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    Method for preparing linear organopolysiloxanediols
    1.
    发明授权
    Method for preparing linear organopolysiloxanediols 失效
    线性有机聚硅氧烷二醇的制备方法

    公开(公告)号：US4762937A

    公开(公告)日：1988-08-09

    申请号：US82606

    申请日：1987-08-06

    申请人： Ralph Ottlinger ,  Rudolf Reitmeier

    发明人： Ralph Ottlinger ,  Rudolf Reitmeier

    IPC分类号： C08G77/06 ,  C08G77/16 ,  C07F7/08

    CPC分类号： C08G77/06 ,  C08G77/16

    摘要： Linear organopolysiloxanediols are prepared by continuously introducing cyclic organopolysiloxanes, water in an amount of at least 14 mols per gram atom of silicon contained in the cyclic organopolysiloxanes used and water-soluble acid into a recirculating reactor and thereafter separating the aqueous phase from the organopolysiloxanediols more or less immediately after the reaction mixture exits from the recirculating reactor.

    摘要翻译： 线性有机聚硅氧烷二醇通过将环状有机聚硅氧烷，所用环状有机聚硅氧烷中所含的至少14摩尔/克原子的硅水溶液和水溶性酸连续引入循环反应器，然后将水相与有机聚硅氧烷二醇分离得更多或 反应混合物从循环反应器中排出后立即减少。

    Process for preparing alkylsilanes having bulky alkyl radicals
    4.
    发明授权
    Process for preparing alkylsilanes having bulky alkyl radicals 失效
    制备具有大体积烷基的烷基硅烷的方法

    公开(公告)号：US5663400A

    公开(公告)日：1997-09-02

    申请号：US611737

    申请日：1996-03-06

    申请人： Rudolf Reitmeier ,  Hermann Braunling ,  Tassilo Lindner ,  Hartmut Menzel

    发明人： Rudolf Reitmeier ,  Hermann Braunling ,  Tassilo Lindner ,  Hartmut Menzel

    IPC分类号： C07F7/18 ,  C07F7/12 ,  C07F7/14 ,  C07F7/08 ,  C07F7/10

    CPC分类号： C07F7/14

    摘要： Di- and trialkylsilanes of the formulaR.sub.a R.sup.1 R.sup.2.sub.b SiX.sub.c (I),which comprises reacting mono- and dialkylsilanes of the formulaR.sup.1 R.sup.2.sub.b SiH.sub.a X.sub.c (II),with alkenes A having at least 4 carbon atoms, which alkenes are unsubstituted or substituted by fluorine, chlorine or bromine atoms or cyano groups, in the presence of a transition metal catalyst and a hydrocarbon as activator, which hydrocarbon has at least one functional group selected from among aldehyde, keto and epoxy groups or halogen atoms, where in the above formulae (I) and (II),R is a branched or cyclic hydrocarbon radical having at least 4 carbon atoms, which radical is unsubstituted or substituted by fluorine, chlorine or bromine atoms or cyano groups,R.sup.1 is an alkyl radical having at least 2 carbon atoms, which radical is unsubstituted or substituted by fluorine, chlorine or bromine atoms or cyano groups,R.sup.2 is a hydrocarbon radical having at least 2 carbon atoms, which radical is unsubstituted or substituted by fluorine, chlorine, or bromine atoms or cyano groups,X is a fluorine, chlorine or bromine atom or an alkoxy radical having from 1 to 18 carbon atoms, which radical is unsubstituted or substituted by fluorine, chlorine or bromine atoms or cyano groups,a is 1 or 2,b is 0 or 1 andc is 1 or 2.

    摘要翻译： 包括式R 1 R 1 R 2 b Si X c（I）的二 - 和三烷基硅烷，其包括使式R 1 R 2 b SiHa X c（II）的单烷氧基硅烷和二烷基硅烷与具有至少4个碳原子的烯烃A反应，该烯烃是未取代的或被氟，氯或溴原子或氰基 在过渡金属催化剂和烃作为活化剂的存在下，该烃具有至少一个选自醛，酮和环氧基或卤素原子的官能团，其中在上式（I）和（II）中， R是具有至少4个碳原子的支链或环状烃基，该基团是未取代的或被氟，氯或溴原子或氰基取代，R 1是具有至少2个碳原子的烷基，该基团是未取代或取代的 通过氟，氯或溴原子或氰基，R 2是具有至少2个碳原子的烃基，该基团是未取代的或被氟，氯或溴取代 原子或氰基，X是氟，氯或溴原子或具有1至18个碳原子的烷氧基，该基团是未取代的或被氟，氯或溴原子或氰基取代的基团，a是1或2， b为0或1，c为1或2。

