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1.发明申请METHODS FOR THE MANUFACTURE OF ACETALS AND KETALS, AND THE ACETALS AND KETALS PRODUCED THEREBY 审中-公开乙酸和乙酸乙酯的制备方法，以及生产的乙醇和乙醇公开(公告)号：US20120035376A1
公开(公告)日：2012-02-09
申请号：US13197593
申请日：2011-08-03
申请人： Brian D. Mullen , Marc D. Scholten , Andrew J. Louwagie , Steven A. Donen , Feng Jing , Vivek Badarinarayana
发明人： Brian D. Mullen , Marc D. Scholten , Andrew J. Louwagie , Steven A. Donen , Feng Jing , Vivek Badarinarayana
IPC分类号： C07D317/30
CPC分类号： C07D317/30 , Y02P20/582
摘要： A method for producing a product that comprises glycerol ketal of ethyl levulinate or propylene glycol ketal of ethyl levulinate comprises reacting either glycerol or propylene glycol with ethyl levulinate in the presence of a homogenous or heterogeneous catalyst system in a reactor system. The ethyl levulinate and either glycerol or propylene glycol are heated to remove water, polyol, and excess ethyl levulinate. The excess ethyl levulinate and polyol is recycled back to the reactor. The product is distilled in a specific fashion and optionally treated by means of a stabilizing agent or acid species removal bed, to obtain a composition comprising glycerol ketal of ethyl levulinate or propylene glycol ketal of ethyl levulinate wherein the composition comprises less than or equal to about 2 wt % contaminants.
摘要翻译： 用于生产包含乙酰乙酸乙酯乙酰丙酸乙酯或丙二醇缩酮的甘油缩酮的产物的方法包括在反应器系统中在均相或非均相催化剂体系存在下使甘油或丙二醇与乙酰乙酸乙酯反应。 将乙酰乙酸乙酯和甘油或丙二醇加热以除去水，多元醇和过量乙酰乙酸乙酯。 过量的乙酰丙酸乙酯和多元醇再循环回到反应器中。 产物以特定方式蒸馏并任选地通过稳定剂或酸物质去除床处理，以获得组合物，其包含乙酰丙酸乙酯的乙酰丙酸乙酯或丙二醇缩酮的甘油缩酮，其中组合物包含小于或等于约 2重量％的污染物。
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公开(公告)号：US20130053564A1
公开(公告)日：2013-02-28
申请号：US13370860
申请日：2012-02-10
申请人： Sergey SELIFONOV , Adam E. GOETZ , Marc D. SCHOLTEN , Ning ZHOU
发明人： Sergey SELIFONOV , Adam E. GOETZ , Marc D. SCHOLTEN , Ning ZHOU
IPC分类号： C07D407/12 , C07D407/14 , C07D405/14
CPC分类号： C07D319/06 , C07D317/30
摘要： Disclosed herein are ketal amide compounds. The ketal amide compounds are synthesized by the reaction of ketal acids or ketal esters with amine functional compounds. Also disclosed are methodologies useful to make the ketal amide compounds. Also disclosed herein are formulations and articles containing the ketal amide compounds.
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3.发明申请公开(公告)号：US20120121911A1
公开(公告)日：2012-05-17
申请号：US13294854
申请日：2011-11-11
IPC分类号： B32B27/36 , C07D317/30 , C08J9/35 , C08K5/156 , C08G63/16 , C08G14/02 , C08G18/32 , C09K3/00 , C09D163/00 , C09D175/06 , C08G64/00 , B05D7/24 , B05D3/00 , B32B27/28 , C07D407/12
CPC分类号： C08K5/1565 , C07D317/02 , C07D317/14 , C07D317/30 , C08G2/32 , C08G18/3218 , C08G63/668 , C08G63/672 , C08G63/91 , C08G64/0208 , C08G64/42 , C08G2101/0025 , C08L59/00 , C08L67/00 , C09D159/00 , C09D167/00 , Y02P20/582 , Y10T428/31507 , Y10T428/31786
摘要： Disclosed herein is a polyhydroxy ketal adduct obtained by the esterification of a hydrocarbon polyol by at least 1.5 equivalents of a ketocarboxy to produce an intermediate ketocarboxylic ester. The intermediate polyketocarboxylic ester is then ketalized to produce the polyhydroxyketal adduct, which can be used to provide a polymeric composition.
