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公开(公告)号：US5420312A
公开(公告)日：1995-05-30
申请号：US979011
申请日：1992-11-20
IPC分类号： C07B61/00 , C07D301/28 , C07D303/22 , C07D303/24 , C07D405/14 , C08G59/04 , C07D303/12 , C07D303/27
CPC分类号： C07D303/22 , C07D303/24 , C07D405/14 , C08G59/04
摘要： A process for the production of glycidyl ether of an aliphatic, cycloaliphatic or araliphatic primary or secondary alcohol, comprising:A) reacting epichlorohydrin with a molar excess of the alcohol in the presence of a Lewis acid catalyst; optionallyB) dehydrochlorinating the product so obtained; andC) reacting the product from step A) or B) with a molar excess of epichlorohydrin in the presence of alkali and a phase transfer catalyst, and then isolating the glycidyl ether product so obtained.
摘要翻译： 一种制备脂肪族，脂环族或芳脂族伯或仲醇的缩水甘油醚的方法，包括：A）在路易斯酸催化剂存在下使表氯醇与摩尔过量的醇反应; 任选地B）如此获得的产物脱氯化氢; 和C）在碱和相转移催化剂存在下使来自步骤A）或B）的产物与摩尔过量的表氯醇反应，然后分离得到的缩水甘油醚产物。
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公开(公告)号：US4933392A
公开(公告)日：1990-06-12
申请号：US376796
申请日：1989-07-07
CPC分类号： C08G59/686 , C08G59/4014 , C08L63/00
摘要： Curable compositions comprise:(A) an epoxide resin(B) as latent curing agent for (A), dicyandiamide or a polycarboxylic acid hydrazide, and(C) as cure accelerator dispersed as a powder in the composition, a Mannich base of a polymeric phenol.The compositions are particularly useful as adhesives and sealants.
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公开(公告)号：US4394492A
公开(公告)日：1983-07-19
申请号：US390466
申请日：1982-06-21
IPC分类号： C08G59/00 , C08G59/40 , C08G59/50 , C08G77/00 , C08G77/48 , C08L63/00 , C08L61/00 , C08L61/06
CPC分类号： C08G59/4085
摘要： Curable compositions contain an epoxide resin and a silamine of the general formula ##STR1## wherein R.sup.1 represents the divalent residue of an aromatic or araliphatic diprimary amine after removal of the two primary amino groups,R.sup.2, R.sup.3, R.sup.4, R.sup.5, and R.sup.6, which may be the same or different, represent alkyl or aryl groups, andn represents zero or an integer of from 1 to 10.These compositions are stable for prolonged periods in the absence of water, but cure rapidly at room temperature or at elevated temperatures in the presence of water.
摘要翻译： 可固化组合物含有环氧化物树脂和通式为“IMAGE”的硅烷，其中R1表示除去两个伯氨基R2，R3，R4，R5和R6之后的芳族或芳脂族二元胺的二价残基， 可以相同或不同，表示烷基或芳基，n表示0或1-10的整数。这些组合物在不存在水的情况下长时间稳定，但在室温或高温下快速固化 水的存在。
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公开(公告)号：US5270120A
公开(公告)日：1993-12-14
申请号：US914488
申请日：1992-07-14
CPC分类号： B42D25/47 , B32B27/08 , B32B7/12 , B42D25/00 , Y10T428/3188
摘要： A data-carrying laminate such as a credit card or identity card comprises a sheet of cellulosic material or synthetic material and a thermoplastic polymeric film, at least one of said sheet and said thermoplastic film carrying data, said sheet and said thermoplastic film being bonded together by a cured adhesive layer obtained by curing a solid film adhesive comprising (A) a solid polymer of a vinyl carboxylic acid and (B) a curable material having at least one acrylate or methacrylate group.
摘要翻译： 诸如信用卡或身份证的数据承载层压板包括一片纤维素材料或合成材料和热塑性聚合物膜，所述片材和所述热塑性薄膜中的至少一个承载数据，所述片材和所述热塑性薄膜粘合在一起 （A）乙烯基羧酸的固体聚合物和（B）具有至少一个丙烯酸酯或甲基丙烯酸酯基团的可固化材料的固体胶粘剂固化的固化粘合剂层。
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公开(公告)号：US4645818A
公开(公告)日：1987-02-24
申请号：US807564
申请日：1985-12-11
CPC分类号： C08G59/4014 , C08G59/4021
摘要： Heat-curable compositions are described, comprising(a) an epoxide resin and(b) an effective amount of a urea of formulaAr--NHCON(R.sup.3)R.sup.4whereAr represents an aromatic group linked through an aromatic carbon atom to the indicated nitrogen atom and which is substituted by an amido group, andR.sup.3 and R.sup.4 each represent an aliphatic, cycloaliphatic, or araliphatic hydrocarbyl group, optionally substituted by a halogen atom or a hydroxyl group, or R.sup.3 may further represent a hydrogen atom, or R.sup.3 nd R.sup.4, together with the indicated nitrogen atom, may represent a heterocyclic ring of 3 to 5 carbon atoms which may also have one oxygen atom in the ring.Such amidoarylureas may be used alone with the epoxide resin, or in combination with an accelerator for the heat-curing reaction, selected from dicyandiamide, carboxylic acid hydrazides, succinimide, cyanoacetamide, 1-cyano-3-(lower alkyl)guanidines, imidazoles, and carboxylic acid-tertiary amine salts.
