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    Depositing nanometer-sized particles of metals onto carbon allotropes
    4.
    发明授权
    Depositing nanometer-sized particles of metals onto carbon allotropes 有权
    将纳米尺寸的金属颗粒沉积在碳同素异形体上

    公开(公告)号：US07704553B2

    公开(公告)日：2010-04-27

    申请号：US11710386

    申请日：2007-02-23

    申请人： Kent A. Watson ,  Michael J. Fallbach ,  Sayata Ghose ,  Joseph G. Smith ,  Donavon M. Delozier ,  John W. Connell

    发明人： Kent A. Watson ,  Michael J. Fallbach ,  Sayata Ghose ,  Joseph G. Smith ,  Donavon M. Delozier ,  John W. Connell

    IPC分类号： B05D7/00 ,  B05D3/02

    CPC分类号： C08J5/005 ,  B22F1/0018 ,  B22F9/20 ,  B22F2999/00 ,  B82Y30/00 ,  B82Y40/00 ,  C01B32/05 ,  C01B32/152 ,  C01B32/168 ,  C01B32/20 ,  C01B32/25 ,  C01B2202/02 ,  C01B2202/06 ,  C22C2026/001 ,  C22C2026/002 ,  Y10T428/31678 ,  B22F9/04 ,  B22F2203/11

    摘要： A process for depositing nanometer-sized metal particles onto a substrate in the absence of aqueous solvents, organic solvents, and reducing agents, and without any required pre-treatment of the substrate, includes preparing an admixture of a metal compound and a substrate by dry mixing a chosen amount of the metal compound with a chosen amount of the substrate; and supplying energy to the admixture in an amount sufficient to deposit zero valance metal particles onto the substrate. This process gives rise to a number of deposited metallic particle sizes which may be controlled. The compositions prepared by this process are used to produce polymer composites by combining them with readily available commodity and engineering plastics. The polymer composites are used as coatings, or they are used to fabricate articles, such as free-standing films, fibers, fabrics, foams, molded and laminated articles, tubes, adhesives, and fiber reinforced articles. These articles are well-suited for many applications requiring thermal conductivity, electrical conductivity, antibacterial activity, catalytic activity, and combinations thereof.

    摘要翻译： 在不含水溶剂，有机溶剂和还原剂的情况下将纳米尺寸金属颗粒沉积到基底上的方法，并且不需要对基底进行任何必要的预处理，包括通过干燥制备金属化合物和基底的混合物 将选定量的金属化合物与选定量的底物混合; 并且以足以将零价金属颗粒沉积到基底上的量向混合物供应能量。 该方法产生可以控制的多个沉积的金属颗粒尺寸。 通过该方法制备的组合物用于通过将它们与容易获得的商品和工程塑料组合来生产聚合物复合材料。 聚合物复合材料用作涂层，或者它们用于制造制品，例如自立膜，纤维，织物，泡沫，模制和层压制品，管，粘合剂和纤维增强制品。 这些制品非常适用于需要导热性，导电性，抗菌活性，催化活性及其组合的许多应用。

    Combination structural support and thermal protection system
    7.
    发明申请
    Combination structural support and thermal protection system 有权
    组合结构支撑和热保护系统

    公开(公告)号：US20090022977A1

    公开(公告)日：2009-01-22

    申请号：US12174360

    申请日：2008-07-16

    申请人： Kenneth L. Dudley ,  Holly A. Elliott ,  John W. Connell ,  Joseph G. Smith ,  Sayata Ghose ,  Kent A. Watson ,  Donavon Mark Delozier

    发明人： Kenneth L. Dudley ,  Holly A. Elliott ,  John W. Connell ,  Joseph G. Smith ,  Sayata Ghose ,  Kent A. Watson ,  Donavon Mark Delozier

    IPC分类号： B32B5/16 ,  C08K3/08

    CPC分类号： C08K3/08 ,  B82Y30/00 ,  C08K2201/011

    摘要： A dielectric material includes a network of nanosubstrates, such as but not limited to nanotubes, nanosheets, or other nanomaterials or nanostructures, a polymer base material or matrix, and nanoparticles constructed at least partially of an elemental metal. The network has a predetermined nanosubstrate loading percentage by weight with respect to a total weight of the dielectric material, and a preferential or predetermined longitudinal alignment with respect to an orientation of an incident electrical field. A method of forming the dielectric material includes depositing the metal-based nanoparticles onto the nanosubstrates and subsequently mixing these with a polymer matrix. Once mixed, alignment can be achieved by melt extrusion or a similar mechanical shearing process. Alignment of the nanosubstrate may be in horizontal or vertical direction with respect to the orientation of an incident electrical field.

