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公开(公告)号：US5646258A
公开(公告)日：1997-07-08
申请号：US555564
申请日：1995-11-08
CPC分类号： C07H15/04
摘要： A method for synthesizing alkyl glucosides by the acetalization of sugars, particularly glucose, with alcohols in excess and subsequent separation of the excess alcohol by extraction, the extraction being carried out with an extraction agent, which is close to the critical point at a reduced pressure in the range of 0.8 to 1.3 and preferably of 0.9 to 1.2 at pressures, which are selected so that the density of the extraction agent, which is close to the critical point, is greater than 180 kg/m.sup.3.
摘要翻译： 通过将醇，特别是葡萄糖与醇过量缩合并随后通过萃取分离过量的醇来合成烷基葡糖苷的方法，用萃取剂进行萃取，该提取剂在减压下接近临界点 在0.8至1.3的范围内，优选在0.9至1.2的压力下进行选择，使得接近临界点的萃取剂的密度大于180kg / m 3。
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公开(公告)号：US5837831A
公开(公告)日：1998-11-17
申请号：US717950
申请日：1996-09-23
CPC分类号： C07H15/04 , Y02P20/544
摘要： The invention relates to a method for separating alkyl glycoside mixtures or alcohol-containing alkyl glycoside mixtures by extraction, which is characterized in that the extraction is carried out with an extraction agent, which is close to or below the critical point at a reduced temperature ranging from 0.9 to 1.2, and at pressures, which are selected so that the density of the extraction agent is at least 180 kg/m.sup.3.
摘要翻译： 本发明涉及一种通过提取分离烷基糖苷混合物或含醇烷基糖苷混合物的方法，其特征在于用提取剂进行萃取，该提取剂在降低的温度范围内接近或低于临界点 0.9至1.2，并且在压力下，其选择使得提取剂的密度为至少180kg / m 3。
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3.发明授权Process for preparing pure monoglycerides, pure diglycerides and/or pure triglycerides 失效制备纯甘油单酯，纯甘油二酯和/或纯甘油三酯的方法
公开(公告)号：US5434280A
公开(公告)日：1995-07-18
申请号：US155923
申请日：1993-11-22
申请人： Siegfried Peter , Bernd Czech , Ulrich Ender , Eckhard Weidner
发明人： Siegfried Peter , Bernd Czech , Ulrich Ender , Eckhard Weidner
CPC分类号： C07C67/58
摘要： The invention relates to a process for recovering monoglycerides and optionally diglycerides and/or triglycerides as well as optionally glycerol from mixtures comprising glycerides and glycerol containing glycerides, respectively, by countercurrent extraction with a circulating extraction. As an extractant, forming a separate phase, there is used a hydrocarbon having a density of more than 180 kg/m.sup.3 and/or trifluoromethane having a density of more than 180 kg/m.sup.3.
摘要翻译： 本发明涉及通过循环提取的逆流提取来分别回收单甘油酯和任选的甘油二酯和/或甘油三酸酯以及任选的甘油，其包含甘油酯和含甘油的甘油酯的混合物。 作为萃取剂，形成分离相，使用密度大于180kg / m 3的烃和/或密度大于180kg / m 3的三氟甲烷。
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4.发明授权Process for the transesterification of fats and oils of biological origin by means of alcoholysis using special carbonic acid salts 失效通过使用特殊的碳酸盐进行醇解来酯交换生物来源的脂肪和油的方法公开(公告)号：US07468450B2
公开(公告)日：2008-12-23
申请号：US11086267
申请日：2005-03-22
申请人： Siegfried Peter , Eckhard Weidner
发明人： Siegfried Peter , Eckhard Weidner
IPC分类号： C11C1/00
摘要： The invention relates to a process for the preparation of fatty acid esters from fats and oils of biological origin by transesterification with monohydric alcohols in the presence of basic catalysts, the catalysts being salts of a basic organic compound and carbonic acid.
摘要翻译： 本发明涉及一种通过在碱性催化剂存在下通过与一元醇的酯交换从生物来源的脂肪和油制备脂肪酸酯的方法，该催化剂是碱性有机化合物和碳酸的盐。
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5.发明申请Process for the transesterification of fats and oils of biological origin by means of alcoholysis using special carbonic acid salts 失效通过使用特殊的碳酸盐进行醇解来酯化生物来源的脂肪和油的方法公开(公告)号：US20060058540A1
公开(公告)日：2006-03-16
申请号：US11086267
申请日：2005-03-22
申请人： Siegfried Peter , Eckhard Weidner
发明人： Siegfried Peter , Eckhard Weidner
IPC分类号： C07C51/43
摘要： The invention relates to a process for the preparation of fatty acid esters from fats and oils of biological origin by transesterification with monohydric alcohols in the presence of basic catalysts, the catalysts being salts of a basic organic compound and carbonic acid.
摘要翻译： 本发明涉及一种通过在碱性催化剂存在下通过与一元醇的酯交换从生物来源的脂肪和油制备脂肪酸酯的方法，该催化剂是碱性有机化合物和碳酸的盐。
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6.发明授权Process for removing free fatty acids from fats and oils of biological origin or their steam distillates 失效从生物来源的油脂或其蒸馏馏分中除去游离脂肪酸的方法公开(公告)号：US06579996B2
公开(公告)日：2003-06-17
申请号：US10046063
申请日：2001-10-20
IPC分类号： C11B300
CPC分类号： C11B3/06
摘要： A method for removing free fatty acids from fats or oils of biological origin or their steam distillates by extracting the free fatty acids with a mixture of basic organic nitrogen compounds and water as an extraction medium at a temperature below the boiling point of the organic nitrogen compounds. The content of the basic organic nitrogen compounds in the extraction medium is 20-30% by weight. In this manner, the formation of a viscous soapstock which is difficult to remove is prevented. The boiling point of the basic organic nitrogen compounds used is the same as or above boiling point of water and below the boiling point of the fatty acids to be extracted in order to enable simple recovery of the extraction medium.