摘要翻译： 描述了可热固化的组合物，其包含（a）环氧树脂和（b）有效量的式Ar-NHCON（R3）R4的脲，其中Ar表示通过芳族碳原子与指定的氮原子连接的芳族基团 并且其被酰胺基取代，并且R 3和R 4各自表示任选被卤素原子或羟基取代的脂族，脂环族或芳脂族烃基，或者R 3可以进一步代表氢原子或R 3和R 4， 与所示的氮原子一起可以表示在环中也可以具有一个氧原子的3至5个碳原子的杂环。 这种酰氨基芳基脲可以与环氧树脂单独使用，或与用于热固化反应的促进剂组合使用，选自双氰胺，羧酸酰肼，琥珀酰亚胺，氰基乙酰胺，1-氰基-3-（低级烷基）胍，咪唑， 和羧酸 - 叔胺盐。
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公开(公告)号：US4431756A
公开(公告)日：1984-02-14
申请号：US430639
申请日：1982-09-30
IPC分类号： C08G59/00 , C08G59/14 , C08K5/5415 , C08L63/00 , C08L77/00 , C09D5/04 , C09D163/00 , C09J163/00 , C08K5/10 , C08K5/16
CPC分类号： C09D5/04 , C09D163/00
摘要： Thixotropic epoxide resin compositions, suitable for use as laminating resins, paints and lacquers, impregnating and casting resins, potting, insulating, and caulking compounds, sealants, and adhesives, are prepared by adding to an epoxide resin(a) a base having a basic strength, pK.sub.b, of 9 or less,(b) an organo-orthosilicate of formula(RO).sub.4 Si where R represents an alkyl group, optionally substituted by one or more halogen atoms or alkoxy groups, an aryl or aralkyl group which may be substituted by one or more halogen atoms, alkyl groups, or alkoxy groups, or a heterocyclylalkyl group, and(c) water.Such compositions may further contain(d) a curing agent for epoxide resins, which agent may be the same as, or different from, the base (a).
摘要翻译： 适用于层压树脂，油漆和漆，浸渍和浇注树脂，灌封，绝缘和填缝化合物，密封剂和粘合剂的触变性环氧树脂组合物通过将环氧树脂（a） 强度，pKb为9以下，（b）式（RO）4Si的有机原硅酸盐，其中R表示任选被一个或多个卤素原子或烷氧基取代的烷基，可被取代的芳基或芳烷基 通过一个或多个卤素原子，烷基或烷氧基或杂环基烷基，和（c）水。 这样的组合物还可以含有（d）环氧树脂的固化剂，该试剂可以与碱（a）相同或不同。
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公开(公告)号：US4507445A
公开(公告)日：1985-03-26
申请号：US538023
申请日：1983-09-30
CPC分类号： C08G59/4021 , C08G59/623 , C08G59/686
摘要： Epoxide resins are cured by heating with a hydroxyphenylurea of formula ##STR1## where R.sup.2 denotes --NH.sub.2, --NO.sub.2, --Cl, --Br, or alkyl, p denotes zero, x and y each denote zero or 1, and the sum of x+y is 1. Such hydroxyphenylureas may be used alone, as accelerators for heat-curing with other agents such as dicyandiamide, melamine, and carboxylic acid hydrazides, or may be used as the primary curing agent with promoters such as dicyandiamide, melamine, and carboxylic hydrazides.
摘要翻译： 环氧树脂通过用式（VI）的羟基苯基脲加成来固化，其中R 2表示-NH 2，-NO 2，-Cl，-Br或烷基，p表示0，x和y各自表示0或1， x + y为1.这样的羟基苯基脲可以单独使用，作为与其它试剂例如双氰胺，三聚氰胺和羧酸酰肼进行热固化的促进剂，或者可以用作主要固化剂，其具有促进剂如双氰胺，三聚氰胺， 和羧酰肼。
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公开(公告)号：US4393180A
公开(公告)日：1983-07-12
申请号：US390468
申请日：1982-06-21
IPC分类号： C09K3/10 , C07F7/10 , C08G59/00 , C08G59/40 , C08G59/42 , C08G59/62 , C08G77/00 , C08G77/48 , C08L63/00 , C08L83/00 , C08L83/04 , C09D163/00 , C09J163/00 , C08L61/00 , C08L61/06
CPC分类号： C08G59/4284 , C07F7/10 , C08G59/4085 , C08G59/62
摘要： Curable compositions contain an epoxide resin and, as curing agent, a mixture of(a) a silamine of the general formula ##STR1## wherein either m represents 1, in which case R.sup.1 represents the divalent residue of an aromatic, aliphatic, araliphatic, or cycloaliphatic diprimary amine after removal of two primary amino groups, and n represents zero or an integer of from 1 to 10, or m represents 2, in which case R.sup.1 represents the trivalent residue of an aliphatic triprimary amine after removal of the three primary amino groups, and n represents zero, andR.sup.2, R.sup.3, R.sup.4, R.sup.5, and R.sup.6, which may be the same or different, represent alkyl or aryl groups, and(b) a substantially anhydrous organic acid or a phenol.These compositions are stable for prolonged periods in the absence of water, but cure rapidly at room temperature or at elevated temperatures in the presence of water, which may be as water vapor or liquid water.
