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    Compositions for protecting plants against disease
    3.
    发明授权
    Compositions for protecting plants against disease 失效

    公开(公告)号：US4980355A

    公开(公告)日：1990-12-25

    申请号：US319017

    申请日：1989-03-03

    申请人： Helmut Zondler ,  Alfred Meyer ,  Wolfgang Eckhardt ,  Walter Kunz

    发明人： Helmut Zondler ,  Alfred Meyer ,  Wolfgang Eckhardt ,  Walter Kunz

    IPC分类号： A01N43/40 ,  A01N43/50 ,  A01N43/54 ,  A01N43/58 ,  A01N43/60 ,  A01N43/653 ,  C07D213/81 ,  C07D401/06 ,  C07D401/12 ,  C07D401/14 ,  C07D413/14

    CPC分类号： C07D213/81 ,  A01N43/40 ,  A01N43/50 ,  A01N43/54 ,  A01N43/58 ,  A01N43/60 ,  A01N43/653 ,  C07D401/06 ,  C07D401/12 ,  C07D401/14

    摘要： Novel substituted isonicotinic acid amides of the general formula ##STR1## in which X in ortho/ortho'-position are equal and represent fluorine, chlorine, bromine or iodine;Q.sub.1 is unsubstituted pyridimin-4-yl, or pyrimidin-4-yl substituted by R.sub.1, R.sub.2 and R.sub.3 ;Q.sub.2 is unsubstituted pyrimidin-2-yl, or pyrimidin-2-yl substituted by R.sub.1, R.sub.2 and R.sub.3 ;Q.sub.3 is unsubstituted pyrimidin-5-yl, or pyrimidin-5-yl substituted by R.sub.1, R.sub.2 and R.sub.3 ;Q.sub.4 is pyridin-2-yl, pyridin-3-yl or pyridin-4-yl each of which is unsubstituted or substituted by R.sub.1, R.sub.2 and R.sub.3 ;Q.sub.5 is pyridazin-3-yl or pyridazin-4-yl each of which is unsubstituted or substituted by R.sub.1, R.sub.2 and R.sub.3 ;Q.sub.6 is unsubstituted pyrazin-2-yl, or pyrazin-2-yl substituted by R.sub.1, R.sub.2 and R.sub.3 ;R.sub.1, R.sub.2, R.sub.3 are hydrogen, halogen, C.sub.1 -C.sub.6 alkyl, C.sub.1 -C.sub.6 haloalkyl having from 1 to 3 halogen atoms, C.sub.1 -C.sub.6 alkoxy, C.sub.2 -C.sub.6 alkoxyalkyl, C.sub.1 -C.sub.6 thioalkyl, C.sub.1 -C.sub.6 haloalkoxy having from 1 to 5 halogen atoms, C.sub.3 -C.sub.6 alkenyloxy, C.sub.3 -C.sub.6 alkynyloxy, C.sub.3 -C.sub.6 thioalkenyl, C.sub.3 -C.sub.6 cycloalkyl, C.sub.3 -C.sub.6 cycloalkyl substituted by methyl, or nitro, cyano, the radical CH(OR.sub.4).sub.2 or COOR.sub.4 in which R.sub.4 is C.sub.1 -C.sub.4 alkyl; also phenyl, phenoxy, thiophenyl, benzyl, benzyloxy or thiobenzyl; or phenyl, phenoxy, thiophenyl, benzyl, benzyloxy or thiobenzyl each substituted at least once by C.sub.1 -C.sub.3 alkyl, C.sub.1 -C.sub.3 -alkoxy, C.sub.1 -C.sub.3 haloalkyl having from 1 to 3 halogen atoms, halogen, nitro or by cyano; and also N(R.sub.5)R.sub.6 in which R.sub.5 and R.sub.6, independently of one another, are each C.sub.1 -C.sub.6 alkyl; and furthermore piperidinyl, pyrrolidinyl, morpholinyl, imidazolyl or triazolyl, or piperidinyl, pyrrolidinyl, morpholinyl, imidazolyl or triazolyl each substituted by C.sub.1 -C.sub.3 alkyl, C.sub.1 -C.sub.3 alkoxy, C.sub.1 -C.sub.3 haloalkyl having from 1 to 3 halogen atoms, halogen, nitro or by cyano.The novel active ingredients have plant-protecting properties and are suitable especially for the preventive protection of plants against attack by phytopathogenic microorganisms such as fungi, bacteria and viruses.