摘要翻译： 通过在低于有机氮化合物的沸点的温度下用碱性有机氮化合物和水的混合物萃取游离脂肪酸作为提取介质，从生物来源的脂肪或油或其蒸汽馏出物中除去游离脂肪酸的方法 。 萃取介质中碱性有机氮化合物的含量为20-60％（重量）。 以这种方式，防止了难以去除的粘性肥皂的形成。 使用的碱性有机氮化合物的沸点与水的沸点相同或高于待提取的脂肪酸的沸点，以使得能够简单地回收萃取介质。
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公开(公告)号：US06211390B1
公开(公告)日：2001-04-03
申请号：US09269090
申请日：1999-12-03
申请人： Siegfried Peter , Ruth Ganswindt , Eckhard Weidner
发明人： Siegfried Peter , Ruth Ganswindt , Eckhard Weidner
IPC分类号： C07C5100
摘要： The invention concerns a method for producing fatty acid esters from fatty acid triglyceride and in particular from animal or vegetable fats and oils by transesterification with a monovalent low-molecular weight alcohol in the presence of a homogeneous or heterogeneous catalyst. In accordance with the invention, the formed fatty acid ester is extracted from the reaction mixture by means of a near-critical extractant. In this way fatty acid esters are obtained at high yield and excellent purity. As the extractant preferably a low pressure gas having a reduced temperature at 20° C. of about 0.7, preferably of equal to or greater than 0.7, is employed. Preferred extractants are carbon dioxide, propane, butane, dimethyl ether, ethyl acetate or mixtures thereof.
摘要翻译： 本发明涉及一种通过在均相或多相催化剂存在下通过与一价低分子量醇的酯交换从脂肪酸甘油三酯，特别是动物或植物脂肪和油制备脂肪酸酯的方法。 根据本发明，通过近临界萃取剂从反应混合物中提取形成的脂肪酸酯。 以这种方式获得高产率和优异纯度的脂肪酸酯。 作为萃取剂，优选使用在20℃下的温度降低约0.7，优选等于或大于0.7的低压气体。 优选的萃取剂是二氧化碳，丙烷，丁烷，二甲醚，乙酸乙酯或其混合物。
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8.发明申请Process for the transesterification of fat and/or oil by heterogeneous catalysis 审中-公开通过非均相催化酯交换脂肪和/或油的方法公开(公告)号：US20050020843A1
公开(公告)日：2005-01-27
申请号：US10887455
申请日：2004-07-08
摘要： A process for preparing fat and/or oil with a modified distribution of fatty acids in the glycerides by heterogeneously catalysed transesterification, wherein the process comprises reaction of the fat and/or oil of biological origin to be transesterified in the presence of a catalyst consisting of a metal salt of a basic amino acid or an amino acid derivative. The disadvantages of conventional transesterification processes can be overcome by using this catalyst.
摘要翻译： 一种通过异构催化酯交换制备具有脂肪酸在甘油酯中的分布改变的脂肪和/或油的方法，其中所述方法包括将生物来源的脂肪和/或油在催化剂存在下进行酯交换反应，所述催化剂由 碱性氨基酸或氨基酸衍生物的金属盐。 通过使用该催化剂可以克服常规酯交换方法的缺点。
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公开(公告)号：US06407306B1
公开(公告)日：2002-06-18
申请号：US09709823
申请日：2000-11-10
IPC分类号： C07C40300
CPC分类号： C07C403/24 , C09B61/00
摘要： A process is described for extracting carotenes from carotene-containing materials, in particular from fats and oils of biological origin, which provides for extraction of carotene-containing material with an extractant comprising at least one member selected from the group consisting of acetonitrile, N-methylpyrrolidone, N,Ndimethylformamide, N,N-dimethylacetamide, 4-formylmorpholine, 4-acetylmorpholine, 4-methylmorpholine, 4-phenylmorpholine.
摘要翻译： 描述了一种用于从含胡萝卜素的材料，特别是从生物来源的脂肪和油中提取胡萝卜素的方法，其提供了含有至少一种选自乙腈，N- N-甲基吡咯烷酮，N，N-二甲基甲酰胺，N，N-二甲基乙酰胺，4-甲酰基吗啉，4-乙酰基吗啉，4-甲基吗啉，4-苯基吗啉。
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10.发明授权公开(公告)号：US06933398B2
公开(公告)日：2005-08-23
申请号：US10669617
申请日：2003-09-24
申请人： Siegfried Peter , Eckhard Weidner
发明人： Siegfried Peter , Eckhard Weidner
摘要： The present invention relates to a process for obtaining fatty acid esters from triglycerides by means of alcoholysis. In particular, the invention relates to a process for the transesterification of fat and/or oil by alcoholysis wherein, in order to accelerate the process in the initial stage, at least one alkanol fatty acid ester is added in a quantity such that the reaction mixture produced thereby consists of one phase. A high reaction rate can thereby be maintained in the process from the beginning.
摘要翻译： 本发明涉及通过醇解从甘油三酯获得脂肪酸酯的方法。 特别地，本发明涉及通过醇解来酯交换脂肪和/或油的方法，其中为了加速初始阶段的方法，加入至少一种链烷醇脂肪酸酯使得反应混合物 由此产生的一个阶段。 因此，从一开始就可以保持高的反应速度。
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