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公开(公告)号：US20230415127A1
公开(公告)日：2023-12-28
申请号：US18242799
申请日：2023-09-06
Applicant: Chevron Phillips Chemical Company LP
Inventor： Jeremy M. PRAETORIUS , Eric D. SCHWERDTFEGER , Max P. MCDANIEL , Ted H. CYMBALUK , Connor D. BOXELL , Alan L. SOLENBERGER , Kathy S. CLEAR
CPC classification number: B01J23/26 , C08F10/02 , B01J21/08 , B01J35/1019 , C08F110/02 , B01J35/1047 , B01J37/0203 , B01J37/0236 , B01J37/08 , B01J35/1023
Abstract: A method comprising a) drying a support material comprising silica at temperature in the range of from about 150° C. to about 220° C. to form a dried support; b) contacting the dried support with methanol to form a slurried support; c) subsequent to b), cooling the slurried support to a temperature of less than about 60° C. to form a cooled slurried support; d) subsequent to c), contacting the cooled slurried support with a titanium alkoxide to form a titanated support; and e) thermally treating the titanated support by heating to a temperature of equal to or greater than about 150° C. for a time period of from about 5 hours to about 30 hours to remove the methanol and yield a dried titanated support.
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公开(公告)号：US20220203333A1
公开(公告)日：2022-06-30
申请号：US17699366
申请日：2022-03-21
Applicant: Chevron Phillips Chemical Company LP
Inventor： Jeremy M. PRAETORIUS , Eric D. SCHWERDTFEGER , Max P. MCDANIEL , Ted H. CYMBALUK , Connor D. BOXELL , Alan L. SOLENBERGER , Kathy S. CLEAR
Abstract: A method comprising a) drying a support material comprising silica at temperature in the range of from about 150° C. to about 220° C. to form a dried support; b) contacting the dried support with methanol to form a slurried support; c) subsequent to b), cooling the slurried support to a temperature of less than about 60° C. to form a cooled slurried support; d) subsequent to c), contacting the cooled slurried support with a titanium alkoxide to form a titanated support; and e) thermally treating the titanated support by heating to a temperature of equal to or greater than about 150° C. for a time period of from about 5 hours to about 30 hours to remove the methanol and yield a dried titanated support.
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公开(公告)号：US20180094087A1
公开(公告)日：2018-04-05
申请号：US15281538
申请日：2016-09-30
Applicant: Chevron Phillips Chemical Company LP
Inventor： Max P. MCDANIEL , Eric D. SCHWERDTFEGER , Jeremy M. PRAETORIUS , Alan L. SOLENBERGER , Kathy S. CLEAR
IPC: C08F110/02
CPC classification number: C08F110/02 , C08F10/02 , C08F4/22 , C08F4/16 , C08F4/025 , C08F2500/04 , C08F2500/12 , C08F210/16 , C08F210/14
Abstract: A method of preparing a catalyst comprising a) contacting (i) a silica-support, (ii) an oxotitanium compound, (iii) a chromium-containing compound, and (iv) an optional solvent to form a first aqueous mixture comprising a pre-catalyst and a reaction media having from about 1 wt. % to about 99 wt. % water; b) thermally treating the pre-catalyst by heating to a temperature of from about 400° C. to about 1000° C. for a time period of from about 1 minute to about 24 hours to form the catalyst. A method of preparing a catalyst comprising contacting a hydrated support material comprising silica with a chromium-containing compound to form a first aqueous mixture comprising a chrominated support; contacting the first aqueous mixture comprising a chrominated support with a solution comprising (i) a solvent and (ii) an oxotitanium compound to form a second aqueous mixture comprising a pre-catalyst; and thermally treating the pre-catalyst to form the catalyst.
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Patent Agency Ranking
公开(公告)号：US20170037158A1
公开(公告)日：2017-02-09
申请号：US15298540
申请日：2016-10-20
Applicant: Chevron Phillips Chemical Company LP
Inventor： Youlu YU , Eric D. SCHWERDTFEGER , Max P. MCDANIEL , Alan L. SOLENBERGER , Kathy S. COLLINS
IPC: C08F110/02
CPC classification number: C08F110/02 , B01J23/26 , B01J35/1009 , B01J35/1014 , B01J35/1019 , C08F10/02 , C08F210/02 , C08F2500/04 , C08F2500/09 , C08F4/69 , C08F4/025
Abstract: A polymer having a long chain branching content peaking at greater than about 20 long chain branches per million carbon atoms, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution. A polymer having a long chain branching content peaking at greater than about 8 long chain branches per million carbon atoms, a polydispersity index of greater than about 20 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution. A polymer having a long chain branching content peaking at greater than about 1 long chain branches per chain, and a polydispersity index of greater than about 10 wherein the long chain branching decreases to approximately zero at the higher molecular weight portion of the molecular weight distribution.