    Compositions for protecting plants against disease
    4.
    发明授权
    Compositions for protecting plants against disease 失效
    防治疾病的植物的组合物

    公开(公告)号：US5112840A

    公开(公告)日：1992-05-12

    申请号：US594889

    申请日：1990-10-09

    申请人： Helmut Zondler ,  Alfred Meyer ,  Wolfgang Eckhardt ,  Walter Kunz

    发明人： Helmut Zondler ,  Alfred Meyer ,  Wolfgang Eckhardt ,  Walter Kunz

    IPC分类号： A01N43/40 ,  A01N43/50 ,  A01N43/54 ,  A01N43/58 ,  A01N43/60 ,  A01N43/653 ,  C07D213/81 ,  C07D401/06 ,  C07D401/12 ,  C07D401/14 ,  C07D413/14

    CPC分类号： C07D213/81 ,  A01N43/40 ,  A01N43/50 ,  A01N43/54 ,  A01N43/58 ,  A01N43/60 ,  A01N43/653 ,  C07D401/06 ,  C07D401/12 ,  C07D401/14

    摘要： Novel substituted isonicotinic acid amides of the general formula ##STR1## in which X in ortho/ortho'-position are equal and represent fluorine, chlorine, bromine or iodine;Q.sub.1 is unsubstituted pyrimidin-4-yl, or pyrimidin-4-yl substituted by R.sub.1, R.sub.2 and R.sub.3 ;Q.sub.2 is unsubstituted pyrimidin-2-yl, or pyrimidin-2-yl substituted by R.sub.1,R.sub.2 and R.sub.3 ;Q.sub.3 is unsubstituted pyrimidin-5-yl, or pyrimidin-5-yl substituted by R.sub.1, R.sub.2 and R.sub.3 ;Q.sub.4 is pyridin-2-yl, pyridin-3-yl or pyridin-4-yl each of which is unsubstituted or substituted by R.sub.1, R.sub.2 and R.sub.3 ;Q.sub.5 is pyridazin-3-yl or pyridazin-4-yl each of which is unsubstituted or substituted by R.sub.1, R.sub.2 and R.sub.3 ;Q.sub.6 is unsubstituted pyrazin-2-yl, or pyrazin-2-yl substituted by R.sub.1, R.sub.2 and R.sub.3 ;R.sub.1, R.sub.2, R.sub.3 are hydrogen, C.sub.1 -C.sub.6 alkyl, C.sub.1 -C.sub.6 haloalkyl having from 1 to 3 halogen atoms, C.sub.1 -C.sub.6 alkoxy, C.sub.2 -C.sub.6 alkoxyalkyl, C.sub.1 -C.sub.6 thioalkyl, C.sub.1 -C.sub.6 haloalkoxy having from 1 to 5 halogen atoms, C.sub.3 -C.sub.6 alkenyloxy, C.sub.3 -C.sub.6 alkynyloxy, C.sub.3 -C.sub.6 thioalkenyl, C.sub.3 -C.sub.6 cycloalkyl, C.sub.3 -C.sub.6 cycloalkyl substituted by methyl, or nitro, cyano, the radical CH(OR.sub.4).sub.2 or COOR.sub.4 in which R.sub.4 is C.sub.1 -C.sub.4 alkyl; also phenyl, phenoxy, thiophenyl, benzyl, benzyloxy or thiobenzyl; or phenyl, phenoxy, thiophenyl, benzyl, benzyloxy or thiobenzyl each substituted at least once by C.sub.1 -C.sub.3 alkyl, C.sub.1 -C.sub.3 -alkoxy, C.sub.1 -C.sub.3 haloalkyl having from 1 to 3 halogen atoms, halogen, nitro or by cyano; and also N(R.sub.5)R.sub.6 in which R.sub.5 and R.sub.6, independently of one another, are each C.sub.1 -C.sub.6 alkyl; and furthermore piperidinyl, pyrrolidinyl, morpholinyl, imidazolyl or triazolyl, or piperidinyl, pyrrolidinyl, morpholinyl, imidazolyl or triazolyl each substituted by C.sub.1 -C.sub.3 alkyl, C.sub.1 -C.sub.3 alkoxy, C.sub.1 -C.sub.3 haloalkyl having from 1 to 3 halogen atoms, halogen, nitro or by cyano.The novel ingredients have plant-protecting properties and are suitable especially for the preventive protection of plants against attack by phytopathogenic microorganisms such as fungi, bacteria and viruses.

