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    Method for the manufacture of electrode for energy-storage devices
    1.
    发明授权
    Method for the manufacture of electrode for energy-storage devices 有权
    用于制造储能装置的电极的方法

    公开(公告)号：US07563354B2

    公开(公告)日：2009-07-21

    申请号：US11088509

    申请日：2005-03-24

    申请人： Alexander Mikhailovich Timonov ,  Sergey Anatolijevich Logvinov ,  Dmitriy Ivanovich Pivunov ,  Svetlana Viktorovna Vasiljeva ,  Nik Shkolnik ,  Sam Kogan

    发明人： Alexander Mikhailovich Timonov ,  Sergey Anatolijevich Logvinov ,  Dmitriy Ivanovich Pivunov ,  Svetlana Viktorovna Vasiljeva ,  Nik Shkolnik ,  Sam Kogan

    IPC分类号： C25D9/00

    CPC分类号： H01M4/0438 ,  C08G12/06 ,  H01G9/0036 ,  H01G9/155 ,  H01M4/0452 ,  H01M4/0466 ,  H01M4/137 ,  H01M4/606 ,  Y02E60/13

    摘要： Application of a redox polymer of the poly-[Me(R-Salen)] type onto a conducting substrate is accomplished by the method of electrochemical polymerization. Said polymerization is accomplished by supplying a voltage between the substrate (that serves as an anode) and a counter electrode (that serves as a cathode), with both of them being submerged into the electrolyte containing an organic solvent and the compounds capable of dissolving in said solvent. The process is accompanied by the production of electrochemically inactive (at concentrations of no less than 0.01 mol/l) ions within the range of potentials from −3.0 V to +1.5 V, and metal complex [Me(R-Salen)] dissolved at a concentration of no less than 5-10−5 mol/l, (where: Me is a transition metal having at least two different degrees of oxidation, R is an electron-donating substituent, Salen is a residue of bis-(salicylaldehyde)-ethylenediamine in Schiff's base.

    摘要翻译： 聚 - [Me（R-Salen）]型氧化还原聚合物在导电基材上的应用是通过电化学聚合的方法实现的。 所述聚合是通过在衬底（用作阳极）和对电极（用作阴极）之间提供电压来实现的，两者都被浸没在含有机溶剂的电解质中，并且能够溶解在 所述溶剂。 该过程伴随着在-3.0V至+1.5V的电位范围内产生电化学惰性的（浓度不小于0.01mol / l）的离子，并且溶解在金属络合物[Me（R-Salen） 浓度不小于5-10-5mol / l（其中：Me是具有至少两个不同氧化程度的过渡金属，R是给电子取代基，Salen是双 - （水杨醛）的残基， 乙二胺在希夫的基地。

    Electrochemical capacitor and method of use
    2.
    发明授权
    Electrochemical capacitor and method of use 有权
    电化学电容器及其使用方法

    公开(公告)号：US07292431B2

    公开(公告)日：2007-11-06

    申请号：US11098698

    申请日：2005-04-04

    申请人： Alexander Mikhailovich Timonov ,  Sergey Anatolijevich Logvinov ,  Dmitriy Ivanovich Pivunov ,  Svetlana Viktorovna Vasiljeva ,  Nik Shkolnik ,  Sam Kogan

    发明人： Alexander Mikhailovich Timonov ,  Sergey Anatolijevich Logvinov ,  Dmitriy Ivanovich Pivunov ,  Svetlana Viktorovna Vasiljeva ,  Nik Shkolnik ,  Sam Kogan

    IPC分类号： H01G9/00

    CPC分类号： H01M4/602 ,  H01G9/042 ,  H01G9/22 ,  H01G11/02 ,  H01G11/26 ,  H01G11/32 ,  H01G11/48 ,  Y02E60/13 ,  Y10T29/417