    Process for the continuous production of high-viscosity crosslinkable silicone compositions
    5.
    发明申请
    Process for the continuous production of high-viscosity crosslinkable silicone compositions 审中-公开
    连续生产高粘度可交联硅氧烷组合物的方法

    公开(公告)号：US20060247406A1

    公开(公告)日：2006-11-02

    申请号：US11410683

    申请日：2006-04-25

    申请人： Rudolf Reitmeier ,  Johann Schuster ,  Stephan Aigner ,  Alois Schlierf

    发明人： Rudolf Reitmeier ,  Johann Schuster ,  Stephan Aigner ,  Alois Schlierf

    IPC分类号： C08L83/04 ,  C08G77/06 ,  C08K3/00

    CPC分类号： B29B7/423 ,  B29B7/481 ,  B29B7/7466 ,  B29B7/7495 ,  B29C48/37 ,  B29C48/39 ,  C08G77/12 ,  C08G77/20 ,  C08L83/04 ,  C08L83/00

    摘要： A process for the continuous production of organopolysiloxane compositions which vulcanize at elevated temperature and have a viscosity of at least 500 Pa·s at 25° C., involves mixing and homogenizing high-viscosity organopolysiloxanes and crosslinking additives in a kneading cascade having at least two kneading chambers arranged in series proximate one another, containing two axially parallel kneading tools which can be driven in the same or opposite directions, and which are connected to one another by means of openings transverse to the axes of the kneading tools, with the first kneading chamber having a feed opening and the last kneading chamber having a discharge opening, and the temperature in the kneading chambers containing crosslinking additives being not more than 95° C.

    摘要翻译： 在高温下硫化并且在25℃下具有至少500Pa.s的粘度的连续生产有机聚硅氧烷组合物的方法包括将混合级联中的高粘度有机聚硅氧烷和交联添加剂混合并均化，所述捏合级联具有至少两个 捏合室彼此串联布置，包含两个可沿相同或相反方向驱动的轴向平行的捏合工具，并且通过横向于揉捏工具的轴线的开口彼此连接，第一次捏合 具有供给开口的腔室和具有排出口的最后一个捏合室，并且包含交联添加剂的捏合室中的温度不超过95℃。

    Process for the preparation of alkylsilanes with bulky alkyl radicals
    6.
    发明授权
    Process for the preparation of alkylsilanes with bulky alkyl radicals 有权
    用于制备具有大体积烷基的烷基硅烷的方法

    公开(公告)号：US06169196A

    公开(公告)日：2001-01-02

    申请号：US09493396

    申请日：2000-01-28

    申请人： Gilbert Geisberger ,  Tassilo Lindner ,  Rudolf Reitmeier

    发明人： Gilbert Geisberger ,  Tassilo Lindner ,  Rudolf Reitmeier

    IPC分类号： C07F708

    CPC分类号： C07F7/14

    摘要： A process for the preparation of di- and trialkylsilanes of the general formula (I) RaR1bSiXc  (I), in which mono- or dialkylsilanes of the general formula (II) R1bSiHaXc  (II) are reacted with alkenes A which have at least 3 carbon atoms and are optionally substituted by fluorine, chlorine or bromine atoms or cyano groups, in the presence of a transition metal catalyst and a trihalogenosilane of the general formula (III) R2SiY3  (III) as an activator, wherein, in the above general formulae (I) to (III), R is a branched or cyclic hydrocarbon radical having at least 3 carbon atoms, optionally substituted by fluorine, chlorine, or bromine, or cyano groups, R1 is an alkyl radical optionally substituted by fluorine, chlorine, or bromine, or cyano groups, R2 is a hydrogen atom, or an alkyl radical optionally substituted by fluorine, chlorine, or bromine, or cyano groups, X is fluorine, chlorine, or bromine, or an alkoxy radical having 1 to 18 carbon atoms optionally substituted by fluorine, chlorine, or bromine, or cyano groups, Y is fluorine, chlorine or bromine, a is 1 or 2, b is 1 or 2, and c is 1 or 2.

    摘要翻译： 制备通式（I）的二 - 和三烷基硅烷的方法，其中通式（II）的单 - 或二烷基硅烷与具有至少3个碳原子且任选被氟，氯或氯原子取代的烯烃A反应 溴原子或氰基，在过渡金属催化剂和通式（III）的三卤代硅烷的存在下作为活化剂，其中在上述通式（I）至（III）中，R是支链或环状烃 具有至少3个碳原子的基团，任选被氟，氯或溴或氰基取代，R 1是任选被氟，氯或溴或氰基取代的烷基，R 2是氢原子或烷基 任选被氟，氯或溴或氰基取代的基团，X是氟，氯或溴，或具有任选被氟，氯或溴或氰基取代的具有1至18个碳原子的烷氧基，Y是 氟，c 芴或溴，a为1或2，b为1或2，c为1或2。