    Compositions for protecting plants against disease
    5.
    发明授权
    Compositions for protecting plants against disease 失效
    用于保护植物免受疾病的组合物

    公开(公告)号：US4959096A

    公开(公告)日：1990-09-25

    申请号：US324876

    申请日：1989-03-17

    申请人： Helmut Zondler ,  Walter Kunz

    发明人： Helmut Zondler ,  Walter Kunz

    IPC分类号： C07D249/08 ,  A01N43/40 ,  A01N43/50 ,  A01N43/653 ,  C07D213/79 ,  C07D233/54 ,  C07D401/12 ,  C07D405/12 ,  C07D409/12 ,  C07D521/00

    CPC分类号： C07D213/79 ,  A01N43/40 ,  A01N43/50 ,  A01N43/653 ,  C07D231/12 ,  C07D233/56 ,  C07D249/08 ,  C07D405/12 ,  C07D409/12

    摘要： Novel substituted isonicotinic acid esters of the general formula ##STR1## in which Y is halogen;X is oxygen or sulfur;Q is C.sub.1 -C.sub.3 alkylene, propenylene, C.sub.1 -C.sub.3 alkylene mono- or di-substituted by R, or propenylene mono- or di-substituted by R;R is C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 haloalkyl having from 1 to 3 halogen atoms, cyano, C.sub.2 -C.sub.5 alkoxycarbonyl, C.sub.3 -C.sub.6 cycloalkyl, phenyl, or phenyl substituted by C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, halogen, trifluoromethyl, tricholoromethyl, nitro or by cyano, or benzoyl or benzoyl substituted by C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, trifluoromethyl, trichloromethyl, nitro or by cyano;A is phenyl, biphenyl, phenoxyphenyl, naphthyl, pyridyl, furyl, thienyl, imidazolyl or triazolyl, it being possible for each of these radicals to be unsubstituted or substituted by halogen, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.3 alkoxy, C.sub.1 -C.sub.3 haloalkoxy having from 1 to 3 halogen atoms, trifluoromethyl, nitro or by cyano; with the proviso (1) that if A is imidazolyl or triazolyl R may not be phenyl or benzoyl, and (2) that A and the R substituent in Q may together contain no more than 3 rings.The novel active ingredients have plant-protecting properties and are suitable especially for the preventive protection of plants against attack by phytopathogenic microorganisms, such as fungi, bacteria and viruses.

    摘要翻译： 新颖的通式为“IMAGE”的取代的异烟酸酯，其中Y是卤素; X是氧或硫; Q是C1-C3亚烷基，亚丙烯基，被R单取代或二取代的C1-C3亚烷基，或被R单取代或二取代的亚丙烯基; R是C1-C4烷基，具有1至3个卤素原子的C 1 -C 4卤代烷基，氰基，C 2 -C 5烷氧基羰基，C 3 -C 6环烷基，苯基或被C 1 -C 4烷基，C 1 -C 4烷氧基，卤素，三氟甲基，三氯甲基，硝基或 氰基或苯甲酰基或被C 1 -C 4烷基，C 1 -C 4烷氧基，三氟甲基，三氯甲基，硝基或氰基取代的苯甲酰基; A是苯基，联苯基，苯氧基苯基，萘基，吡啶基，呋喃基，噻吩基，咪唑基或三唑基，这些基团中的每一个可以是未取代的或被卤素，C 1 -C 4烷基，C 1 -C 3烷氧基，C 1 -C 3卤代烷氧基 至3个卤素原子，三氟甲基，硝基或氰基; 条件是（1）如果A是咪唑基或三唑基R可以不是苯基或苯甲酰基，和（2）A中的A和R中的R取代基可以一起含有不多于3个环。 新型活性成分具有植物保护性质，特别适用于植物防止植物病原微生物如真菌，细菌和病毒侵袭的预防性保护。

    N-(2-nitrophenyl)-2-aminopyrimidine derivatives, the preparation and use thereof
    6.
    发明授权
    N-(2-nitrophenyl)-2-aminopyrimidine derivatives, the preparation and use thereof 失效
    N-（2-硝基苯基）-2-氨基嘧啶衍生物，的制备及应用

