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1.发明申请PREPARATION OF PRIMARY DIAMINES HAVING A LINEAR MAIN CHAIN FOR POLYAMIDE SYNTHESES 失效具有聚酰胺合成线性主链的主要原料的制备公开(公告)号：US20120203033A1
公开(公告)日：2012-08-09
申请号：US13364493
申请日：2012-02-02
申请人： Franz-Erich Baumann , Matthias Ullrich , Martin Roos , Peter Hannen , Frank-Martin Petrat , Harald Haeger , Angela Koeckritz , Guido Walther , Jens Deutsch , Andreas Martin
发明人： Franz-Erich Baumann , Matthias Ullrich , Martin Roos , Peter Hannen , Frank-Martin Petrat , Harald Haeger , Angela Koeckritz , Guido Walther , Jens Deutsch , Andreas Martin
IPC分类号： C07C209/16 , C07C209/84
CPC分类号： C07C209/16 , Y02P20/544 , C07C211/09
摘要： The invention provides a method to produce primary diamines by catalytic conversion of diols having a linear main chain of from 4 to 31 carbon atoms into the corresponding diamines. The reaction is conducted in a liquid or supercritical phase and is catalyzed by a homogeneous ruthenium-containing complex. The primary diamines obtained may be suitable for polyamide syntheses.
摘要翻译： 本发明提供了通过将具有4至31个碳原子的直链主链的二醇催化转化成相应的二胺来生产伯胺的方法。 该反应在液相或超临界相中进行，并由均匀的含钌络合物催化。 所得到的伯胺可适用于聚酰胺合成。
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2.发明授权Preparation of primary diamines having a linear main chain for polyamide syntheses 失效制备具有聚酰胺合成线性主链的伯二胺公开(公告)号：US08642811B2
公开(公告)日：2014-02-04
申请号：US13364493
申请日：2012-02-02
申请人： Franz-Erich Baumann , Matthias Ullrich , Martin Roos , Peter Hannen , Frank-Martin Petrat , Harald Haeger , Angela Koeckritz , Guido Walther , Jens Deutsch , Andreas Martin
发明人： Franz-Erich Baumann , Matthias Ullrich , Martin Roos , Peter Hannen , Frank-Martin Petrat , Harald Haeger , Angela Koeckritz , Guido Walther , Jens Deutsch , Andreas Martin
IPC分类号： C07C209/16
CPC分类号： C07C209/16 , Y02P20/544 , C07C211/09
摘要： The invention provides a method to produce primary diamines by catalytic conversion of diols having a linear main chain of from 4 to 31 carbon atoms into the corresponding diamines. The reaction is conducted in a liquid or supercritical phase and is catalyzed by a homogeneous ruthenium-containing complex. The primary diamines obtained may be suitable for polyamide syntheses.
摘要翻译： 本发明提供了通过将具有4至31个碳原子的直链主链的二醇催化转化成相应的二胺来生产伯胺的方法。 该反应在液相或超临界相中进行，并由均匀的含钌络合物催化。 所得到的伯胺可适用于聚酰胺合成。
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公开(公告)号：US08604227B2
公开(公告)日：2013-12-10
申请号：US13634111
申请日：2010-11-19
申请人： Frank-Martin Petrat , Franz-Erich Baumann , Harald Haeger , Guido Walther , Andreas Martin , Angela Koeckritz
发明人： Frank-Martin Petrat , Franz-Erich Baumann , Harald Haeger , Guido Walther , Andreas Martin , Angela Koeckritz
IPC分类号： C07C51/10
摘要： The invention provides a process for preparing linear alpha,omega-dicarboxylic diesters by reacting a triglyceride containing fatty acid residues having monounsaturated or polyunsaturated carbon chains with carbon monoxide, an acid and an OH-group donor in one reaction step in the presence of a catalyst.
摘要翻译： 本发明提供了通过在一个反应步骤中在催化剂存在下使含有单不饱和或多不饱和碳链的脂肪酸残基与一氧化碳，酸和OH-给体的甘油三酯反应制备线性α，ω-二羧酸二酯的方法 。
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公开(公告)号：US20130006005A1
公开(公告)日：2013-01-03
申请号：US13634111
申请日：2010-11-19
申请人： Frank-Martin Petrat , Franz-Erich Baumann , Harald Haeger , Guido Walther , Andreas Martin , Angela Koeckritz
发明人： Frank-Martin Petrat , Franz-Erich Baumann , Harald Haeger , Guido Walther , Andreas Martin , Angela Koeckritz
IPC分类号： C07C67/36
摘要： The invention provides a process for preparing linear alpha,omega-dicarboxylic diesters by reacting a triglyceride containing fatty acid residues having monounsaturated or polyunsaturated carbon chains with carbon monoxide, an acid and an OH-group donor in one reaction step in the presence of a catalyst.
