-C10 aryloxy group, a C2-C40 alkenyl group, a C7-C40 arylalkyl group, a C7-C40 alkylaryl group, a C8-C40 arylalkenyl group, an OH group or a halogen atom or a conjugated diene which is optionally substituted with one or more hydrocarbyl, tri(hydrocarbyl)silyl groups or tri(hydrocarbyl)silylhydrocarbyl groups, said diene having up to 30 atoms not counting hydrogen; R3 are identical or different and are each a hydrogen atom, a halogen atom, a C1-C10 alkyl group which may be halogenated, a C6-C10 aryl group which may be halogenated, a C2-C10 alkenyl group, a C7-C40-arylalkyl group, a C7-C40 alkylaryl group, a C8-C40 arylalkenyl group, a —NR′2, —SR′, —OR′, —OSiR′3 or —PR′2 radical, wherein R is one of a halogen atom, a C1-C10 alkyl group, or a C6-C10 aryl group; R4 to R7 are identical or different and are hydrogen, as defined for R3 or two or more adjacent radicals R5 to R7 together with the atoms connecting them form one or more rings; R13 is  —B(R14)—, —Al(R14)—, —Ge—, —Sn—, —O—, —S—, —SO—, —SO2—, —N(R14)—, —CO—, —P(R14)—, or P(O)(R14)—, or an amidoborane radical;  wherein: R14, R15and R16 are identical or different and are a hydrogen atom, a halogen atom, a C1-C20 alkyl group, a C1-C20 fluoroalkyl or silaalkyl group, a C6-C30 aryl group, a C6-C30 fluoroaryl group, a C1-C20 alkoxy group, a C2-C20 alkenyl group, a C7-C40 arylalkyl group, a C8-C40 arylalkenyl group, a C7-C40 alkylaryl group, or R14 and R15, together with the atoms binding them, form a cyclic ring; or, R13 is represented by the formula: wherein R17 to R24 are as defined for R1 and R2, or two or more adjacent radicals R17 to R24, including R20 and R21, together with the atoms connecting them form one or more rings; M2 is one or more carbons, silicon, germanium or tin; R8, R10 and R12 are identical or different and have the meanings stated for R4 to R7; R9 and R11 are identical or different and are a Group 14 radical having from 1 to 20 carbon atoms or are each primary, secondary or tertiary butyl groups, aryl groups, isopropyl groups, fluoroalkyl groups, triallyl silyl groups, or other groups of similar size.

    SHARED DATA COLLECTIONS
    10.
    发明申请
    SHARED DATA COLLECTIONS 有权
    共享数据收集

    公开(公告)号：US20110320407A1

    公开(公告)日：2011-12-29

    申请号：US12821971

    申请日：2010-06-23

    申请人： Matthew S. Augustine ,  John Burkhardt ,  Brian M. Lambert ,  Raymond E. Ozzie ,  Jason E. Schleifer ,  Richard Z. Speyer ,  Paresh S. Suthar

    发明人： Matthew S. Augustine ,  John Burkhardt ,  Brian M. Lambert ,  Raymond E. Ozzie ,  Jason E. Schleifer ,  Richard Z. Speyer ,  Paresh S. Suthar

    IPC分类号： G06F17/30

    CPC分类号： G06F17/30351 ,  G06F9/543 ,  G06Q10/109

    摘要： A data sharing mechanism may allow programs to share access to data collections. The mechanisms that implement the sharing may allow programs written in any language to read and write a shared collection. The mechanisms may make the shared nature of the collection relatively transparent to the program and to the programmer, by allowing a program to operate on the data more or less as if it were purely local data. The sharing of collections may be managed by a shared object runtime on each machine on which a collection is used, and by a shared object server. The shared object server maintains the true state of the collection, and deterministically resolves collections when programs operate on the same collection without knowledge of each other's operations. The mechanisms by which collections are shared may be implemented so as to be agnostic as to the kind of data in the collection.

    摘要翻译： 数据共享机制可能允许程序共享对数据收集的访问。 实现共享的机制可能允许以任何语言编写的程序来读写共享集合。 这些机制可以使程序和程序员的共享性能相对透明化，允许程序对数据的操作或多或少就像纯粹的本地数据一样。 集合的共享可以由使用集合的每个机器上的共享对象运行时以及共享对象服务器来管理。 共享对象服务器维护集合的真实状态，并且当程序在相同集合上运行时确定性地解析集合，而不了解对方的操作。 可以实现共享收藏的机制，以便与收藏中的数据类型无关。