    公开(公告)号：US4659363A

    公开(公告)日：1987-04-21

    申请号：US632161

    申请日：1984-07-18

    申请人： Adolf Hubele ,  Helmut Zondler ,  Peter Riebli ,  Wolfgang Eckhardt

    发明人： Adolf Hubele ,  Helmut Zondler ,  Peter Riebli ,  Wolfgang Eckhardt

    IPC分类号： A01N43/54 ,  C07D239/42 ,  C07D239/46 ,  C07D239/47 ,  C07D239/52 ,  C07D239/56 ,  C07D401/12

    CPC分类号： C07D239/42 ,  A01N43/54 ,  C07D239/47 ,  C07D239/52 ,  C07D239/56 ,  C07D401/12

    摘要： The invention discloses novel N-(2-nitrophenyl)-2-aminopyrimidine derivatives of the general formula I ##STR1## wherein R.sub.1 and R.sub.2 are each independently NO.sub.2 or CF.sub.3, with the proviso that only R.sub.1 or R.sub.2 can be NO.sub.2R.sub.3 is halogen,R.sub.4 is hydrogen or the --C(O)R' group, in which R' is C.sub.1 -C.sub.4 alkyl which is unsubstituted or substituted by halogen, C.sub.1 -C.sub.3 alkoxy or C.sub.1 -C.sub.3 alkylthio,R.sub.5, R.sub.6 and R.sub.7 are each independently hydrogen, halogen, nitro, cyano, thiocyano, C.sub.1 -C.sub.12 alkyl, C.sub.3 -C.sub.8 cycloalkyl, C.sub.1 -C.sub.8 alkylthio, C.sub.1 -C.sub.6 alkylsulfonyl, C.sub.1 -C.sub.6 alkylsulfoxyl, C.sub.3 -C.sub.6 alkenyl, C.sub.3 -C.sub.6 haloalkenyl, C.sub.3 -C.sub.6 alkynyl, C.sub.3 -C.sub.6 haloalkynyl, C.sub.3 -C.sub.6 alkenyloxy, C.sub.3 -C.sub.6 -haloalkenyloxy, C.sub.3 -C.sub.6 alkenylthio, C.sub.3 -C.sub.6 alkynyloxy, C.sub.3 -C.sub.6 haloalkynyloxy, C.sub.1 -C.sub.8 alkyl which is substituted by halogen, cyano and/or C.sub.1 -C.sub.4 alkoxy, unsubstituted C.sub.1 -C.sub.8 alkoxy or halogen-substituted C.sub.1 -C.sub.8 alkoxy, the alkyl moiety of which may be interrupted by one or more single oxygen atoms; or are the Q--(E).sub.n --(X).sub.m -group, in which n is 0 or 1, m is 0 or 1, Q is phenyl which is unsubstituted or substituted by halogen, nitro, C.sub.1 -C.sub.3 alkyl, CF.sub.3 and/or C.sub.1 -C.sub.3 alkoxy, or is a saturated or unsaturated heterocyclic radical containing one or more hetero atoms, E is a C.sub.1 -C.sub.3 alkylene bridge, and X is oxygen or sulfur.Also disclosed are methods of preparing these compounds, and also agrochemical compositions which contain one such compound as active ingredient. The invention further relates to the use of the novel compounds, or, compositions containing them, in agriculture and related fields.

