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19 条记录 (耗时 0.015 秒)

    Method for producing (meth)acrylate derivative having isocyanate group
    2.
    发明授权
    Method for producing (meth)acrylate derivative having isocyanate group 有权
    具有异氰酸酯基的（甲基）丙烯酸酯衍生物的制造方法

    公开(公告)号：US07632965B2

    公开(公告)日：2009-12-15

    申请号：US10594231

    申请日：2005-03-22

    申请人： Kaneo Nozawa ,  Katsutoshi Morinaka

    发明人： Kaneo Nozawa ,  Katsutoshi Morinaka

    IPC分类号： C07C263/20 ,  C07C265/04

    CPC分类号： C07C263/20 ,  C07C263/16 ,  C07C265/04

    摘要： The invention aims to provide a method whereby (meth)acrylate derivatives having an isocyanate group can be obtained in high yield by dehydrochlorination of 3-chloropropionate derivatives having an isocyanate group under industrially advantageous and mild conditions, and the content of residual hydrolyzable chlorine can be reduced. A method for producing a (meth)acrylate derivative having an isocyanate group comprises performing dehydrochlorination of a 3-chloropropionate derivative having an isocyanate group in the presence of a basic nitrogen compound having a tertiary nitrogen, the tertiary nitrogen of the basic nitrogen compound having at least one group other than an aromatic ring group.

    摘要翻译： 本发明的目的在于提供一种方法，可以在工业上有利且温和的条件下，通过使具有异氰酸酯基的3-氯丙酸酯衍生物的脱氯化氢以高产率获得具有异氰酸酯基的（甲基）丙烯酸酯衍生物，残留的可水解氯的含量可以为 减少 具有异氰酸酯基的（甲基）丙烯酸酯衍生物的制造方法包括在具有叔氮的碱性氮化合物的存在下，对具有异氰酸酯基的3-氯丙酸酯衍生物进行脱氯化氢，碱式氮化合物的叔氮具有 除芳香族环以外的至少一个基团。

    Process for preparing high purity (meth)acryloyloxyalkyl, isocyanate
    3.
    发明申请
    Process for preparing high purity (meth)acryloyloxyalkyl, isocyanate 有权
    制备高纯度（甲基）丙烯酰氧基烷基，异氰酸酯的方法

    公开(公告)号：US20060241319A1

    公开(公告)日：2006-10-26

    申请号：US10566178

    申请日：2004-07-27

    申请人： Katsutoshi Morinaka ,  Kazuyoshi Hoshi

    发明人： Katsutoshi Morinaka ,  Kazuyoshi Hoshi

    IPC分类号： C07C263/18

    CPC分类号： C07C263/18 ,  C07C263/20 ,  C07C265/04

    摘要： A process for preparing a high purity (meth)acryloyloxyalkyl isocyanate having a very small hydrolyzable chlorine content is provided. The high purity (meth)acryloyloxyalkyl isocyanate is prepared by subjecting a hydrolyzable chlorine containing (meth)acryloyloxyalkyl isocyanate to mixing treatment with an epoxy compound and an amine at a temperature of from 110 to 160° C. to prepare a mixture; and preparing a high purity (meth)acryloyloxyalkyl isocyanate from the resulting mixture with distillation. In particular, it is possible to effectively prevent (meth)acryloyloxyalkyl isocyanate from polymerization during the distillation by adding a polymerization inhibitor such as phenothiazine and the like.

    摘要翻译： 提供了制备具有非常小的可水解氯含量的高纯度（甲基）丙烯酰氧基烷基异氰酸酯的方法。 高纯度（甲基）丙烯酰氧基烷基异氰酸酯通过使可水解的含氯（甲基）丙烯酰氧基烷基异氰酸酯在环境化合物和胺混合处理，在110〜160℃的温度下进行混合来制备。 并通过蒸馏从所得混合物中制备高纯度（甲基）丙烯酰氧基烷基异氰酸酯。 特别地，可以通过加入阻聚剂如吩噻嗪等在蒸馏期间有效地防止（甲基）丙烯酰氧基烷基异氰酸酯聚合。

    Stabilized (meth)acryloyloxyalkyl isocyanate a process for stabilization thereof and a process for preparation of the same
    4.
    发明申请
    Stabilized (meth)acryloyloxyalkyl isocyanate a process for stabilization thereof and a process for preparation of the same 审中-公开
    稳定的（甲基）丙烯酰氧基烷基异氰酸酯，其稳定化方法及其制备方法

