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    Preparation of aqueous polymer dispersions with a bimodal particle-size distribution
    1.
    发明授权
    Preparation of aqueous polymer dispersions with a bimodal particle-size distribution 失效
    制备具有双峰粒度分布的聚合物水分散体

    公开(公告)号：US5990221A

    公开(公告)日：1999-11-23

    申请号：US889591

    申请日：1997-07-08

    Applicant: Burkhardt Dames ,  Klemens Mathauer ,  Walter Machtle

    Inventor： Burkhardt Dames ,  Klemens Mathauer ,  Walter Machtle

    IPC: C08F2/22 ,  C08F2/24 ,  C08J3/02

    CPC classification number: C08F2/24

    Abstract: A process for preparing aqueous polymer dispersions by emulsion polymerization of free-radically polymerizable compounds (monomers) comprises adding, during the polymerization of the monomers, a miniemulsion which is an aqueous, surfactant-stabilized emulsion of monomers whose emulsified droplets have a size of from 10 to 500 nm and which comprises a compound (stabilizer) which is dissolved in the monomers of the droplets and whose solubility in the monomers is at least twice its solubility in water.

    Abstract translation: 通过可自由基聚合的化合物（单体）的乳液聚合制备含水聚合物分散体的方法包括在单体的聚合期间加入细乳液，该乳液是单体的水性表面活性剂稳定的乳液，其乳化液滴的尺寸为 10-500nm，其包含溶解在液滴单体中的化合物（稳定剂），其在单体中的溶解度至少为其在水中的溶解度的两倍。

    Emulsion polymerization process with combination macroemulsion and miniemulsion feed streams
    3.
    发明授权
    Emulsion polymerization process with combination macroemulsion and miniemulsion feed streams 失效
    乳液聚合工艺与组合的大乳液和微乳液进料流

    公开(公告)号：US6160049A

    公开(公告)日：2000-12-12

    申请号：US147203

    申请日：1998-10-28

    Applicant: Klemens Mathauer ,  Walter Machtle ,  Graham Edmund McKee ,  Hubertus Kroner

    Inventor： Klemens Mathauer ,  Walter Machtle ,  Graham Edmund McKee ,  Hubertus Kroner

    IPC: C08F2/00 ,  C08F2/22 ,  C08F2/24 ,  C08F2/38

    CPC classification number: C08F2/24

    Abstract: A process for preparing an aqueous polymer dispersion by free-radically initiated polymerization of free-radically polymerizable compounds I with moderate solubility in water, whose disperse polymer particles contain not only compounds I but also compounds II with a very low solubility in water where a mixture consisting of a portion of the compounds I and consisting of the compounds II is used to produce an aqueous emulsion I with a droplet size .ltoreq.500 nm, and at least a portion of the aqueous emulsion I is supplied continuously to the polymerization vessel as a feed stream I, in the course of continuing free-radical polymerization, during which the continuous feed stream I is accompanied, at least some of the time, by a feed stream II consisting of another portion of the compounds I or of the aqueous emulsion II thereof with a droplet size .gtoreq.1000 nm.

    Abstract translation: PCT No.PCT / EP97 / 03397 371 1998年10月28日第 102（e）1998年10月28日PCT 1997年6月30日PCT公布。 公开号WO98 / 02466 日期1998年1月22日一种通过自由基引发聚合可自由基聚合的化合物I制备水性聚合物分散体的方法，该可自由基聚合的化合物I在水中具有适度的溶解度，其分散聚合物颗粒不仅含有化合物I，而且包含非常低的溶解度的化合物II 在其中使用由化合物I的一部分组成并且由化合物II组成的混合物的水中，以产生具有小滴尺寸为500nm的水性乳液I，并且连续供应至少一部分水性乳液I 作为进料流I作为进料流I，在连续自由基聚合的过程中，连续进料流I至少在一段时间内由由化合物I的另一部分组成的进料流II 或其水乳液II的液滴尺寸> 1000nm。

    Determining production parameters of scale flow device
    8.
    发明授权
    Determining production parameters of scale flow device 失效
    确定秤流量装置的生产参数

    公开(公告)号：US06515030B1

    公开(公告)日：2003-02-04

    申请号：US09581820

    申请日：2000-06-19

    Applicant: Siegfried Bechtel ,  Sabine Kielhorn-Bayer ,  Klemens Mathauer

    Inventor： Siegfried Bechtel ,  Sabine Kielhorn-Bayer ,  Klemens Mathauer

    IPC: B01F1102

    CPC classification number: B01F3/0815 ,  B01F11/0241 ,  B01F11/0266 ,  B01J19/10 ,  Y10S516/924 ,  Y10S526/909

    Abstract: A device for producing disperse mixtures by ultrasound, containing a housing, and a reaction chamber within the housing and at least one sonotrode having a free emitting surface which is directly in effective connection with the reaction chamber and whose end remote from the free emitting surface is coupled to an ultrasonic transducer, wherein the sonotrode is designed as a rod-shaped, axially emitting longitudinal oscillator with the emitting surface corresponding essentially to the surface of the reaction chamber, and wherein the reaction chamber depth which is essentially vertical with respect to the emitting surface is lower than a maximum effective depth of the sonotrode.

    Abstract translation: 一种用于通过超声波产生分散混合物的装置，其包含壳体和在壳体内的反应室，并且至少一个具有自由发射表面的超声波发生器，其直接与反应室有效连接，并且其远离自由发射表面的一端是 耦合到超声波换能器，其中所述超声波发生器被设计为棒状的轴向发射的纵向振荡器，所述发射表面基本上对应于所述反应室的表面，并且其中所述反应室深度相对于所述发射基本上是垂直的 表面低于超声波发生器的最大有效深度。

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