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1.发明授权Nanocomposite for fuel cell, method of preparing the nanocomposite, and fuel cell including the nanocomposite 有权用于燃料电池的纳米复合材料，制备纳米复合材料的方法和包括纳米复合材料的燃料电池公开(公告)号：US08084167B2
公开(公告)日：2011-12-27
申请号：US11985531
申请日：2007-11-14
Applicant: Jeong-hee Lee , Jae-young Choi , Chan-ho Pak , Eun-ju Ra , Young-hee Lee , Kay-hyeok An
Inventor： Jeong-hee Lee , Jae-young Choi , Chan-ho Pak , Eun-ju Ra , Young-hee Lee , Kay-hyeok An
IPC: H01M4/02
CPC classification number: H01M4/92 , B82Y30/00 , D01F9/20 , D01F11/04 , H01M4/90 , H01M4/9083 , H01M4/926 , H01M2008/1095 , Y10S977/948
Abstract: Provided is a nanocomposite for the catalyst layer of a fuel cell electrode including: a carbon nanofiber; and metal catalyst particles uniformly applied to the surface of the carbon nanofiber, wherein the carbon nanofiber has a surface oxygen content of at least 0.03 calculated by the formula: Oxygen content=[atomic percentage of oxygen/atomic percentage of carbon] using atomic percentages of oxygen and carbon, respectively calculated from an area of an oxygen peak having a binding energy of 524 to 540 eV, an area of a nitrogen peak having a binding energy of 392 to 404 eV, and an area of a carbon peak having a binding energy of 282 to 290 eV in X-ray photoelectron spectroscopy. The nanocomposite according to the present invention has high surface oxygen content and has metal catalyst nano particles densely and uniformly distributed on the outer wall of the carbon fibers, thereby having high electrochemical efficiency. Thus, efficiency of fuel cells can be improved using the nanocomposite.
Abstract translation: 提供一种用于燃料电池电极的催化剂层的纳米复合材料，其包括：碳纳米纤维; 和金属催化剂颗粒均匀地施加到碳纳米纤维的表面上，其中碳纳米纤维的表面氧含量至少为0.03，由下式计算：氧含量= [原子百分比的氧/原子百分比的碳]使用原子百分比 氧和碳分别由具有524至540eV的结合能的氧峰的面积，具有392至404eV的结合能的氮峰的面积和具有结合能的碳峰的面积计算 在X射线光电子能谱中为282〜290eV。 根据本发明的纳米复合材料具有高的表面氧含量，并且在碳纤维的外壁上密集均匀地分布有金属催化剂纳米颗粒，从而具有高的电化学效率。 因此，可以使用纳米复合材料来提高燃料电池的效率。
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2.发明申请Nanocomposite for fuel cell, method of preparing the nanocomposite, and fuel cell including the nanocomposite 有权用于燃料电池的纳米复合材料，制备纳米复合材料的方法和包括纳米复合材料的燃料电池公开(公告)号：US20080176129A1
公开(公告)日：2008-07-24
申请号：US11985531
申请日：2007-11-14
Applicant: Jeong-hee Lee , Jae-young Choi , Chan-ho Pak , Eun-ju Ra , Young-hee Lee , Kay-hyeok An
Inventor： Jeong-hee Lee , Jae-young Choi , Chan-ho Pak , Eun-ju Ra , Young-hee Lee , Kay-hyeok An
CPC classification number: H01M4/92 , B82Y30/00 , D01F9/20 , D01F11/04 , H01M4/90 , H01M4/9083 , H01M4/926 , H01M2008/1095 , Y10S977/948
Abstract: Provided is a nanocomposite for the catalyst layer of a fuel cell electrode including: a carbon nanofiber; and metal catalyst particles uniformly applied to the surface of the carbon nanofiber, wherein the carbon nanofiber has a surface oxygen content of at least 0.03 calculated by the formula: Oxygen content=[atomic percentage of oxygen/atomic percentage of carbon] using atomic percentages of oxygen and carbon, respectively calculated from an area of an oxygen peak having a binding energy of 524 to 540 eV, an area of a nitrogen peak having a binding energy of 392 to 404 eV, and an area of a carbon peak having a binding energy of 282 to 290 eV in X-ray photoelectron spectroscopy. The nanocomposite according to the present invention has high surface oxygen content and has metal catalyst nano particles densely and uniformly distributed on the outer wall of the carbon fibers, thereby having high electrochemical efficiency. Thus, efficiency of fuel cells can be improved using the nanocomposite.