    摘要翻译： 本发明公开了通式I（I）的新型N-（2-硝基苯基）-2-氨基嘧啶衍生物，其中R 1和R 2各自独立地为NO 2或CF 3，条件是仅R 1或R 2可为NO 2 R 3 C 1 -C 3烷氧基或C 1 -C 3烷硫基，R 5，R 6和R 7各自独立地为氢，R 4为氢或-C（O）R'基团，其中R'为未被取代或被卤素取代的C 1 -C 4烷基， 卤素，硝基，氰基，硫氰基，C 1 -C 12烷基，C 3 -C 8环烷基，C 1 -C 8烷硫基，C 1 -C 6烷基磺酰基，C 1 -C 6烷基亚磺酰基，C 3 -C 6烯基，C 3 -C 6卤代烯基，C 3 -C 6炔基，C 3 -C 6卤代炔基，C 3 -C 6烯氧基， C 6-卤代链烯氧基，C 3 -C 6烯基硫基，C 3 -C 6炔氧基，C 3 -C 6卤代炔氧基，被卤素，氰基和/或C 1 -C 4烷氧基取代的C 1 -C 8烷基，未取代的C 1 -C 8烷氧基或卤素取代的C 1 -C 8烷氧基， 其可被一个或多个单个氧原子中断; 或者是Q-（E）n-（X）m-基，其中n为0或1，m为0或1，Q为未被取代或被卤素，硝基，C 1 -C 3烷基，CF 3和 或C1-C3烷氧基，或是含有一个或多个杂原子的饱和或不饱和杂环基，E是C1-C3亚烷基桥，X是氧或硫。 还公开了制备这些化合物的方法，以及含有一种这样的化合物作为活性成分的农药组合物。 本发明还涉及在农业和相关领域中新颖化合物或含有它们的组合物的用途。

    Coating compound based on epoxide resin, an amine curing agent, and a hydrazone modifier
    8.
    发明授权
    Coating compound based on epoxide resin, an amine curing agent, and a hydrazone modifier 失效
    基于环氧树脂的涂料化合物，胺固化剂和腙改性剂

    公开(公告)号：US4163098A

    公开(公告)日：1979-07-31

    申请号：US938190

    申请日：1978-08-30

    申请人： Helmut Zondler ,  Wolfgang Schneider

    发明人： Helmut Zondler ,  Wolfgang Schneider

    IPC分类号： C08G59/40 ,  C08G59/56 ,  C08G59/62

    CPC分类号： C08G59/4014 ,  C08G59/56

    摘要： The coating compound according to the invention contains an epoxide resin, a diprimary amine curing agent and as modifier a hydrazone of the formula ##STR1## wherein the radical R.sup.1 -R.sup.4 represent hydrogen or alkyl, provides after curing coatings having a smooth, lustrous and glass-like surface which has a good resistence to chemicals.

    摘要翻译： 根据本发明的涂料化合物含有环氧树脂，二原子胺固化剂和作为改性剂的式“IMAGE”的腙，其中基团R 1 -R 4表示氢或烷基，在固化具有光滑，光泽和玻璃的涂层之后提供 对化学品具有很好的耐受性。

    Polymers flameproofed with 1,2-oxaphospholanes
    10.
    发明授权
    Polymers flameproofed with 1,2-oxaphospholanes 失效
    聚合物用1,2-氧代磷杂环戊烷隔离

    公开(公告)号：US4113669A

    公开(公告)日：1978-09-12

    申请号：US806044

    申请日：1977-06-13

    申请人： Helmut Zondler ,  Emil Saladin ,  Rudolf Kirchmayr

    发明人： Helmut Zondler ,  Emil Saladin ,  Rudolf Kirchmayr

    IPC分类号： C07F9/40 ,  C07F9/6571 ,  C08K5/5357 ,  C08K5/53

    CPC分类号： C08K5/5357 ,  C07F9/4006 ,  C07F9/657181 ,  Y10S521/906

    摘要： 2-Oxo-2-alkoxy-5-dialkylphosphono-1,2-oxaphospholanes of the formula ##STR1## in which R.sub.1 to R.sub.7 are hydrocarbon radicals can be prepared from .alpha.,.beta.-unsaturated ketones and 2 or more moles of a dialkyl phosphite. Obviously .gamma.-ketophosphonates are intermediates of this reaction, as these compounds react with 1 or more moles of dialkyl phosphite in yielding the oxaphospholanes too. Both reactions are promoted by alkaline catalysts.The new oxaphospholane derivatives are considerably stable against thermal decomposition. They are compatible with polymeric materials and can be used as flame protecting agent for plastics and resins, for example, in polyurethane foams.

    摘要翻译： 其中R 1至R 7为烃基的式“IMAGE”的2-氧代-2-烷氧基-5-二烷基膦酰基-1,2-氧代磷杂环戊烷可以由α，β-不饱和酮和2或更多摩尔的亚磷酸二烷基酯制备 。 显然，γ-酮膦酸盐是该反应的中间体，因为这些化合物也与1摩尔或更多摩尔的亚磷酸二烷基酯反应，产生氧代山梨醇。 两种反应均由碱性催化剂促进。