    摘要： The invention is an electrochemical capacitor with its electrodes made on a conducting substrate with a layer of a redox polymer of the poly[Me(R-Salen)] type deposited onto the substrate. Me is a transition metal (for example, Ni, Pd, Co, Cu, Fe), R is an electron-donating substituent (for example, CH3O—, C2H5O—, HO—, —CH3), Salen is a residue of bis(salicylaldehyde)-ethylendiamine in Schiff's base. The electrolyte comprises of an organic solvent, compounds capable of dissolving in such solvents with the resulting concentration of no less than 0.01 mol/l and dissociating with the formation of ions, which are electrochemically inactive within the range of potentials from −3.0 V to +1.5 V (for example, salts of tetramethyl ammonium, tetrapropyl ammonium, tetrabutyl ammonium), and a dissolved metal complex [Me(R-Salen)]. The method of using the capacitor contemplates periodically alternating the connection polarity of the electrodes, causing the electrochemical characteristics of the electrodes to regenerate.

    摘要翻译： 本发明是一种电化学电容器，其电极在导电衬底上制成，其上沉积有一层聚[Me（R-Salen）]型氧化还原聚合物。 Me是过渡金属（例如Ni，Pd，Co，Cu，Fe），R是给电子取代基（例如CH 3 O，C 2， H 2 O-，HO-，-CH 3 3），Salen是席夫碱中双（水杨醛） - 乙二胺的残基。 电解质包括有机溶剂，能够溶解在这样的溶剂中的化合物，所得到的浓度不低于0.01mol / l，并​​且在电位从-3.0V到+ 1.5V（例如，四甲基铵，四丙基铵，四丁基铵的盐）和溶解的金属络合物[Me（R-Salen）]。 使用电容器的方法考虑周期性地交替电极的连接极性，导致电极的电化学特性再生。

    Method for the manufacture of electrode for energy-storage devices
    5.
    发明申请
    Method for the manufacture of electrode for energy-storage devices 有权
    用于制造储能装置的电极的方法

    公开(公告)号：US20050217998A1

    公开(公告)日：2005-10-06

    申请号：US11088509

    申请日：2005-03-24

    申请人： Alexander Timonov ,  Sergey Logvinov ,  Dmitriy Pivunov ,  Svetlana Vasiljeva ,  Nik Shkolnik ,  Sam Kogan

    发明人： Alexander Timonov ,  Sergey Logvinov ,  Dmitriy Pivunov ,  Svetlana Vasiljeva ,  Nik Shkolnik ,  Sam Kogan

    IPC分类号： H01G9/04 ,  H01G9/155 ,  H01M4/137 ,  H01M4/60 ,  H01M4/04

    CPC分类号： H01M4/0438 ,  C08G12/06 ,  H01G9/0036 ,  H01G9/155 ,  H01M4/0452 ,  H01M4/0466 ,  H01M4/137 ,  H01M4/606 ,  Y02E60/13

    摘要： Application of a redox polymer of the poly-[Me(R-Salen)] type onto a conducting substrate is accomplished by the method of electrochemical polymerization. Said polymerization is accomplished by supplying a voltage between the substrate (that serves as an anode) and a counter electrode (that serves as a cathode), with both of them being submerged into the electrolyte containing an organic solvent and the compounds capable of dissolving in said solvent. The process is accompanied by the production of electrochemically inactive (at concentrations of no less than 0.01 mol/l) ions within the range of potentials from −3.0 V to +1.5 V, and metal complex [Me(R-Salen)] dissolved at a concentration of no less than 5·10−5 mol/l, (where: Me is a transition metal having at least two different degrees of oxidation, R is an electron-donating substituent, Salen is a residue of bis-(salicylaldehyde)-ethylenediamine in Schiff's base.