Abstract translation: 提供一种用于燃料电池电极的催化剂层的纳米复合材料，其包括：碳纳米纤维; 和金属催化剂颗粒均匀地施加到碳纳米纤维的表面上，其中碳纳米纤维的表面氧含量至少为0.03，由下式计算：氧含量= [原子百分比的氧/原子百分比的碳]使用原子百分比 氧和碳分别由具有524至540eV的结合能的氧峰的面积，具有392至404eV的结合能的氮峰的面积和具有结合能的碳峰的面积计算 在X射线光电子能谱中为282〜290eV。 根据本发明的纳米复合材料具有高的表面氧含量，并且在碳纤维的外壁上密集均匀地分布有金属催化剂纳米颗粒，从而具有高的电化学效率。 因此，可以使用纳米复合材料来提高燃料电池的效率。
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3.发明申请METHOD FOR EFFICIENT AL-C COVALENT BOND FORMATION BETWEEN ALUMINUM AND CARBON MATERIAL 审中-公开铝和碳材料之间有效的AL-C共价键结合方法公开(公告)号：US20090176090A1
公开(公告)日：2009-07-09
申请号：US12179541
申请日：2008-07-24
Applicant: Kang Pyo So , Young Hee Lee , Kay Hyeok An
Inventor： Kang Pyo So , Young Hee Lee , Kay Hyeok An
CPC classification number: C25D5/54 , C22C26/00 , C22C32/0084 , C22C47/02 , C22C49/06 , C22C2026/002 , C25D3/44 , Y10T428/2918 , Y10T428/2982
Abstract: Disclosed is a method of forming an Al—C covalent bond between aluminum and a carbon material by applying an electric arc to a mixture of the aluminum and the carbon material under vacuum, heated and pressurized conditions. In order to enhance the reactivity of the carbon material, the method may include the step of introducing defects in the carbon material and thus functionalizing the carbon material by treating the carbon material with acid, a microwave, or plasma.
Abstract translation: 公开了通过在真空，加热和加压条件下向铝和碳材料的混合物施加电弧而在铝和碳材料之间形成Al-C共价键的方法。 为了提高碳材料的反应性，该方法可以包括在碳材料中引入缺陷并由此通过用酸，微波或等离子体处理碳材料来官能化碳材料的步骤。
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4.发明授权Supercapacitor using electrode of new material and method of manufacturing the same 失效使用新材料的电极的超级电容器及其制造方法公开(公告)号：US06454816B1
公开(公告)日：2002-09-24
申请号：US09805921
申请日：2001-03-15
Applicant: Young-hee Lee , Kay-hyeok An , Jae-eun Yoo
Inventor： Young-hee Lee , Kay-hyeok An , Jae-eun Yoo
IPC: H01G900
CPC classification number: H01G9/155 , B82Y10/00 , Y02E60/13 , Y02T10/7022 , Y10S977/948 , Y10T29/417
Abstract: A supercapacitor using an electrode formed of a new material is provided. The supercapacitor includes two electrodes facing each other, the electrodes being composed of carbon nanotubes, an electrolyte provided between the two electrodes, and a separator for separating the electrolyte between the two electrodes.
