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公开(公告)号：US20180327935A1
公开(公告)日：2018-11-15
申请号：US16045470
申请日：2018-07-25
发明人： Shao C. Chiu
IPC分类号： D01F11/12 , D01F9/22 , D06M101/40
CPC分类号： D01F11/128 , D01F9/22 , D01F11/122 , D06M11/34 , D06M11/60 , D06M2101/40
摘要： A gas phase surface treatment for treating carbon fiber including (a) exposing a carbon fiber to a gaseous oxidizing atmosphere to form a modified carbon fiber with an oxidized fiber surface; followed by (b) exposing the oxidized fiber surface to a gaseous nitrogen-containing atmosphere to form a modified carbon fiber with a nitrogen-enriched surface, wherein the nitrogen-enriched surface exhibits an increase in surface nitrogen to surface carbon (N/C) ratio as compared to the surface of the carbon fiber prior to exposure at (a). Steps (a) and (b) are carried out continuously without any additional intervening surface treatment.
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公开(公告)号：US20160263803A1
公开(公告)日：2016-09-15
申请号：US15043771
申请日：2016-02-15
发明人： John Desmond Cook , Thomas Taylor , Girish Vishnukant Deshpande , Longgui Tang , Barry DeWayne Meece , Suzanne Crawford , Shao C. Chiu , Billy D. Harmon , Alan Thomas
CPC分类号： D01D5/06 , B29C48/022 , B29C48/05 , B29K2033/20 , B29L2031/731 , D01F6/18 , D01F6/38 , D01F9/12 , D01F9/22 , D01F9/225
摘要： The present disclosure relates generally to carbon fibers having high tensile strength and modulus of elasticity, as well as a process for the manufacture of such carbon fiber. The process comprises spinning a polymer/solvent solution into a solvent/water bath in the range of 78%-85% solvent, thereby producing a dense fiber structure, and subsequently carbonizing the polymer precursor fiber at a lower than typical carbonization temperature to form carbon fibers.
摘要翻译： 本公开一般涉及具有高拉伸强度和弹性模量的碳纤维，以及制造这种碳纤维的方法。 该方法包括将聚合物/溶剂溶液在78％-85％溶剂范围内的溶剂/水浴中纺丝，从而产生致密的纤维结构，随后在低于典型的碳化温度下使聚合物前体纤维碳化以形成碳 纤维。
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公开(公告)号：US11479881B2
公开(公告)日：2022-10-25
申请号：US15315220
申请日：2016-02-15
发明人： John Desmond Cook , Thomas Taylor , Girish Vishnukant Deshpande , Longgui Tang , Barry DeWayne Meece , Suzanne Crawford , Shao C. Chiu , Billy D. Harmon , Alan Thomas
IPC分类号： B29C48/05 , D01D5/06 , B29C48/00 , D01F6/18 , D01F9/22 , D01F9/12 , D01F6/38 , B29K33/20 , B29L31/00
摘要： The present disclosure relates generally to carbon fibers having high tensile strength and modulus of elasticity, as well as a process for the manufacture of such carbon fiber. The process comprises spinning a polymer/solvent solution into a solvent/water bath in the range of 78%-85% solvent, thereby producing a dense fiber structure, and subsequently carbonizing the polymer precursor fiber at a lower than typical carbonization temperature to form carbon fibers.
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公开(公告)号：US10060053B2
公开(公告)日：2018-08-28
申请号：US15382832
申请日：2016-12-19
发明人： Shao C. Chiu
CPC分类号： D01F11/128 , C08J5/06 , D01F9/22 , D01F11/122 , D06M11/34 , D06M11/60 , D06M2101/40
摘要： A gas phase surface treatment for treating carbon fiber including (a) exposing a carbon fiber to a gaseous oxidizing atmosphere to form a modified carbon fiber with an oxidized fiber surface; followed by (b) exposing the oxidized fiber surface to a gaseous nitrogen-containing atmosphere to form a modified carbon fiber with a nitrogen-enriched surface, wherein the nitrogen-enriched surface exhibits an increase in surface nitrogen to surface carbon (N/C) ratio as compared to the surface of the carbon fiber prior to exposure at (a). Steps (a) and (b) are carried out continuously without any additional intervening surface treatment.
