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    NOVEL FORMULATION OF A WARE WASHING SOLID CONTROLLING HARDNESS
    4.
    发明申请
    NOVEL FORMULATION OF A WARE WASHING SOLID CONTROLLING HARDNESS 有权
    一种清洁固体控制硬度的新型配方

    公开(公告)号：US20110021403A1

    公开(公告)日：2011-01-27

    申请号：US12843999

    申请日：2010-07-27

    申请人： Altony J. Miralles ,  Carter M. Silvernail

    发明人： Altony J. Miralles ,  Carter M. Silvernail

    IPC分类号： C11D3/37 ,  C02F5/10

    CPC分类号： C11D3/365 ,  C02F5/14 ,  C11D3/044 ,  C11D3/10 ,  C11D3/3757

    摘要： A water hardness controlling agent includes a polyacrylic acid or salt thereof having a molecular weight of between about 1,000 and about 50,000 g/mol, an acrylic-maleic acid copolymer or salt thereof having a molecular weight of between about 1,000 and about 100,000 g/mol and a phosphonocarboxylic acid or salt thereof. A ratio of acrylic-maleic acid copolymer or salt thereof to polyacrylic acid or salt thereof to phosphonocarboxylic acid or salt thereof in parts per million is about 1-30:10-80:6-20.

    摘要翻译： 水硬度控制剂包括分子量为约1,000至约50,000g / mol的聚丙烯酸或其盐，分子量为约1,000至约100,000g / mol的丙烯酸 - 马来酸共聚物或其盐 和膦酰基羧酸或其盐。 丙烯酸 - 马来酸共聚物或其盐与聚丙烯酸或其盐与膦酰基羧酸或其盐的百万分之比为约1-30:1-80:6-20。

    NOVEL SYNTHESIS AND APPLICATIONS OF AMINO CARBOXYLATES
    6.
    发明申请
    NOVEL SYNTHESIS AND APPLICATIONS OF AMINO CARBOXYLATES 有权
    氨基甲酸酯的新合成及应用

    公开(公告)号：US20090264677A1

    公开(公告)日：2009-10-22

    申请号：US12401715

    申请日：2009-03-11

    申请人： Altony J. Miralles ,  Carter M. Silvernail

    发明人： Altony J. Miralles ,  Carter M. Silvernail

    IPC分类号： C07C229/04

    CPC分类号： C07C227/08 ,  C07C319/12 ,  C07C323/52 ,  C07C229/16 ,  C07C229/24

    摘要： A method of synthesizing carboxylated amines is disclosed. The method comprises reacting a mixture of a potassium salt of either a primary or secondary amine with a potassium salt of a halogenated carboxylic acid wherein the halogenated carboxylic acid is selected from the group consisting of brominated, chlorinated, or iodinated carboxylic acid in the presence of potassium hydroxide, and optionally in heating the reacting mixture; precipitating the potassium salt by optionally chilling the mixture and discarding the precipitate; purifying the carboxylate amine potassium salt from the liquid phase using water soluble alcohol and optionally adding formic acid to obtain the free aminocarboxylic acid and potassium formate. In a preferred embodiment, the halogenated carboxylic acid is chloroacetic acid.

    摘要翻译： 公开了一种合成羧化胺的方法。 该方法包括将伯胺或仲胺的钾盐与卤代羧酸的钾盐的混合物反应，其中卤代羧酸选自溴化，氯化或碘化的羧酸，在 氢氧化钾，任选地加热反应混合物; 通过任选地冷却混合物并抛弃沉淀物沉淀钾盐; 使用水溶性醇从液相中纯化羧酸胺钾盐，并任选加入甲酸得到游离氨基羧酸和甲酸钾。 在优选的实施方案中，卤代羧酸是氯乙酸。

    Formulation of a ware washing solid controlling hardness
    7.
    发明授权
    Formulation of a ware washing solid controlling hardness 有权
    制品清洗固体控制硬度

    公开(公告)号：US08883035B2

    公开(公告)日：2014-11-11

    申请号：US12843999

    申请日：2010-07-27

    申请人： Altony J. Miralles ,  Carter M. Silvernail

    发明人： Altony J. Miralles ,  Carter M. Silvernail

    IPC分类号： C02F5/02 ,  C02F5/14 ,  C11D3/04 ,  C11D3/10 ,  C11D3/36 ,  C11D3/37

    CPC分类号： C11D3/365 ,  C02F5/14 ,  C11D3/044 ,  C11D3/10 ,  C11D3/3757

    摘要： A water hardness controlling agent includes a polyacrylic acid or salt thereof having a molecular weight of between about 1,000 and about 50,000 g/mol, an acrylic-maleic acid copolymer or salt thereof having a molecular weight of between about 1,000 and about 100,000 g/mol and a phosphonocarboxylic acid or salt thereof. A ratio of acrylic-maleic acid copolymer or salt thereof to polyacrylic acid or salt thereof to phosphonocarboxylic acid or salt thereof in parts per million is about 1-30:10-80:6-20.