Abstract translation: 提供了使用由新材料形成的电极的超级电容器。 超级电容器包括彼此面对的两个电极，电极由碳纳米管组成，设置在两个电极之间的电解质和用于在两个电极之间分离电解质的隔板。
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5.发明授权Carbon-fiber web structure type field emitter electrode and fabrication method of the same 失效碳纤维网结构型场发射极电极及其制造方法相同公开(公告)号：US08058787B2
公开(公告)日：2011-11-15
申请号：US12236337
申请日：2008-09-23
Applicant: Seung Hyun Ra , Kay Hyeok An , Young Hee Lee , Jong Myeon Lee
Inventor： Seung Hyun Ra , Kay Hyeok An , Young Hee Lee , Jong Myeon Lee
IPC: H01J9/02
CPC classification number: H01J1/304 , B82Y10/00 , D01D5/003 , H01J9/025 , H01J2201/30469
Abstract: The present invention provides a field emitter electrode and a method for fabricating the same. The method comprises the steps of mixing a carbonizable polymer, carbon nanotubes and a solvent to prepare a carbon nanotube-containing polymer solution, electrospinning (or electrostatic spinning) the polymer solution to form a nanofiber web layer on a substrate, stabilizing the nanofiber web layer such that the polymer present in the nanofiber web layer is crosslinked, and carbonizing the nanofiber web layer such that the crosslinked polymer is converted to a carbon fiber.
Abstract translation: 本发明提供一种场致发射电极及其制造方法。 该方法包括将可碳化聚合物，碳纳米管和溶剂混合以制备含碳纳米管的聚合物溶液，静电纺丝（或静电纺丝）聚合物溶液以在基材上形成纳米纤维网层，稳定纳米纤维网层 使得存在于纳米纤维网层中的聚合物交联，并将纳米纤维网层碳化，使得交联聚合物转化为碳纤维。
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Patent Agency Ranking
6.发明授权Carbon nanotube, support catalyst, method of preparing the support catalyst and a fuel cell comprising the support catalyst 有权碳纳米管，载体催化剂，制备载体催化剂的方法和包含载体催化剂的燃料电池公开(公告)号：US08017282B2
公开(公告)日：2011-09-13
申请号：US11897144
申请日：2007-08-28
Applicant: Jae-young Choi , Chan-ho Pak , Seok-gwang Doo , Jeong-hee Lee , Young-hee Lee , Kay-hyeok An , Sung-jin Kim
Inventor： Jae-young Choi , Chan-ho Pak , Seok-gwang Doo , Jeong-hee Lee , Young-hee Lee , Kay-hyeok An , Sung-jin Kim
IPC: H01M4/36
CPC classification number: H01M4/8605 , B01J21/185 , B01J23/42 , B01J35/006 , B01J37/06 , B01J37/346 , B82Y30/00 , B82Y40/00 , C01B32/168 , H01M4/9008 , H01M4/9041 , H01M4/9083 , H01M8/086 , H01M2008/1095 , Y10S977/948
Abstract: Carbon nanotubes have an R value of at least 1.3, where R is defined as the ratio (ID/IG) of an integral value of D band intensity (ID) to an integral value of G band intensity (IG) in the Raman spectrum. Such carbon nanotubes can be used to form a support catalyst with good catalyst activity because the surface defects on the carbon nanotubes promote improved catalyst distribution in that the support catalyst includes catalyst particles having a small mean particle size and a slight variation in particle size. Such a support catalyst has particularly useful properties when used as a catalyst layer for a fuel cell electrode.