Abstract translation: 具有长链支化含量高于每百万个碳原子大于约20个长支链的聚合物，多分散指数大于约10，其中长链支化在分子量的较高分子量部分下降至约零 分配。 具有长链支化含量高于每百万个碳原子大于约8个长链分支的聚合物，多分散指数大于约20，其中长链支化在分子量分布的较高分子量部分下降至约零 。 具有长链支化含量在每链大于约1个长链分支峰值的聚合物，以及大于约10的多分散指数，其中在分子量分布的较高分子量部分，长链支链降至约为零。
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公开(公告)号：US20190134610A1
公开(公告)日：2019-05-09
申请号：US16237011
申请日：2018-12-31
Applicant: Chevron Phillips Chemical Company LP
Inventor： Jeremy M. PRAETORIUS , Eric D. SCHWERDTFEGER , Max P. MCDANIEL , Ted H. CYMBALUK , Connor D. BOXELL , Alan L. SOLENBERGER , Kathy S. CLEAR
Abstract: A method comprising a) drying a support material comprising silica at temperature in the range of from about 150° C. to about 220° C. to form a dried support; b) contacting the dried support with methanol to form a slurried support; c) subsequent to b), cooling the slurried support to a temperature of less than about 60° C. to form a cooled slurried support; d) subsequent to c), contacting the cooled slurried support with a titanium alkoxide to form a titanated support; and e) thermally treating the titanated support by heating to a temperature of equal to or greater than about 150° C. for a time period of from about 5 hours to about 30 hours to remove the methanol and yield a dried titanated support.
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公开(公告)号：US20140275457A1
公开(公告)日：2014-09-18
申请号：US13799516
申请日：2013-03-13
Applicant: CHEVRON PHILLIPS CHEMICAL COMPANY LP
Inventor： Max P. MCDANIEL , Kathy S. COLLINS , Eric D. SCHWERDTFEGER , Alan L. SOLENBERGER
IPC: C08F4/22
CPC classification number: C08F4/22 , C08F10/00 , C08F4/24 , C08F4/025 , C08F110/02 , C08F2500/12
Abstract: A method comprising contacting a support material with a transition metal compound to produce a mixture; thermally treating the mixture in the presence of oxygen at a temperature in a range of from about 100° C. to about 500° C. for a period of from about 1 hour to about 10 hours, wherein at least a portion of the transition metal sublimes onto the support material to produce a support material comprising a dispersed transition metal; and thermally treating the support material comprising the dispersed transition metal in an oxidizing atmosphere at a temperature in a range of from about 550° C. to about 900° C. for a period of from about 1 hour to about 10 hours to produce a polymerization catalyst.
Abstract translation: 一种方法，包括使支撑材料与过渡金属化合物接触以产生混合物; 在氧气存在下，在约100℃至约500℃的温度范围内热处理混合物约1小时至约10小时，其中至少一部分过渡金属 升华到支撑材料上以产生包含分散的过渡金属的支撑材料; 并在包含分散的过渡金属的载体材料的氧化气氛中，在约550℃至约900℃的温度范围内热处理约1小时至约10小时，以产生聚合 催化剂。
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公开(公告)号：US20180305473A1
公开(公告)日：2018-10-25
申请号：US15495116
申请日：2017-04-24
Applicant: Chevron Phillips Chemical Company LP
Inventor： Eric D. SCHWERDTFEGER , Max P. MCDANIEL , Ted H. CYMBALUK , Jeremy M. PRAETORIUS , Kathy S. CLEAR , Alan L. SOLENBERGER
IPC: C08F10/02
CPC classification number: C08F10/02 , B01J23/26 , B01J35/023 , B01J35/1019 , B01J35/1023 , B01J35/1038 , B01J35/1042 , B01J35/1047 , B01J37/0203 , B01J37/0205 , B01J37/08 , B01J37/086 , B01J37/14 , B01J2523/00 , C08F2/34 , C08F4/025 , C08F4/24 , C08F4/76 , C08F4/78 , C08F110/02 , B01J2523/41 , B01J2523/47 , B01J2523/67
Abstract: A method comprising calcining a catalyst precursor comprising chromium and a silica support material at a temperature in the range of from about 95° C. to about 400° C. in a bed fluidized by a gas flowing at a volumetric flow rate of from about 2.5 to about 30 times the settled volume of the bed per minute to form a calcined catalyst precursor. A method comprising calcining a catalyst precursor comprising chromium and silica at a temperature in the range of from about 95° C. to about 400° C. with a gas flowing through the bed at a gas hourly space velocity of from about 15 to about 200 per hour. A method comprising calcining a catalyst precursor comprising chromium and silica at a temperature in the range of from about 95° C. to about 400° C. with a gas flowing through the bed at a weight hourly space velocity of from about 1.9 to about 240 per hour.
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公开(公告)号：US20170080406A1
公开(公告)日：2017-03-23
申请号：US14858512
申请日：2015-09-18
Applicant: Chevron Phillips Chemical Company LP
Inventor： Jeremy M. PRAETORIUS , Eric D. SCHWERDTFEGER , Max P. MCDANIEL , Ted H. CYMBALUK , Connor D. BOXELL , Alan L. SOLENBERGER , Kathy S. CLEAR
CPC classification number: B01J23/26 , B01J21/08 , B01J35/1019 , B01J35/1023 , B01J35/1047 , B01J37/0203 , B01J37/0236 , B01J37/08 , C08F10/02 , C08F110/02 , C08F4/22 , C08F4/24 , C08F4/025 , C08F4/16 , C08F2500/12
Abstract: A method comprising a) drying a support material comprising silica at temperature in the range of from about 150° C. to about 220° C. to form a dried support; b) contacting the dried support with methanol to form a slurried support; c) subsequent to b), cooling the slurried support to a temperature of less than about 60° C. to form a cooled slurried support; d) subsequent to c), contacting the cooled slurried support with a titanium alkoxide to form a titanated support; and e) thermally treating the titanated support by heating to a temperature of equal to or greater than about 150° C. for a time period of from about 5 hours to about 30 hours to remove the methanol and yield a dried titanated support.
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