    摘要翻译： 聚 - [Me（R-Salen）]型氧化还原聚合物在导电基材上的应用是通过电化学聚合的方法实现的。 所述聚合是通过在衬底（用作阳极）和对电极（用作阴极）之间提供电压来实现的，两者都被浸没在含有机溶剂的电解质中，并且能够溶解在 所述溶剂。 该过程伴随着在-3.0V至+1.5V的电位范围内产生电化学惰性的（浓度不小于0.01mol / l）的离子，并且溶解在金属络合物[Me（R-Salen） 浓度不低于5.10〜5mol / l，（其中：Me是具有至少两个不同氧化程度的过渡金属，R是给电子取代基，Salen是 双（水杨醛） - 乙二胺在希夫碱。

    Electrochemical capacitor and method of use
    6.
    发明申请
    Electrochemical capacitor and method of use 有权
    电化学电容器及其使用方法

    公开(公告)号：US20050225928A1

    公开(公告)日：2005-10-13

    申请号：US11098698

    申请日：2005-04-04

    申请人： Alexander Timonov ,  Sergey Logvinov ,  Dmitriy Pivunov ,  Svetlana Vasiljeva ,  Nik Shkolnik ,  Sam Kogan

    发明人： Alexander Timonov ,  Sergey Logvinov ,  Dmitriy Pivunov ,  Svetlana Vasiljeva ,  Nik Shkolnik ,  Sam Kogan

    IPC分类号： H01G9/00 ,  H01G9/022 ,  H01G9/04 ,  H01G9/042 ,  H01G9/22 ,  H01M4/04 ,  H01M4/60

    CPC分类号： H01M4/602 ,  H01G9/042 ,  H01G9/22 ,  H01G11/02 ,  H01G11/26 ,  H01G11/32 ,  H01G11/48 ,  Y02E60/13 ,  Y10T29/417

    摘要： The invention is an electrochemical capacitor with its electrodes made on a conducting substrate with a layer of a redox polymer of the poly[Me(R-Salen)] type deposited onto the substrate. Me is a transition metal (for example, Ni, Pd, Co, Cu, Fe), R is an electron-donating substituent (for example, CH3O—, C2H5O—, HO—, —CH3), Salen is a residue of bis(salicylaldehyde)-ethylendiamine in Schiff's base. The electrolyte comprises of an organic solvent, compounds capable of dissolving in such solvents with the resulting concentration of no less than 0.01 mol/l and dissociating with the formation of ions, which are electrochemically inactive within the range of potentials from −3.0 V to +1.5 V (for example, salts of tetramethyl ammonium, tetrapropyl ammonium, tetrabutyl ammonium), and a dissolved metal complex [Me(R-Salen)]. The method of using the capacitor contemplates periodically alternating the connection polarity of the electrodes, causing the electrochemical characteristics of the electrodes to regenerate.

    摘要翻译： 本发明是一种电化学电容器，其电极在导电衬底上制成，其上沉积有一层聚[Me（R-Salen）]型氧化还原聚合物。 Me是过渡金属（例如Ni，Pd，Co，Cu，Fe），R是给电子取代基（例如CH 3 O，C 2， H 2 O-，HO-，-CH 3 3），Salen是席夫碱中双（水杨醛） - 乙二胺的残基。 电解质包括有机溶剂，能够溶解在这样的溶剂中的化合物，所得到的浓度不低于0.01mol / l，并​​且在电位从-3.0V到+ 1.5V（例如四甲基铵，四丙基铵，四丁基铵的盐）和溶解的金属络合物[Me（R-Salen）]。 使用电容器的方法考虑周期性地交替电极的连接极性，导致电极的电化学特性再生。

    Method for Producing Electrode Material
    8.
    发明申请
    Method for Producing Electrode Material 审中-公开
    生产电极材料的方法

    公开(公告)号：US20080213500A1

    公开(公告)日：2008-09-04

    申请号：US11664286

    申请日：2004-09-30

    申请人： Hidenori Uchi ,  Kenji Tamamitsu ,  Satori Tsumeda ,  Alexander M. Timonov ,  Sergey Nikolay Shkolnik ,  Sam Kogan

    发明人： Hidenori Uchi ,  Kenji Tamamitsu ,  Satori Tsumeda ,  Alexander M. Timonov ,  Sergey Nikolay Shkolnik ,  Sam Kogan

    IPC分类号： C08F2/58

    CPC分类号： H01G9/155 ,  H01M4/0438 ,  H01M4/0452 ,  H01M4/0466 ,  H01M4/137 ,  H01M4/1399 ,  H01M4/602 ,  H01M10/0525 ,  Y02E60/13 ,  Y02T10/7022