    摘要翻译： 电介质材料包括纳米基层网络，例如但不限于纳米管，纳米片或其它纳米材料或纳米结构，聚合物基材或基体，以及至少部分由元素金属构成的纳米颗粒。 网络具有相对于电介质材料的总重量的预定的纳米基质载荷百分比，以及相对于入射电场的取向的优选或预定的纵向对准。 形成电介质材料的方法包括将金属基纳米颗粒沉积到纳米基板上，随后将其与聚合物基体混合。 一旦混合，可以通过熔体挤出或类似的机械剪切工艺来实现对准。 纳米基板的对准可以相对于入射电场的取向在水平或垂直方向上。

    Tailorable dielectric material with complex permittivity characteristics
    8.
    发明授权
    Tailorable dielectric material with complex permittivity characteristics 有权
    具有复介电常数特性的可调电介质材料

    公开(公告)号：US08790773B2

    公开(公告)日：2014-07-29

    申请号：US12174360

    申请日：2008-07-16

    申请人： Kenneth L. Dudley ,  Holly A Elliott ,  John W. Connell ,  Joseph G. Smith ,  Sayata Ghose ,  Kent A. Watson ,  Donavon Mark Delozier

    发明人： Kenneth L. Dudley ,  Holly A Elliott ,  John W. Connell ,  Joseph G. Smith ,  Sayata Ghose ,  Kent A. Watson ,  Donavon Mark Delozier

    IPC分类号： B32B5/16 ,  C08K3/08

    CPC分类号： C08K3/08 ,  B82Y30/00 ,  C08K2201/011

    摘要： A dielectric material includes a network of nanosubstrates, such as but not limited to nanotubes, nanosheets, or other nanomaterials or nanostructures, a polymer base material or matrix, and nanoparticles constructed at least partially of an elemental metal. The network has a predetermined nanosubstrate loading percentage by weight with respect to a total weight of the dielectric material, and a preferential or predetermined longitudinal alignment with respect to an orientation of an incident electrical field. A method of forming the dielectric material includes depositing the metal-based nanoparticles onto the nanosubstrates and subsequently mixing these with a polymer matrix. Once mixed, alignment can be achieved by melt extrusion or a similar mechanical shearing process. Alignment of the nanosubstrate may be in horizontal or vertical direction with respect to the orientation of an incident electrical field.

    摘要翻译： 电介质材料包括纳米基层网络，例如但不限于纳米管，纳米片或其它纳米材料或纳米结构，聚合物基材或基体，以及至少部分由元素金属构成的纳米颗粒。 网络具有相对于电介质材料的总重量的预定的纳米基质载荷百分比，以及相对于入射电场的取向的优选或预定的纵向对准。 形成电介质材料的方法包括将金属基纳米颗粒沉积到纳米基板上，随后将其与聚合物基体混合。 一旦混合，可以通过熔体挤出或类似的机械剪切工艺来实现对准。 纳米基板的对准可以相对于入射电场的取向在水平或垂直方向上。

    Composition of and method for making high performance resins for infusion and transfer molding processes
    9.
    发明授权
    Composition of and method for making high performance resins for infusion and transfer molding processes 有权
    用于制备用于输液和传递模塑工艺的高性能树脂的组合物和方法

    公开(公告)号：US06359107B1

    公开(公告)日：2002-03-19

    申请号：US09575826

    申请日：2000-05-18

    申请人： John W. Connell ,  Joseph G. Smith ,  Paul M. Hergenrother

    发明人： John W. Connell ,  Joseph G. Smith ,  Paul M. Hergenrother

    IPC分类号： C08G7310

    CPC分类号： C09J179/08 ,  C08G73/101 ,  C08G73/1014 ,  C08G73/1042 ,  C09D179/08 ,  Y10S526/935 ,  Y10T428/2969 ,  Y10T428/31504 ,  Y10T428/31721

    摘要： A composition of and method for making high performance imide resins that are processable by resin transfer molding (RTM) and resin infusion (RI) techniques were developed. Materials with a combination of properties, making them particularly useful for the fabrication of composite parts via RTM and/or RI processes, were prepared, characterized and fabricated into moldings and carbon fiber reinforced composites and their mechanical properties were determined. These materials are particularly useful for the fabrication of structural composite components for aerospace applications. The method for making high performance resins for RTM and RI processes is a multi-faceted approach. It involves the preparation of a mixture of products from a combination of aromatic diamines and aromatic dianhydrides at relatively low calculated molecular weights (i.e. high stoichiometric offsets) and endcapping with latent reactive groups. The combination of these monomers results in a mixture of products, in the imide form, that exhibits a stable melt viscosity of less than approximately 60 poise below approximately 300° C.

