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    EXTREME DURABILITY COMPOSITE DIAMOND FILM
    2.
    发明申请
    EXTREME DURABILITY COMPOSITE DIAMOND FILM 审中-公开
    极致耐久性复合金刚石膜

    公开(公告)号：US20160348236A1

    公开(公告)日：2016-12-01

    申请号：US15167363

    申请日：2016-05-27

    申请人： Advanced Diamond Technologies, Inc.

    发明人： Hongjun Zeng ,  John Arthur Carlisle ,  Ian Wakefield Wylie

    IPC分类号： C23C16/27 ,  C04B41/45 ,  C04B41/87 ,  C04B41/50 ,  C23C16/50 ,  C04B35/52

    摘要： A novel composite diamond film comprising of a relatively thick layer of UNCD (Ultrananocrystalline Diamond) with a Young's modulus of less than 900 GPa and an underlying relatively thin MCD (microcrystalline diamond) layer with a Young's modulus of greater than 900 GPa, has been shown to exhibit superior delamination resistance under extreme shear stress. It is hypothesized that this improvement is due to a combination of stress relief by the composite film with a slightly “softer” UNCD layer, a disruption of the fracture mechanism through the composite layer(s), and the near ideal chemical and thermal expansion coefficient match between the two diamond layers. The combination of a thick but “softer” underlying UNCD layer with a thin but harder overlying MCD layer provides an excellent compromise between the low deposition cost and smoothness of UNCD with the extreme hardness and unparalleled chemical, electrochemical and immunological inertness of even a thin layer of MCD. The MCD layer's roughness is minimized and its adhesion maximized by the use of a thin layer of MCD and its deposition on the smooth surface of the chemically nearly identical underlying UNCD layer. The composite film can be applied to any application currently utilizing a diamond or a similar hard film, including cutting tools, abrasive surfaces, electrochemistry, biomedical applications such as human implants or thermally conductive films and the like, requiring superior durability, chemical resistance and/or immunological inertness.

    摘要翻译： 已经示出了由杨氏模量小于900GPa的相对较厚的UNCD层（Ultrananocrystalline Diamond）和具有大于900GPa的杨氏模量的相对薄的MCD（微晶金刚石）层组成的新型复合金刚石薄膜。 在极端剪切应力下表现出优异的耐分层性。 假设这种改进是由于复合膜与轻微“较软”的UNCD层的应力释放的组合，通过复合层的断裂机理的破坏以及接近理想的化学和热膨胀系数 两颗钻石层之间的匹配。 厚厚但“较软”的底层UNCD层与薄但较硬的覆盖MCD层的组合在UNCD的低沉积成本和平滑度之间提供了极好的折中，具有极高的硬度和无与伦比的化学，电化学和免疫惰性甚至薄层 的MCD。 MCD层的粗糙度被最小化，并且其粘附通过使用MCD的薄层及其沉积在化学上几乎相同的底层UNCD层的光滑表面上而最大化。 复合膜可以应用于目前使用金刚石或类似硬膜的任何应用，包括切割工具，磨料表面，电化学，生物医学应用如人造植物或导热膜等，需要优异的耐久性，耐化学性和/ 或免疫惰性。

    RECYCLING LOOP METHOD FOR PREPARATION OF HIGH CONCENTRATION OZONE
    4.
    发明申请
    RECYCLING LOOP METHOD FOR PREPARATION OF HIGH CONCENTRATION OZONE 审中-公开
    回收循环方法制备高浓度臭氧

    公开(公告)号：US20160347629A1

    公开(公告)日：2016-12-01

    申请号：US15167389

    申请日：2016-05-27

    申请人： Advanced Diamond Technologies, Inc.

