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    Hydroquinone ethers having juvenile hormone activity
    2.
    发明授权
    Hydroquinone ethers having juvenile hormone activity 失效
    具有幼体激素活性的对苯二酚醚

    公开(公告)号：US4356329A

    公开(公告)日：1982-10-26

    申请号：US198488

    申请日：1980-10-20

    Applicant: Franco Bettarini ,  Pietro Massardo ,  Paolo Piccardi ,  Angelo Longoni

    Inventor： Franco Bettarini ,  Pietro Massardo ,  Paolo Piccardi ,  Angelo Longoni

    IPC: A01N31/16 ,  C07C43/225 ,  C07C43/23 ,  C07C43/215

    CPC classification number: C07C43/225 ,  A01N31/16 ,  C07C43/23

    Abstract: There are disclosed two hydroquinone diethers having at least one acetylenic and halogen-substituted chain and exhibiting juvenile hormone and acaricide activity and which show unexpected activity on Tenebrio molitor and Tribolium confusum.The two hydroquinone ethers are obtained by:(a) reacting one mole of hydroquinone alkali metal salt with two moles of 1,5-dichloropent-4-yne, or equimolar quantities of an alkali metal salt of 4-phenoxy-phenol with 1,5-dichlorpent-4-yne; or(b) by reacting the hydroquinone alkali metal salt or the 4-phenoxy-phenol alkali metal salt with the indicated quantities of 1,1,1,5-tetrachloropentane and then dehydrohalogenating the condensation product with alkali metal carbonates or hydroxides in dimethylsulphoxide.

    Abstract translation: 公开了具有至少一个炔属和卤素取代链的两个氢醌二醚，并表现出幼体激素和杀螨剂的活性，并且对三烯氰菊酯和苦苣属植物显示出意想不到的活性。 通过以下方法获得两种对苯二酚醚：（a）使1摩尔氢醌碱金属盐与2摩尔1,5-二氯-4-戊烯或等摩尔量的4-苯氧基苯酚的碱金属盐与1摩尔 5-二氯戊-4-炔; 或（b）通过使氢醌碱金属盐或4-苯氧基苯酚碱金属盐与指定量的1,1,1,5-四氯戊烷反应，然后使缩合产物与二甲基亚砜中的碱金属碳酸盐或氢氧化物脱卤氢化。

    Benzoyl-ureas having insecticide activity
    5.
    发明授权
    Benzoyl-ureas having insecticide activity 失效
    具有杀虫活性的苯甲酰脲

    公开(公告)号：US4980376A

    公开(公告)日：1990-12-25

    申请号：US540464

    申请日：1990-06-19

    Applicant: Pietro Massardo ,  Paolo Piccardi ,  Franco Rama ,  Vincenzo Caprioli

    Inventor： Pietro Massardo ,  Paolo Piccardi ,  Franco Rama ,  Vincenzo Caprioli

    IPC: A01N47/34 ,  C07C67/00 ,  C07C239/00 ,  C07C273/18 ,  C07C275/54 ,  C07C313/00 ,  C07C319/20 ,  C07C323/44

    CPC classification number: C07C275/54 ,  A01N47/34

    Abstract: Compounds are disclosed having formula: ##STR1## wherein: R is Cl, F;R.sub.1 is H, Cl, F;R.sub.2 and R.sub.5, equal to or differing from each other, are H, halogen, alkyl C.sub.1 -C.sub.4 ;R.sub.3 and R.sub.4, equal to or differing from each other, are: H, halogen, alkyl, haloalkyl, alkoxy, haloalkoxy, alkenyl, haloalkenyl, alkenyloxy, haloalkenyloxy or alkynyl;Z is O, S or a group NR.sub.7, wherein R.sub.7 is alkyl C.sub.1 -C.sub.3 or H;Y is alkylene C.sub.2 -C.sub.4, haloethylene or haloethenyl;R.sub.6 is alkyl C.sub.1 -C.sub.4, haloalkyl C.sub.1 -C.sub.4, alkenyl C.sub.3 -C.sub.4, haloalkenyl C.sub.3 -C.sub.4, cycloalkyl C.sub.3 -C.sub.4, halocycloalkyl C.sub.3 -C.sub.4 or cycloalkenyl C.sub.3 -C.sub.4.The compounds having formula (I) are endowed with an elevated insecticide activity, which shows itself chiefly against insect larvae and eggs.