摘要翻译： 可固化组合物含有环氧树脂，和作为固化剂的（a）通式为“IMAGE”的硅烷的混合物，其中m表示1，在这种情况下，R 1表示芳族，脂族，芳脂族或 除去两个伯氨基后的脂环族二元胺，n表示0或1〜10的整数，或m表示2，在这种情况下，R1表示除去三个伯氨基后的脂肪族三原子胺的三价残基 ，n表示0，R 2，R 3，R 4，R 5和R 6可以相同或不同，表示烷基或芳基，（b）基本无水的有机酸或苯酚。 这些组合物在不存在水的情况下长时间稳定，但在室温或高温下在水的存在下快速固化，水可以作为水蒸气或液态水。
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公开(公告)号：US5511898A
公开(公告)日：1996-04-30
申请号：US320295
申请日：1994-10-11
申请人： Martin C. Pettesch , Michael P. Breheny , Christopher M. Andrews , Thomas G. Nelson , Joseph V. Milo
发明人： Martin C. Pettesch , Michael P. Breheny , Christopher M. Andrews , Thomas G. Nelson , Joseph V. Milo
IPC分类号： E02D29/14
CPC分类号： E02D29/1418
摘要： A manhole includes a carriage mounted on the underside of the cover that cooperates with a supporting guide channel located across the mouth of the manhole. the guide channel can be rotated to an incline so that the carriage can easily roll onto and from the supporting guide member. The free end of the guide channel is raised and lowered by a standard ratchet wrench inserted through the cover so that the operator need not lift any part of the cover manually. Once raised to the ready position, the operator simply pulls laterally on the cover handle to roll the cover slightly upward and laterally from the manhole opening. Once the cover clears the manhole, the guide channel can be rotated up and outward to provide access to the entire manhole area , if desired. To replace the cover, the guide channel is rotated to again extend across the manhole, the cover/carriage assembly is rolled laterally on to the guide channel until the cover edge contacts the ring edge. The channel is then lowered with use of the tool to seat the cover on to the manhole ring. The operator at no time manually lifts the cover. The guide channel precisely orients the cover when moved to the closed position.
摘要翻译： 人孔包括安装在盖的下侧上的滑架，其与位于人孔口的支撑引导通道配合。 引导通道可以旋转到倾斜，使得滑架能够容易地滚动到支撑引导构件上和从支撑引导构件滚动。 引导通道的自由端通过插入通过盖的标准棘轮扳手升高和降低，使得操作者不需要手动提起盖的任何部分。 一旦抬起到就绪位置，操作者简单地在盖手柄上侧向拉动，以便从人孔开口稍微向上和向外滚动盖。 一旦盖子清除了检修孔，引导通道可以向上和向外旋转，以便在需要时提供对整个人孔区域的通路。 为了更换盖子，引导通道被旋转以再次延伸穿过人孔，盖/托架组件横向滚动到引导通道，直到盖边缘接触环形边缘。 然后使用工具降低通道，将盖子安放在人孔环上。 操作人员随时手动提起盖子。 当移动到关闭位置时，引导通道精确定位盖。
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10.发明授权
公开(公告)号：US4866133A
公开(公告)日：1989-09-12
申请号：US95725
申请日：1987-09-14
摘要： Curable liquid compositions comprise(A) a liquid epoxide resin and(B) as curing agent for (A), more than 10% by weight, based on the weight of (A), of a solid solution of a polymeric phenol, such as a polymer of p-vinyl phenol or a phenolic novolak resin, and a polyamine having at least one primary amine group, such as diethylenetriamine or triethylenetetramine, the solid solution (B) being disposed as a powder in the epoxide resin. The compositions are useful as adhesives.
摘要翻译： 可固化液体组合物包含（A）液体环氧树脂和（B）作为（A）的固化剂，基于（A）的重量，超过10重量％的聚合苯酚的固溶体，例如 对乙烯基苯酚或酚醛清漆树脂的聚合物和具有至少一个伯胺基团的多胺如二亚乙基三胺或三亚乙基四胺，固溶体（B）作为粉末设置在环氧树脂中。 该组合物可用作粘合剂。
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