    公开(公告)号：US20060229464A1

    公开(公告)日：2006-10-12

    申请号：US10566184

    申请日：2004-07-27

    申请人： Katsutoshi Morinaka ,  Toshiaki Ishikawa ,  Kazuyoshi Hoshi

    发明人： Katsutoshi Morinaka ,  Toshiaki Ishikawa ,  Kazuyoshi Hoshi

    IPC分类号： C07C265/16

    CPC分类号： C07C263/18 ,  C07C265/16

    摘要： The present invention provides a stabilized (meth)acryloyloxyalkyl isocyanate, a process for stabilization thereof and a process for preparation of the same. More particularly, it provides a (meth)acryloyloxyalkyl isocyanate having a small hydrolyzable chlorine content and good storage stability, a process for stabilizing a (meth)acryloyloxyalkyl isocyanate prepared using phosgene which process comprises decreasing the amount of a hydrolyzable chlorine with purification and a process for preparation of a stabilized (meth)acryloyloxyalkyl isocyanate. An acidic gas such as carbon dioxide or the like was forcedly dissolved in (meth)acryloyloxyalkyl isocyanate, particularly (meth)acryloyloxyalkyl isocyanate which content of hydrolyzable chlorine is decreased with purification and thereby the storage stability of the (meth)acryloyloxyalkyl isocyanate is improved.

    摘要翻译： 本发明提供稳定的（甲基）丙烯酰氧基烷基异氰酸酯，其稳定化方法及其制备方法。 更具体地说，它提供了具有小的可水解氯含量和良好的储存稳定性的（甲基）丙烯酰氧基烷基异氰酸酯，稳定使用光气制备的（甲基）丙烯酰氧基烷基异氰酸酯的方法，该方法包括通过纯化降低可水解氯的量和方法 用于制备稳定的（甲基）丙烯酰氧基烷基异氰酸酯。 特别是（甲基）丙烯酰氧基烷基异氰酸酯，特别是可水解氯的含量降低的（甲基）丙烯酰氧基烷基异氰酸酯的酸性气体等二氧化碳等，从而提高了（甲基）丙烯酰氧基烷基异氰酸酯的保存稳定性。

    Epoxy group-containing organosiloxane compound, curable composition for transfer materials and method for forming micropattern using the composition
    7.
    发明授权
    Epoxy group-containing organosiloxane compound, curable composition for transfer materials and method for forming micropattern using the composition 失效
    含有环氧基的有机硅氧烷化合物，转印材料用固化性组合物和使用该组合物形成微图案的方法

    公开(公告)号：US08604150B2

    公开(公告)日：2013-12-10

    申请号：US12741148

    申请日：2008-11-05

    申请人： Katsutoshi Morinaka ,  Yoshikazu Arai ,  Hiroshi Uchida ,  Toshio Fujita

    发明人： Katsutoshi Morinaka ,  Yoshikazu Arai ,  Hiroshi Uchida ,  Toshio Fujita

    IPC分类号： C08G77/08

    CPC分类号： B82Y40/00 ,  B82Y10/00 ,  C07F7/0838 ,  C07F7/21 ,  C08G59/306 ,  C08G59/3281 ,  C08G59/42 ,  G03F7/0002 ,  G03F7/0757

    摘要： The present invention has an object to provide a curable composition for transfer materials. The curable composition is applicable to a UV nanoimprint process capable of forming micropatterns with high throughput, is applicable to a thermal nanoimprint process in some cases, and is capable of forming a micropattern having high selectivity on etching rates regarding a fluorine-based gas and an oxygen gas. A curable composition for transfer materials of the present invention contains a curable silicon compound produced by subjecting a silicon compound (A) having a Si—H group and a compound (B) having a curable functional group and a carbon-carbon double bond other than the curable functional group to a hydrosilylation reaction.

    摘要翻译： 本发明的目的是提供一种转印材料用固化性组合物。 该可固化组合物可应用于能够形成具有高通量的微图案的UV纳米压印法，在一些情况下可应用于热纳米压印工艺，并且能够形成对氟基气体和 氧气 本发明的转印材料用固化性组合物含有通过使具有Si-H基的硅化合物（A）和具有固化性官能团的化合物（B）和碳 - 碳双键以外的碳 - 碳双键 可固化的官能团进行氢化硅烷化反应。

    Photosensitive resin composition, cured product thereof and production method of printed circuit board using the same
    8.
    发明授权
    Photosensitive resin composition, cured product thereof and production method of printed circuit board using the same 有权
    光敏树脂组合物，其固化产物和使用其的印刷电路板的制备方法

