Plasma resistant multi-layer architecture for high aspect ratio parts

    公开(公告)号:US10858741B2

    公开(公告)日:2020-12-08

    申请号:US16298964

    申请日:2019-03-11

    摘要: Disclosed herein is an article comprising one or more channels and a multi-layer protective coating on the one or more channels. The multi-layer protective coating includes an anodization layer comprising a plurality of cracks and a plurality of pores, a sealing layer on the anodization layer, and a top layer on the sealing layer. The sealing layer comprises a metal oxide, the seals the plurality of cracks and the plurality of pores, and has a porosity of approximately 0%. The top layer comprises a rare earth oxide, a rare earth fluoride, or a rare earth oxyfluoride, has a different material composition than the sealing layer, and has a porosity of approximately 0%.

    PLASMA RESISTANT MULTI-LAYER ARCHITECTURE FOR HIGH ASPECT RATIO PARTS

    公开(公告)号:US20200291528A1

    公开(公告)日:2020-09-17

    申请号:US16298964

    申请日:2019-03-11

    IPC分类号: C23C28/04

    摘要: Disclosed herein is an article comprising one or more channels and a multi-layer protective coating on the one or more channels. The multi-layer protective coating includes an anodization layer comprising a plurality of cracks and a plurality of pores, a sealing layer on the anodization layer, and a top layer on the sealing layer. The sealing layer comprises a metal oxide, the seals the plurality of cracks and the plurality of pores, and has a porosity of approximately 0%. The top layer comprises a rare earth oxide, a rare earth fluoride, or a rare earth oxyfluoride, has a different material composition than the sealing layer, and has a porosity of approximately 0%.

    MULTI-LAYER PLASMA EROSION PROTECTION FOR CHAMBER COMPONENTS

    公开(公告)号:US20180330923A1

    公开(公告)日:2018-11-15

    申请号:US15965794

    申请日:2018-04-27

    IPC分类号: H01J37/32 C23C16/40

    摘要: A method of applying a multi-layer plasma resistant coating on an article comprises performing plating or ALD to form a conformal first plasma resistant layer on an article, wherein the conformal first plasma resistant layer is formed on a surface of the article and on walls of high aspect ratio features in the article. The conformal first plasma resistant coating has a porosity of approximately 0% and a thickness of approximately 200 nm to approximately 1 micron. One of electron beam ion assisted deposition (EB-IAD), plasma enhanced chemical vapor deposition (PECVD), aerosol deposition or plasma spraying is then performed to form a second plasma resistant layer that covers the conformal first plasma resistant layer at a region of the surface but not at the walls of the high aspect ratio features.