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公开(公告)号：US20160221034A1
公开(公告)日：2016-08-04
申请号：US14551128
申请日：2014-11-24
发明人： Shao C. Chiu , Longgui Tang , Billy D. Harmon
CPC分类号： B05D3/007 , B05D1/18 , B05D3/0254 , B05D3/107 , B05D7/24 , B05D2203/00 , B05D2203/30 , B05D2256/00 , B05D2401/20 , B05D2401/21 , B05D2504/00 , B05D2505/50 , B05D2508/00 , D06M15/327 , D06M15/53 , D06M15/55 , D06M15/59 , D06M15/63 , D06M23/10 , D06M2101/40
摘要： Various embodiments directed towards methods of applying sizing to fibers are disclosed herein. In some embodiments, solvent can be used to dissolve a sizing material into a solution, which can then be used to coat the fibers. In some embodiments, a water bath is used to coagulate a sizing on the fiber surface and to remove the remove solvent after coating the fibers, so that water vapor can be created during a subsequent drying step as opposed to solvent vapors. In some embodiments, strong acids or strong bases can be used as the solvent.
摘要翻译： 本文公开了针对纤维施加尺寸的方法的各种实施方案。 在一些实施方案中，可以使用溶剂将上浆材料溶解到溶液中，然后可以将其涂覆在纤维上。 在一些实施方案中，水浴用于凝结纤维表面上的上浆并且在涂覆纤维之后去除除去溶剂，使得在随后的干燥步骤中可以产生水蒸汽，而不是溶剂蒸气。 在一些实施方案中，可以使用强酸或强碱作为溶剂。
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公开(公告)号：US09757768B2
公开(公告)日：2017-09-12
申请号：US14551128
申请日：2014-11-24
发明人： Shao C. Chiu , Longgui Tang , Billy D. Harmon
IPC分类号： B05D1/18 , B05D3/10 , B05D3/00 , B05D7/24 , D06M15/327 , D06M15/53 , D06M15/55 , D06M15/59 , D06M15/63 , D06M23/10 , B05D3/02 , D06M101/40
CPC分类号： B05D3/007 , B05D1/18 , B05D3/0254 , B05D3/107 , B05D7/24 , B05D2203/00 , B05D2203/30 , B05D2256/00 , B05D2401/20 , B05D2401/21 , B05D2504/00 , B05D2505/50 , B05D2508/00 , D06M15/327 , D06M15/53 , D06M15/55 , D06M15/59 , D06M15/63 , D06M23/10 , D06M2101/40
摘要： Various embodiments directed towards methods of applying sizing to fibers are disclosed herein. In some embodiments, solvent can be used to dissolve a sizing material into a solution, which can then be used to coat the fibers. In some embodiments, a water bath is used to coagulate a sizing on the fiber surface and to remove the remove solvent after coating the fibers, so that water vapor can be created during a subsequent drying step as opposed to solvent vapors. In some embodiments, strong acids or strong bases can be used as the solvent.
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公开(公告)号：US20170175298A1
公开(公告)日：2017-06-22
申请号：US15382832
申请日：2016-12-19
发明人： Shao C. Chiu
CPC分类号： D01F11/128 , D01F9/22 , D01F11/122 , D06M2101/40
摘要： A gas phase surface treatment for treating carbon fiber including (a) exposing a carbon fiber to a gaseous oxidizing atmosphere to form a modified carbon fiber with an oxidized fiber surface; followed by (b) exposing the oxidized fiber surface to a gaseous nitrogen-containing atmosphere to form a modified carbon fiber with a nitrogen-enriched surface, wherein the nitrogen-enriched surface exhibits an increase in surface nitrogen to surface carbon (N/C) ratio as compared to the surface of the carbon fiber prior to exposure at (a). Steps (a) and (b) are carried out continuously without any additional intervening surface treatment.
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