    Abstract translation: 公开了具有下式的化合物：其中：R是Cl，F; R1是H，Cl，F; R2和R5彼此相同或不同，为H，卤素，C1-C4烷基; R 3和R 4彼此相同或不同，为：H，卤素，烷基，卤代烷基，烷氧基，卤代烷氧基，烯基，卤代烯基，烯氧基，卤代烯氧基或炔基; Z是O，S或NR 7，其中R 7是烷基C 1 -C 3或H; Y是亚烷基C2-C4，卤代乙烯或卤代乙烯基; R6是烷基C1-C4，卤代烷基C1-C4，烯基C3-C4，卤代烯基C3-C4，环烷基C3-C4，卤代环烷基C3-C4或环烯基C3-C4。 具有式（I）的化合物具有升高的杀虫活性，其主要表现为抗昆虫幼虫和卵。

    Process for preparing 1,1-dihalo-1,2,2,2-tetrafluoroethanes
    6.
    发明授权
    Process for preparing 1,1-dihalo-1,2,2,2-tetrafluoroethanes 失效
    制备1,1二卤代-1,2,2,2-四氟乙烷的方法

    公开(公告)号：US4748284A

    公开(公告)日：1988-05-31

    申请号：US943898

    申请日：1986-12-19

    Applicant: Franco Gozzo ,  Nicola Troiani ,  Paolo Piccardi

    Inventor： Franco Gozzo ,  Nicola Troiani ,  Paolo Piccardi

    IPC: C07C19/075 ,  B01J31/00 ,  B01J31/22 ,  C07B61/00 ,  C07C17/00 ,  C07C17/358 ,  C07C19/08 ,  C07C19/12 ,  C07C19/14 ,  C07C67/00 ,  C07C17/20

    CPC classification number: C07C17/358

    Abstract: A process for preparing 1,1-dihalo-1,2,2,2-tetrafluoroethanes by isomerization of 1,2-dihalotetrafluoroethanes at their reflux temperature, by using, as a catalyst, the reaction product prepared "in situ" from an anhydrous aluminum halide with at least equimolecular amounts of the isomer, 1,1-dihalo-1,2,2,2-tetrafluoroethane in a medium consisting of 1,2-dihalotetrafluoroethane. The products find application as intermediates for pyrethroid insecticides.

    Abstract translation: 一种通过1,2-二卤代四氟乙烷在其回流温度下异构化制备1,1-二卤-1,2 -1,2,4-四氟乙烷的方法，通过使用“无规”原位制备的反应产物作为催化剂， 在由1,2-二卤四氟乙烷组成的介质中具有至少等摩尔量的异构体1,1-二卤代-1,2,2,2-四氟乙烷的卤化铝。 该产品适用于拟除虫菊酯杀虫剂的中间体。

    Pyrethroids
    8.
    发明授权
    Pyrethroids 失效
    拟除虫菊酯

    公开(公告)号：US4379163A

    公开(公告)日：1983-04-05

    申请号：US273541

    申请日：1981-06-15

    Applicant: Paolo Piccardi ,  Francesco Corda ,  Franco Gozzo ,  Augusto Menconi ,  Angelo Longoni

    Inventor： Paolo Piccardi ,  Francesco Corda ,  Franco Gozzo ,  Augusto Menconi ,  Angelo Longoni

    IPC: A01N53/00 ,  C07C61/40 ,  C07D307/45 ,  A01N43/08 ,  C07D307/54

    CPC classification number: C07D307/42 ,  A01N53/00 ,  C07C61/40

    Abstract: Pyrethroid type insecticides are described having the formula: ##STR1## wherein: R.sup.1 =H, CN, C.tbd.CHR.sup.2 =3-phenoxy, 3-benzyl, 4-allyl, 4-propargyl.R.sup.3 =H, alkyl bound to the heterocyclic ring in position 3 or 2;R.sup.4 =(in position 4 or 5 of the heterocyclic ring)=benzyl, benzoyl, phenoxy, allyl, propargyl;Y=O, SR.sup.5 and R.sup.6 =alkyl C.sub.1 -C.sub.3, or R.sup.5 and R.sup.6 together form an orthocondensed aromatic, heteroaromatic or aliphatic, saturated or unsaturated ring;R.sup.7 and R.sup.8 (equal to or different from each other)=H, halogen, CH.sub.3 ;R.sup.9 =phenyl, vinyl, vinyl substituted, phenoxy.Compounds of general formula I are endowed with a high insecticide and acaricide activity.

    Abstract translation: 描述了拟除虫菊酯型杀虫剂，具有下式：其中（I）（X = H，F，Cl，Br; Y = Cl，Br） + TR 其中 ：R1 = H，CN，C3BCH2 = 3-苯氧基，3-苄基，4-烯丙基，4-炔丙基。 R3 = H，与3或2位杂环结合的烷基; R4 =（杂环的4或5位）=苄基，苯甲酰基，苯氧基，烯丙基，炔丙基; Y = O，S R5和R6 =烷基C1-C3，或R5和R6一起形成正缩合的芳族，杂芳族或脂族饱和或不饱和环; R7和R8（彼此相同或不同）= H，卤素，CH 3; R9 =苯基，乙烯基，乙烯基取代的苯氧基。 通式I的化合物具有高杀虫剂和杀螨剂活性。

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