摘要翻译： 本文公开了通过烃多元醇通过至少1.5当量的酮羧基酯化以产生中间体酮羧酸酯而获得的多羟基缩酮加合物。 然后中间体多酮羧酸酯被缩醛化以产生可用于提供聚合物组合物的多羟基缩酮加合物。
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公开(公告)号：US20120118201A1
公开(公告)日：2012-05-17
申请号：US13294690
申请日：2011-11-11
IPC分类号： C08K5/1565 , C08L67/04 , C08L27/06 , C08L23/00 , C08L69/00 , C08L79/08 , C08L25/06 , C08L77/00 , C08L1/02 , C08L81/04 , C08L81/06 , C07D407/12 , C08L83/04
CPC分类号： C07D407/12 , C08K5/1565 , C08L59/02 , C08L77/00 , C08L79/08 , Y02P20/582 , C08L27/06
摘要： Disclosed herein is a polyketal adduct obtained by forming an ester between a hydrocarbon polyol and a ketocarboxylic acid to produce an intermediate polyketocarboxylic ester. The intermediate polyketocarboxylic ester can be purified via crystallization to achieve purities of greater than 99.0% and then ketalized to produce the polyketal adduct, which can be used in polymer compositions. The polyketal adduct I is obtained at high purity and at high yield.
摘要翻译： 本文公开了通过在烃多元醇和酮羧酸之间形成酯以产生中间体多酮羧酸酯而获得的聚缩酮加成物。 可以通过结晶纯化中间体多酮羧酸酯以实现大于99.0％的纯度，然后缩醛化以产生可用于聚合物组合物中的聚缩酮加合物。 以高纯度和高收率获得聚缩酮加成物I.
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5.发明授权公开(公告)号：US09187598B2
公开(公告)日：2015-11-17
申请号：US13294854
申请日：2011-11-11
IPC分类号： C08G63/91 , C07D317/02 , C07D317/14 , C07D317/30 , C08G2/32 , C08G63/668 , C08G64/02 , C08G64/42 , C08L59/00 , C09D159/00 , C09D167/00 , C08G18/32 , C08L67/00 , C08G101/00
CPC分类号： C08K5/1565 , C07D317/02 , C07D317/14 , C07D317/30 , C08G2/32 , C08G18/3218 , C08G63/668 , C08G63/672 , C08G63/91 , C08G64/0208 , C08G64/42 , C08G2101/0025 , C08L59/00 , C08L67/00 , C09D159/00 , C09D167/00 , Y02P20/582 , Y10T428/31507 , Y10T428/31786
摘要： Disclosed herein is a polyhydroxy ketal adduct obtained by the esterification of a hydrocarbon polyol by at least 1.5 equivalents of a ketocarboxy to produce an intermediate ketocarboxylic ester. The intermediate polyketocarboxylic ester is then ketalized to produce the polyhydroxyketal adduct, which can be used to provide a polymeric composition.