    摘要翻译： 水硬度控制剂包括分子量为约1,000至约50,000g / mol的聚丙烯酸或其盐，分子量为约1,000至约100,000g / mol的丙烯酸 - 马来酸共聚物或其盐 和膦酰基羧酸或其盐。 丙烯酸 - 马来酸共聚物或其盐与聚丙烯酸或其盐与膦酰基羧酸或其盐的百万分之比为约1-30:1-80:6-20。

    Solidification matrix comprising phosphinosuccinic acid derivatives
    8.
    发明授权
    Solidification matrix comprising phosphinosuccinic acid derivatives 有权
    包含膦基琥珀酸衍生物的凝固基质

    公开(公告)号：US08748365B2

    公开(公告)日：2014-06-10

    申请号：US13614150

    申请日：2012-09-13

    申请人： Erik C. Olson ,  Carter M. Silvernail

    发明人： Erik C. Olson ,  Carter M. Silvernail

    IPC分类号： C11D17/00 ,  C11D11/00 ,  C11D3/36 ,  C11D3/10

    CPC分类号： C11D3/365 ,  C11D3/10 ,  C11D17/0047

    摘要： Stability enhancement agents for use in a solidification matrices and solid detergent compositions are described. Stability enhancement is provided by a hydratable salt, water and phosphinosuccinic acid (PSO) derivative binding agents forming a dimensionally stable composition. Preferred phosphinosuccinic acid (PSO) derivatives include phosphinosuccinic acid and mono-, bis- and oligomeric phosphinosuccinic acid (PSO) derivatives. The stability enhancement composition for use in a solid detergent and solid detergent compositions are preferably biodegradable and substantially free of phosphate and NTA-free.

    摘要翻译： 描述了用于固化基质和固体洗涤剂组合物的稳定性增强剂。 通过形成尺寸稳定的组合物的可水合盐，水和次膦酸琥珀酸（PSO）衍生物结合剂提供稳定性增强。 优选的次膦酸琥珀酸（PSO）衍生物包括膦基琥珀酸和单 - ，双 - 和低聚膦酰基琥珀酸（PSO）衍生物。 用于固体洗涤剂和固体洗涤剂组合物的稳定性增强组合物优选是可生物降解的并且基本上不含磷酸盐和不含NTA。

    SOLIDIFICATION MATRIX COMPRISING PHOSPHINOSUCCINIC ACID DERIVATIVES
    9.
    发明申请
    SOLIDIFICATION MATRIX COMPRISING PHOSPHINOSUCCINIC ACID DERIVATIVES 有权

    公开(公告)号：US20140073550A1

    公开(公告)日：2014-03-13

    申请号：US13614150

    申请日：2012-09-13

    申请人： Erik C. Olson ,  Carter M. Silvernail

    发明人： Erik C. Olson ,  Carter M. Silvernail

    IPC分类号： C11D3/60 ,  C11D17/00

    CPC分类号： C11D3/365 ,  C11D3/10 ,  C11D17/0047

    摘要： Stability enhancement agents for use in a solidification matrices and solid detergent compositions are described. Stability enhancement is provided by a hydratable salt, water and phosphinosuccinic acid (PSO) derivative binding agents forming a dimensionally stable composition. Preferred phosphinosuccinic acid (PSO) derivatives include phosphinosuccinic acid and mono-, bis- and oligomeric phosphinosuccinic acid (PSO) derivatives. The stability enhancement composition for use in a solid detergent and solid detergent compositions are preferably biodegradable and substantially free of phosphate and NTA-free.

    Synthesis and applications of amino carboxylates
    10.
    发明授权
    Synthesis and applications of amino carboxylates 有权
    氨基羧酸盐的合成与应用

    公开(公告)号：US08501988B2

    公开(公告)日：2013-08-06

    申请号：US12401715

    申请日：2009-03-11

    申请人： Altony J. Miralles ,  Carter M. Silvernail

    发明人： Altony J. Miralles ,  Carter M. Silvernail

    IPC分类号： C07C229/04

    CPC分类号： C07C227/08 ,  C07C319/12 ,  C07C323/52 ,  C07C229/16 ,  C07C229/24

    摘要： A method of synthesizing carboxylated amines is disclosed. The method comprises reacting a mixture of a potassium salt of either a primary or secondary amine with a potassium salt of a halogenated carboxylic acid wherein the halogenated carboxylic acid is selected from the group consisting of brominated, chlorinated, or iodinated carboxylic acid in the presence of potassium hydroxide, and optionally in heating the reacting mixture; precipitating the potassium salt by optionally chilling the mixture and discarding the precipitate; purifying the carboxylate amine potassium salt from the liquid phase using water soluble alcohol and optionally adding formic acid to obtain the free aminocarboxylic acid and potassium formate. In a preferred embodiment, the halogenated carboxylic acid is chloroacetic acid.

    摘要翻译： 公开了一种合成羧化胺的方法。 该方法包括将伯胺或仲胺的钾盐与卤代羧酸的钾盐的混合物反应，其中卤代羧酸选自溴化，氯化或碘化的羧酸，在 氢氧化钾，任选地加热反应混合物; 通过任选地冷却混合物并抛弃沉淀物沉淀钾盐; 使用水溶性醇从液相中纯化羧酸胺钾盐，并任选加入甲酸得到游离氨基羧酸和甲酸钾。 在优选的实施方案中，卤代羧酸是氯乙酸。