    摘要： To provide a method for producing an electrode material which is improved in energy density and is excellent in output characteristics. The present invention provides a manufacturing method for the electrode material comprising the steps of: 1) immersing a conductive material having a specific surface area of 200 to 3000 m2g−1 in a complex monomer solution of a transition metal having at least two different oxidation numbers, 2) performing electro polymerization by applying pulse voltage using the conductive material as an electrode to stack the complex monomer under the condition that electrolyzation time is 0.1 to 60 second and a downtime is 10 to 600 second, and 3) forming on the surface of the conductive material an energy accumulating redox polymer layer containing polymer complex compound of transition metal formed by the stacked complex monomer, thereby accumulating energy via a redox reaction: wherein a thin and uniform electrode film is formed, namely the electrode material which is excellent in output characteristics and improves energy density is manufactured according to the method.

    摘要翻译： 提供能够提高能量密度且输出特性优异的电极材料的制造方法。 本发明提供一种电极材料的制造方法，包括以下步骤：1）将比表面积为200〜3000μm2〜 在具有至少两个不同氧化数的过渡金属的复合单体溶液中，2）通过使用导电材料作为电极施加脉冲电压来进行电聚合，以在电解时间为0.1至60秒的条件下堆叠复合单体，以及 停机时间为10〜600秒，3）在导电材料的表面上形成能量积聚的氧化还原聚合物层，其含有由层叠的复合单体形成的过渡金属的聚合物络合物，由此通过氧化还原反应积累能量：其中薄 形成均匀的电极膜，即根据该方法制造输出特性优异，能量密度提高的电极材料。

    Method for manufacturing an energy storage device
    10.
    发明授权
    Method for manufacturing an energy storage device 有权
    储能装置的制造方法

    公开(公告)号：US07888229B2

    公开(公告)日：2011-02-15

    申请号：US11726985

    申请日：2007-03-23

    申请人： Irina Chepurnaya ,  Alexander Timonov ,  Sergey Logvinov ,  Sam Kogan

    发明人： Irina Chepurnaya ,  Alexander Timonov ,  Sergey Logvinov ,  Sam Kogan

    IPC分类号： H01L21/20

    CPC分类号： H01G9/155 ,  H01G9/038 ,  H01G9/058 ,  H01G9/15 ,  H01G11/02 ,  H01G11/24 ,  H01G11/26 ,  H01G11/58 ,  Y02E60/13 ,  Y10T29/417

    摘要： The present invention relates to methods of manufacturing an electrochemical energy storage device, such as a hybrid capacitor. The method comprises saturating a porous electrically conductive material in a solution comprising an organic solvent and a metal complex or a mixture of metal complexes; assembling a capacitor comprising the positive electrode made of porous electrically conductive material saturated with a metal complex, a negative electrode, and a separator in a casing; introducing the electrolyte solution into the casing; sealing the casing; and subsequent charge-discharge cycling of the capacitor. The charge-discharge cycling deposits a layer of an energy-accumulating redox polymer on the positive electrode. The electrolyte solution for filling the hybrid capacitor contains an organic solvent, a metal complex, and substances soluble to a concentration of no less than 0.01 mol/L and containing ions that are electrochemically inactive within the range of potentials between −3.0 V to +1.5 V.

    摘要翻译： 本发明涉及电化学储能装置如混合电容器的制造方法。 该方法包括在包含有机溶剂和金属络合物或金属络合物的混合物的溶液中饱和多孔导电材料; 组装一个电容器，该电容器包括由壳体中的金属络合物，负极和隔板饱和的多孔导电材料制成的正电极; 将电解质溶液引入壳体中; 密封套管; 以及随后的电容器的充放电循环。 充电 - 放电循环在正电极上沉积一层能量聚集的氧化还原聚合物。 用于填充混合电容器的电解液包含有机溶剂，金属络合物和可溶于0.01mol / L浓度的物质，并且在-3.0V至+1.5之间的电势范围内含有电化学惰性的离子 五