    发明人： Donato M. Ceres ,  John Arthur Carlisle ,  Prabhu Arumugam ,  Matthew Hart

    IPC分类号： C02F1/467 ,  C25B1/13 ,  C25B15/08 ,  C02F1/461

    CPC分类号： C02F1/4672 ,  C02F1/46104 ,  C02F1/46109 ,  C02F2001/46133 ,  C02F2001/46147 ,  C02F2001/46185 ,  C02F2201/46115 ,  C02F2305/023 ,  C25B1/13 ,  C25B15/08

    摘要： The present invention relates to an apparatus for the production of ozone from water comprising at least one cell, consisting of an anode, a cathode and an interposed cation-conducting membrane, wherein the membrane conductively connects the anode and the cathode while forming flow channels for water that are separated from one another as anode and cathode chambers and wherein the flow channels are configured to allow for the recirculation of the water flow within the chambers. The present invention further relates to an electrochemical method and apparatus for producing ozone or dissolved ozone in water in high concentrations by mean of recirculation of water between at least one chamber and at least one water tank.

    摘要翻译： 本发明涉及一种用于从水中生产臭氧的装置，包括由阳极，阴极和插入的阳离子导电膜组成的至少一个电池，其中膜导电地连接阳极和阴极，同时形成用于 作为阳极和阴极室彼此分离的水，并且其中流动通道被配置为允许在室内的水流的再循环。 本发明还涉及通过在至少一个室和至少一个水箱之间再循环水来以高浓度产生臭氧或溶解的臭氧在水中的电化学方法和装置。

    Recycling loop method for preparation of high concentration ozone
    6.
    发明授权
    Recycling loop method for preparation of high concentration ozone 有权

    公开(公告)号：US10239772B2

    公开(公告)日：2019-03-26

    申请号：US15167389

    申请日：2016-05-27

    申请人： Advanced Diamond Technologies, Inc.

    发明人： Donato M. Ceres ,  John Arthur Carlisle ,  Prabhu Arumugam ,  Matthew Hart

    IPC分类号： C25B1/13 ,  C02F1/461 ,  C02F1/467 ,  C25B15/08

    摘要： The present invention relates to an apparatus for the production of ozone from water comprising at least one cell, consisting of an anode, a cathode and an interposed cation-conducting membrane, wherein the membrane conductively connects the anode and the cathode while forming flow channels for water that are separated from one another as anode and cathode chambers and wherein the flow channels are configured to allow for the recirculation of the water flow within the chambers. The present invention further relates to an electrochemical method and apparatus for producing ozone or dissolved ozone in water in high concentrations by mean of recirculation of water between at least one chamber and at least one water tank.

    METHOD OF DETERMINING THE CONCENTRATION OF PATHOGENS OR OXIDIZABLE ORGANIC COMPOUNDS USING AN OZONE TITRATION SENSOR
    7.
    发明申请
    METHOD OF DETERMINING THE CONCENTRATION OF PATHOGENS OR OXIDIZABLE ORGANIC COMPOUNDS USING AN OZONE TITRATION SENSOR 审中-公开
    使用臭氧浓度传感器测定病原体或可氧化有机化合物浓度的方法

    公开(公告)号：US20160369318A1

    公开(公告)日：2016-12-22

    申请号：US15189380

    申请日：2016-06-22

    申请人： Advanced Diamond Technologies, Inc.

    发明人： John Arthur Carlisle ,  Donato M. Ceres ,  John Wagner ,  John d. Yerger, III

    IPC分类号： C12Q1/04 ,  G01N31/16

    CPC分类号： C12Q1/04 ,  C12Q1/06 ,  C12Q2304/20 ,  C12Q2304/80 ,  G01N31/005

    摘要： The invention describes a method of ozone titration sensing which utilizes an ozone addition to a target solution, detection of ozone using an Oxidation-Reduction Potential (ORP) electrode or an Ultraviolet (UV) absorption photodiode or other means to detect ozone and the determination of the relative concentration of organics or pathogens subject to ozone oxidation which are present in the target solution. The inventive sensing method can be usefully employed to determine the relative concentration of pathogens such as viruses, bacteria and/or parasites that are readily oxidizable by ozone in aqueous solutions. The inventive sensing method may be used to control an ozone (or other oxidizing or disinfecting) compound dispensing system to optimize the dosage of ozone (or other disinfecting compound) necessary to produce a desired kill ratio or to generate a desired residual of ozone concentration in an aqueous solution after pathogen disinfection.