摘要翻译： 本文公开了通过烃多元醇通过至少1.5当量的酮羧基酯化以产生中间体酮羧酸酯而获得的多羟基缩酮加合物。 然后中间体多酮羧酸酯被缩醛化以产生可用于提供聚合物组合物的多羟基缩酮加合物。
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公开(公告)号：US09212176B2
公开(公告)日：2015-12-15
申请号：US13294690
申请日：2011-11-11
申请人： Brian D. Mullen , Marc D. Scholten , Tara J. Mullen , Cora M. Leibig , Vivek Badarinarayana , Matthew J. Tjosaas
发明人： Brian D. Mullen , Marc D. Scholten , Tara J. Mullen , Cora M. Leibig , Vivek Badarinarayana , Matthew J. Tjosaas
IPC分类号： C07D407/12 , C08K5/1565 , C08L79/08 , C08L77/00 , C08L59/02
CPC分类号： C07D407/12 , C08K5/1565 , C08L59/02 , C08L77/00 , C08L79/08 , Y02P20/582 , C08L27/06
摘要： Disclosed herein is a polyketal adduct obtained by forming an ester between a hydrocarbon polyol and a ketocarboxylic acid to produce an intermediate polyketocarboxylic ester. The intermediate polyketocarboxylic ester can be purified via crystallization to achieve purities of greater than 99.0% and then ketalized to produce the polyketal adduct, which can be used in polymer compositions. The polyketal adduct I is obtained at high purity and at high yield.
摘要翻译： 本文公开了通过在烃多元醇和酮羧酸之间形成酯以产生中间体多酮羧酸酯而获得的聚缩酮加成物。 可以通过结晶纯化中间体多酮羧酸酯以实现大于99.0％的纯度，然后缩醛化以产生可用于聚合物组合物中的聚缩酮加合物。 以高纯度和高收率获得聚缩酮加成物I.
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公开(公告)号：US08969559B2
公开(公告)日：2015-03-03
申请号：US13370860
申请日：2012-02-10
申请人： Sergey Selifonov , Adam E. Goetz , Marc D. Scholten , Ning Zhou
发明人： Sergey Selifonov , Adam E. Goetz , Marc D. Scholten , Ning Zhou
IPC分类号： C07D317/30 , C07D407/12 , C07D407/14 , C07D405/14
CPC分类号： C07D319/06 , C07D317/30
摘要： Disclosed herein are ketal amide compounds. The ketal amide compounds are synthesized by the reaction of ketal acids or ketal esters with amine functional compounds. Also disclosed are methodologies useful to make the ketal amide compounds. Also disclosed herein are formulations and articles containing the ketal amide compounds.
摘要翻译： 本文公开的是缩酮酰胺化合物。 缩酮酰胺化合物通过缩酮酸或缩酮与胺官能化合物的反应合成。 还公开了可用于制备缩酮酰胺化合物的方法。 本文还公开了含有缩酮酰胺化合物的制剂和制品。
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公开(公告)号：US20120122745A1
公开(公告)日：2012-05-17
申请号：US13333273
申请日：2011-12-21
IPC分类号： C10M169/04 , C07D317/30 , C07D319/06 , C08K5/1575 , C09K3/00 , C08L27/06 , C08L67/04 , C08L31/04 , C08L69/00 , C07D407/12 , C08K5/1565
CPC分类号： C07D407/12 , C07D317/30 , C08K5/1515 , C08K5/1565 , C08K5/1575 , C10M129/20 , C10M129/70 , C10M2207/044
摘要： Various esterified alkyl ketal ester or hydroxyalkyl ketal ester products are useful as components of organic polymer compositions. The ketal esters are produced in certain transesterifications between alkyl ketal esters and/or hydroxyalkyl ketal esters and polyols, aminoalcohols, polyamines and/or polycarboxylic acids. The products are excellent plasticizers for a variety of organic polymers, notable poly(vinyl chloride) plastisols. The products are also very good lubricants for many lubrication applications.
摘要翻译： 各种酯化的烷基缩酮酯或羟烷基缩酮酯产物可用作有机聚合物组合物的组分。 缩酮是在烷基缩酮酯和/或羟烷基缩酮酯和多元醇，氨基醇，多胺和/或多元羧酸之间的某些酯交换中产生的。 该产品是各种有机聚合物，着名的聚（氯乙烯）增塑溶胶的优异增塑剂。 该产品对于许多润滑应用也是非常好的润滑剂。
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