Abstract translation: 碳纳米管的R值至少为1.3，其中R被定义为拉曼光谱中D带强度（ID）的积分值与G带强度（IG）的积分值的比（ID / IG）。 这种碳纳米管可用于形成具有良好催化剂活性的载体催化剂，因为碳纳米管上的表面缺陷促进了催化剂分布的改善，因为载体催化剂包括具有小的平均粒径和微小粒度变化的催化剂颗粒。 当用作燃料电池电极的催化剂层时，这种载体催化剂具有特别有用的特性。
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7.发明授权公开(公告)号：US07438622B2
公开(公告)日：2008-10-21
申请号：US11064960
申请日：2005-02-25
Applicant: Seung Hyun Ra , Kay Hyeok An , Young Hee Lee , Jong Myeon Lee
Inventor： Seung Hyun Ra , Kay Hyeok An , Young Hee Lee , Jong Myeon Lee
CPC classification number: H01J1/304 , B82Y10/00 , D01D5/003 , H01J9/025 , H01J2201/30469
Abstract: The present invention provides a field emitter electrode and a method for fabricating the same. The method comprises the steps of mixing a carbonizable polymer, carbon nanotubes and a solvent to prepare a carbon nanotube-containing polymer solution, electrospinning (or electrostatic spinning) the polymer solution to form a nanofiber web layer on a substrate, stabilizing the nanofiber web layer such that the polymer present in the nanofiber web layer is crosslinked, and carbonizing the nanofiber web layer such that the crosslinked polymer is converted to a carbon fiber.
Abstract translation: 本发明提供一种场致发射电极及其制造方法。 该方法包括将可碳化聚合物，碳纳米管和溶剂混合以制备含碳纳米管的聚合物溶液，静电纺丝（或静电纺丝）聚合物溶液以在基材上形成纳米纤维网层，稳定纳米纤维网层 使得存在于纳米纤维网层中的聚合物交联，并将纳米纤维网层碳化，使得交联聚合物转化为碳纤维。
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8.发明授权公开(公告)号：US08283091B2
公开(公告)日：2012-10-09
申请号：US13200256
申请日：2011-09-21
Applicant: Jeong-hee Lee , Jae-young Choi , Chan-ho Pak , Eun-ju Ra , Young-hee Lee , Kay-hyeok An
Inventor： Jeong-hee Lee , Jae-young Choi , Chan-ho Pak , Eun-ju Ra , Young-hee Lee , Kay-hyeok An
IPC: H01M4/02
CPC classification number: H01M4/92 , B82Y30/00 , D01F9/20 , D01F11/04 , H01M4/90 , H01M4/9083 , H01M4/926 , H01M2008/1095 , Y10S977/948
Abstract: Provided is a carbon nanofiber, wherein the carbon nanofiber has a surface oxygen content of at least 0.03 calculated by the formula: Oxygen content=[atomic percentage of oxygen/atomic percentage of carbon] using atomic percentages of oxygen and carbon, respectively calculated from an area of an oxygen peak having a binding energy of 524 to 540 eV, an area of a nitrogen peak having a binding energy of 392 to 404 eV, and an area of a carbon peak having a binding energy of 282 to 290 eV in X-ray photoelectron spectroscopy. The nanofibers have high surface oxygen content and may have metal catalyst nano particles densely and uniformly distributed on the outer wall of the carbon nanofibers, thereby having high electrochemical efficiency.