    摘要翻译： 本发明描述了一种利用臭氧添加到目标溶液中的臭氧滴定检测方法，使用氧化还原电位（ORP）电极或紫外线（UV）吸收光电二极管或其他检测臭氧的方法检测臭氧， 存在于目标溶液中的受臭氧氧化的有机物或病原体的相对浓度。 本发明的感测方法可有效地用于确定在水溶液中容易被臭氧氧化的病毒，细菌和/或寄生虫等病原体的相对浓度。 本发明的感测方法可用于控制臭氧（或其它氧化或消毒）化合物分配系统，以优化产生所需杀死率所需的臭氧（或其它消毒化合物）的剂量或产生期望的臭氧浓度残留量 病原体消毒后的水溶液。

    Extreme durability composite diamond electrodes
    8.
    发明授权
    Extreme durability composite diamond electrodes 有权

    公开(公告)号：US10907264B2

    公开(公告)日：2021-02-02

    申请号：US15179337

    申请日：2016-06-10

    申请人： Advanced Diamond Technologies, Inc.

    发明人： Hongjun Zeng ,  John Arthur Carlisle ,  Ian Wakefield Wylie

    IPC分类号： C25B11/12 ,  C25B11/04 ,  C25B1/13 ,  C25B1/26 ,  C25B1/28 ,  C25B1/02

    摘要： A durable composite diamond electrode is disclosed which comprise at least a relatively thicker conductive UNCD (Ultrananocrystalline Diamond) layer, with low deposition cost, on a substrate underlying a relatively thinner conductive MCD (Microcrystalline Diamond) layer. The electrode exhibits long life and superior delamination resistance under extremely stressed electrochemical oxidation conditions. It is hypothesized that this improvement in electrode reliability is due to a combination of stress relief by the composite film with the slightly “softer” underlying UNCD “root” layer and the electrochemically durable overlying MCD “shield” layer, an effective disruption mechanism of the fracture propagation between the compositing layers, and thermal expansion coefficient match between the diamond layers and the substrate. The diamond composite electrode can be applied to any electrochemical application requiring extreme voltages/current densities, extreme reliability or biomedical inertness such as electrochemical systems to generate ozone, hydroxyl radicals, or biomedical electrode applications.

    Extreme durability composite diamond film
    9.
    发明授权
    Extreme durability composite diamond film 有权

    公开(公告)号：US10662523B2

    公开(公告)日：2020-05-26

    申请号：US15167363

    申请日：2016-05-27

    申请人： Advanced Diamond Technologies, Inc.

    发明人： Hongjun Zeng ,  John Arthur Carlisle ,  Ian Wakefield Wylie

    IPC分类号： C04B35/52 ,  C23C16/27 ,  C23C16/50 ,  C04B35/622 ,  C04B35/528 ,  B32B18/00

    摘要： A novel composite diamond film comprising of a relatively thick layer of UNCD (Ultrananocrystalline Diamond) with a Young's modulus of less than 900 GPa and a relatively thin MCD (microcrystalline diamond) outermost layer with a Young's modulus of greater than 900 GPa, has been shown to exhibit superior delamination resistance under extreme shear stress. It is hypothesized that this improvement is due to a combination of stress relief by the composite film with a slightly “softer” UNCD layer, a disruption of the fracture mechanism through the composite layer(s), and the near ideal chemical and thermal expansion coefficient match between the two diamond layers. The combination of a thick but “softer” underlying UNCD layer with a thin but harder overlying MCD layer provides an excellent compromise between the low deposition cost and smoothness of UNCD with the extreme hardness and unparalleled chemical, electrochemical and immunological inertness of even a thin layer of MCD. The MCD layer's roughness is minimized and its adhesion maximized by the use of a thin layer of MCD and its deposition on the smooth surface of the chemically nearly identical underlying UNCD layer. The composite film can be applied to any application currently utilizing a diamond or a similar hard film, including cutting tools, abrasive surfaces, electrochemistry, biomedical applications such as human implants or thermally conductive films and the like, requiring superior durability, chemical resistance and/or immunological inertness.