    公开(公告)号：US07790354B2

    公开(公告)日：2010-09-07

    申请号：US11587162

    申请日：2005-04-21

    申请人： Satoru Ishigaki ,  Hiroshi Uchida ,  Yoshio Miyajima ,  Katsutoshi Morinaka

    发明人： Satoru Ishigaki ,  Hiroshi Uchida ,  Yoshio Miyajima ,  Katsutoshi Morinaka

    IPC分类号： G03F7/00 ,  G03F7/004 ,  G03F7/035

    CPC分类号： G03F7/027 ,  C08G18/0823 ,  C08G18/4854 ,  C08G18/672 ,  C08G18/755 ,  C09D175/16 ,  G03F7/032 ,  G03F7/033 ,  G03F7/035 ,  G03F7/038 ,  G03F7/0388 ,  H05K3/287 ,  Y10T428/31855 ,  C08G18/6692

    摘要： There are provided a novel photosensitive resin composition, a cured film of which has ample flexibility, and which yields an insulating protective coating having superior soldering heat resistance, thermal degradation resistance and electroless gold plating resistance. The photosensitive resin composition as claimed in the present invention comprises: a photopolymerizable component containing a urethane acrylate compound (A) and a compound (B) having an ethylenic unsaturated group other than said urethane acrylate compound (A), a thermosetting resin (C), a photopolymerization initiator (D) and a thermal polymerization catalyst (E); wherein, said urethane acrylate compound (A) is the reaction product of an isocyanate compound (a-1) of the following general formula (1): CH2═CH—COO—R—NCO  (1) (wherein, R represents a hydrocarbon group having 1 to 30 carbon atoms) with a polyhydroxy compound (a-2).

    摘要翻译： 提供了一种新颖的感光性树脂组合物，其固化膜具有充分的柔软性，并且产生具有优异的耐焊接耐热性，耐热劣化性和无电镀金电镀性的绝缘保护涂层。 本发明的感光性树脂组合物包含：含有氨基甲酸酯丙烯酸酯化合物（A）和除所述氨基甲酸酯丙烯酸酯化合物（A）以外具有乙烯性不饱和基团的化合物（B）的光聚合性成分，热固性树脂（C） ，光聚合引发剂（D）和热聚合催化剂（E）; 其中，所述氨基甲酸酯丙烯酸酯化合物（A）是以下通式（1）的异氰酸酯化合物（a-1）：CH 2 = CH-COO-R-NCO（1）（其中，R表示烃 具有1至30个碳原子的基团）与多羟基化合物（a-2）反应。

    Process for preparing high purity (meth) acryloyloxyalkyl isocyanate
    10.
    发明授权
    Process for preparing high purity (meth) acryloyloxyalkyl isocyanate 有权
    制备高纯度（甲基）丙烯酰氧基烷基异氰酸酯的方法

    公开(公告)号：US07417163B2

    公开(公告)日：2008-08-26

    申请号：US10566178

    申请日：2004-07-27

    申请人： Katsutoshi Morinaka ,  Kazuyoshi Hoshi

    发明人： Katsutoshi Morinaka ,  Kazuyoshi Hoshi

    IPC分类号： C07C263/18

    CPC分类号： C07C263/18 ,  C07C263/20 ,  C07C265/04

    摘要： A process for preparing a high purity (meth)acryloyloxyalkyl isocyanate having a very small hydrolyzable chlorine content is provided. The high purity (meth)acryloyloxyalkyl isocyanate is prepared by subjecting a hydrolyzable chlorine containing (meth)acryloyloxyalkyl isocyanate to mixing treatment with an epoxy compound and an amine at a temperature of from 110 to 160° C. to prepare a mixture; and preparing a high purity (meth)acryloyloxyalkyl isocyanate from the resulting mixture with distillation. In particular, it is possible to effectively prevent (meth)acryloyloxyalkyl isocyanate from polymerization during the distillation by adding a polymerization inhibitor such as phenothiazine and the like.

    摘要翻译： 提供了制备具有非常小的可水解氯含量的高纯度（甲基）丙烯酰氧基烷基异氰酸酯的方法。 高纯度（甲基）丙烯酰氧基烷基异氰酸酯通过使可水解的含氯（甲基）丙烯酰氧基烷基异氰酸酯在环境化合物和胺混合处理，在110〜160℃的温度下进行混合来制备。 并通过蒸馏从所得混合物中制备高纯度（甲基）丙烯酰氧基烷基异氰酸酯。 特别地，可以通过加入阻聚剂如吩噻嗪等在蒸馏期间有效地防止（甲基）丙烯酰氧基烷基异氰酸酯聚合。