Abstract translation: 本发明提供一种碳纳米纤维，其中，所述碳纳米纤维的表面氧含量为0.03以下，由下列公式计算：氧含量= [氧的原子百分比/碳的原子百分比]，使用原子百分比的氧和碳，分别由 具有结合能为524至540eV的氧峰的面积，结合能为392至404eV的氮峰的面积，以及具有282至290eV的结合能的碳峰的面积， ray光电子能谱。 纳米纤维具有高表面氧含量，并且可以使金属催化剂纳米颗粒密集均匀地分布在碳纳米纤维的外壁上，从而具有高的电化学效率。
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9.发明申请Nanocomposite for fuel cell, method of preparing the nanocomposite, and fuel cell including the nanocomposite 失效用于燃料电池的纳米复合材料，制备纳米复合材料的方法和包括纳米复合材料的燃料电池公开(公告)号：US20120046434A1
公开(公告)日：2012-02-23
申请号：US13200256
申请日：2011-09-21
Applicant: Jeong-hee Lee , Jae-young Choi , Chan-ho Pak , Eun-ju Ra , Young-hee Lee , Kay-hyeok An
Inventor： Jeong-hee Lee , Jae-young Choi , Chan-ho Pak , Eun-ju Ra , Young-hee Lee , Kay-hyeok An
CPC classification number: H01M4/92 , B82Y30/00 , D01F9/20 , D01F11/04 , H01M4/90 , H01M4/9083 , H01M4/926 , H01M2008/1095 , Y10S977/948
Abstract: Provided is a nanocomposite for the catalyst layer of a fuel cell electrode including: a carbon nanofiber; and metal catalyst particles uniformly applied to the surface of the carbon nanofiber, wherein the carbon nanofiber has a surface oxygen content of at least 0.03 calculated by the formula: Oxygen content=[atomic percentage of oxygen/atomic percentage of carbon] using atomic percentages of oxygen and carbon, respectively calculated from an area of an oxygen peak having a binding energy of 524 to 540 eV, an area of a nitrogen peak having a binding energy of 392 to 404 eV, and an area of a carbon peak having a binding energy of 282 to 290 eV in X-ray photoelectron spectroscopy. The nanocomposite has high surface oxygen content and has metal catalyst nano particles densely and uniformly distributed on the outer wall of the carbon fibers, thereby having high electrochemical efficiency.
Abstract translation: 提供一种用于燃料电池电极的催化剂层的纳米复合材料，其包括：碳纳米纤维; 和金属催化剂颗粒均匀地施加到碳纳米纤维的表面上，其中碳纳米纤维的表面氧含量至少为0.03，由下式计算：氧含量= [原子百分比的氧/原子百分比的碳]使用原子百分比 氧和碳分别由具有524至540eV的结合能的氧峰的面积，具有392至404eV的结合能的氮峰的面积和具有结合能的碳峰的面积计算 在X射线光电子能谱中为282〜290eV。 纳米复合材料具有高表面氧含量，并且具有金属催化剂纳米颗粒密集均匀地分布在碳纤维的外壁上，从而具有高的电化学效率。
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10.发明申请CARBON-FIBER WEB STRUCTURE TYPE FIELD EMITTER ELECTRODE AND FABRICATION METHOD OF THE SAME 失效碳纤维网状结构型场发射体电极及其制造方法公开(公告)号：US20100277052A1
公开(公告)日：2010-11-04
申请号：US12236337
申请日：2008-09-23
Applicant: Seung Hyun Ra , Kay Hyeok An , Young Hee Lee , Jong Myeon Lee
Inventor： Seung Hyun Ra , Kay Hyeok An , Young Hee Lee , Jong Myeon Lee
IPC: H01J1/02
CPC classification number: H01J1/304 , B82Y10/00 , D01D5/003 , H01J9/025 , H01J2201/30469
Abstract: The present invention provides a field emitter electrode and a method for fabricating the same. The method comprises the steps of mixing a carbonizable polymer, carbon nanotubes and a solvent to prepare a carbon nanotube-containing polymer solution, electrospinning (or electrostatic spinning) the polymer solution to form a nanofiber web layer on a substrate, stabilizing the nanofiber web layer such that the polymer present in the nanofiber web layer is crosslinked, and carbonizing the nanofiber web layer such that the crosslinked polymer is converted to a carbon fiber.
Abstract translation: 本发明提供一种场致发射电极及其制造方法。 该方法包括将可碳化聚合物，碳纳米管和溶剂混合以制备含碳纳米管的聚合物溶液，静电纺丝（或静电纺丝）聚合物溶液以在基材上形成纳米纤维网层，使纳米纤维网层 使得存在于纳米纤维网层中的聚合物交联，并将纳米纤维网层碳化，使得交联聚合物转化为碳纤维。
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