    摘要翻译： 开发了可通过树脂传递模塑（RTM）和树脂浸渍（RI）技术加工的制备高性能酰亚胺树脂的组合物和方法。 制备具有组合性能的材料，使其对于通过RTM和/或RI工艺制造复合材料部分特别有用，其特征和制造成模制品和碳纤维增强复合材料，并确定其机械性能。 这些材料对于制造用于航空航天应用的结构复合材料部件特别有用。 用于制造RTM和RI工艺的高性能树脂的方法是一种多方面的方法。 它涉及以相当低的计算分子量（即高化学计量偏移）和具有潜在反应性基团的封端物从芳族二胺和芳族二酸酐的组合制备产物的混合物。 这些单体的组合产生了酰亚胺形式的产物的混合物，其在约300℃以下显示出小于约60泊的稳定的熔融粘度。

    Anisotropic Copoly(imide Oxetane) Coatings and Articles of Manufacture, Copoly(imide Oxetane)s Containing Pendant Fluorocarbon Moieties, Oligomers and Processes Therefor
    10.
    发明申请
    Anisotropic Copoly(imide Oxetane) Coatings and Articles of Manufacture, Copoly(imide Oxetane)s Containing Pendant Fluorocarbon Moieties, Oligomers and Processes Therefor 有权
    各向异性共聚（酰亚胺氧杂环丁烷）涂料及其制造方法，含有侧链碳氟化合物部分，低聚物及其工艺的共聚（酰亚胺氧杂环丁烷）

    公开(公告)号：US20120252968A1

    公开(公告)日：2012-10-04

    申请号：US13286715

    申请日：2011-11-01

    申请人： Christopher J. Wohl ,  John W. Connell ,  Emilie J. Siochi ,  Joseph G. Smith

    发明人： Christopher J. Wohl ,  John W. Connell ,  Emilie J. Siochi ,  Joseph G. Smith

    IPC分类号： C09D167/00 ,  B05D3/00 ,  C07D305/08 ,  B05D7/24 ,  C08G63/682 ,  C08L67/00

    CPC分类号： C07D305/08 ,  C08G65/18 ,  C08G65/322 ,  C08G65/33389 ,  C08G73/1042 ,  C08G73/105 ,  C09D179/08

    摘要： Copoly(imide oxetane) materials are disclosed that can exhibit a low surface energy while possessing the mechanical, thermal, chemical and optical properties associated with polyimides. The copoly(imide oxetane)s are prepared using a minor amount of fluorinated oxetane-derived oligomer with sufficient fluorine-containing segments of the copoly(imide oxetane)s that migrate to the exterior surface of the polymeric material to yield low surface energies. Thus the coatings and articles of manufacture made with the copoly(imide oxetane)s of this invention are characterized as having an anisotropic fluorine composition. The low surface energies can be achieved with very low content of fluorinated oxetane-derived oligomer. The copolymers of this invention can enhance the viability of polyimides for many applications and may be acceptable where homopolyimide materials have been unacceptable.

    摘要翻译： 公开了共聚（酰亚胺氧杂环丁烷）材料，其具有低表面能，同时具有与聚酰亚胺相关的机械，热学，化学和光学性能。 使用少量的具有足够的共聚（酰亚胺氧杂环丁烷）的含氟链段的氟化氧杂环丁烷衍生的低聚物制备共聚（酰亚胺氧杂环丁烷），其迁移到聚合物材料的外表面以产生低的表面能。 因此，用本发明的共聚（酰亚胺氧杂环丁烷）制备的涂料和制品被表征为具有各向异性氟组合物。 低表面能可以用非常低含量的氟化氧乙烷衍生的低聚物来实现。 本发明的共聚物可以增强聚酰亚胺在许多应用中的存活力，并且在均聚酰亚胺材料已经不可接受的情况下可以是可接受的。