摘要翻译： 本发明提供了通过在一个反应步骤中在催化剂存在下使含有单不饱和或多不饱和碳链的脂肪酸残基与一氧化碳，酸和OH-给体的甘油三酯反应制备线性α，ω-二羧酸二酯的方法 。
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5.发明授权Molding compound on the basis of a copolyamide containing terephthalic acid and trimethylhexamethylene diamine units 有权基于含有对苯二甲酸和三甲基六亚甲基二胺单元的共聚酰胺的成型化合物公开(公告)号：US08871862B2
公开(公告)日：2014-10-28
申请号：US13377949
申请日：2010-07-08
CPC分类号： C08G69/265 , C08L77/06
摘要： A molding compound, containing at least 30% by weight of a copolyamide, which is derived from the following monomers: a) 50 to 95 mole percent of the combination of a diamine, selected from the group consisting of 1,9-nonane diamine, 1,10-decane diamine, 1,11-undecane diamine and 1,12-dodecane diamine, and terephthalic acid, and b) 5 to 50 mole percent of the combination of a diamine, selected from the group consisting of 2,2,4-trimethylhexamethylene diamine, 2,4,4-trimethylhexamethylene diamine, and mixtures thereof, and terephthalic acid. The copolyamide is crystalline and has low water absorption.
摘要翻译： 含有至少30重量％的共聚酰胺的模制化合物，其衍生自以下单体：a）50-95摩尔％的二胺的组合，其选自1,9-壬二胺， 1,10-癸烷二胺，1,11-十一烷二胺和1,12-十二烷二胺和对苯二甲酸，以及b）5至50摩尔％的二胺的组合，其选自2,2， 4-三甲基六亚甲基二胺，2,4,4-三甲基六亚甲基二胺及其混合物和对苯二甲酸。 共聚酰胺是结晶的，吸水率低。
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6.发明申请MOLDING COMPOUND ON THE BASIS OF A COPOLYAMIDE CONTAINING TEREPHTHALIC ACID AND TRIMETHYLHEXAMETHYLENE DIAMINE UNITS 有权含有十五烷酸和三甲基乙酰胺二胺单体的共聚酰胺的成型化合物公开(公告)号：US20120095161A1
公开(公告)日：2012-04-19
申请号：US13377949
申请日：2010-07-08
CPC分类号： C08G69/265 , C08L77/06
摘要： A molding compound, containing at least 30% by weight of a copolyamide, which is derived from the following monomers: a) 50 to 95 mole percent of the combination of a diamine, selected from the group consisting of 1,9-nonane diamine, 1,10-decane diamine, 1,11-undecane diamine and 1,12-dodecane diamine, and terephthalic acid, and b) 5 to 50 mole percent of the combination of a diamine, selected from the group consisting of 2,2,4-trimethylhexamethylene diamine, 2,4,4-trimethylhexamethylene diamine, and mixtures thereof, and terephthalic acid. The copolyamide is crystalline and has low water absorption.
摘要翻译： 含有至少30重量％的共聚酰胺的模制化合物，其衍生自以下单体：a）50-95摩尔％的二胺的组合，其选自1,9-壬二胺， 1,10-癸烷二胺，1,11-十一烷二胺和1,12-十二烷二胺和对苯二甲酸，以及b）5至50摩尔％的二胺的组合，其选自2,2， 4-三甲基六亚甲基二胺，2,4,4-三甲基六亚甲基二胺及其混合物和对苯二甲酸。 共聚酰胺是结晶的，吸水率低。
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7.发明申请UNSATURATED DICARBOXYLIC ACIDS FROM UNSATURATED CYCLIC HYDROCARBONS AND ACRYLIC ACID BY WAY OF METATHESIS, THE USE THEREOF AS MONOMERS FOR POLYAMIDES, POLYESTERS AND POLYURETHANES, AND SUBSEQUENT REACTION TO DIOLS AND DIAMINES 失效不饱和二羧酸由不饱和环状烃和丙烯酸通过METATHESIS的方式，其作为聚合物，聚酯和聚氨酯的单体使用，以及后续反应与DIAMINES公开(公告)号：US20100312012A1
公开(公告)日：2010-12-09
申请号：US12865018
申请日：2009-04-17
申请人： Peter Hannen , Martin Roos , Harald Haeger
发明人： Peter Hannen , Martin Roos , Harald Haeger
CPC分类号： C07C51/43 , C07C51/353 , C07C51/44 , C07C57/13
摘要： The invention relates to a method for producing α/β-unsaturated dicarboxylic acids and the corresponding saturated dicarboxylic acids, whereby the corresponding cycloalkene and acrylic acid are reacted with a ruthenium catalyst by way of a metathesis reaction at high substrate concentrations until the reaction takes place in substance, the resulting dicarboxylic acid being precipitated.
摘要翻译： 本发明涉及一种生产α/β-不饱和二羧酸和相应的饱和二羧酸的方法，其中相应的环烯烃和丙烯酸通过在高底物浓度下的复分解反应与钌催化剂反应，直到反应 置于物质中，所得二羧酸沉淀。
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8.发明申请SYNTHESIS OF ALPHA,OMEGA-DICARBOXYLIC ACIDS AND ESTERS THEREOF FROM UNSATURATED FATTY ACID DERIVATIVES 失效从不饱和脂肪酸衍生物合成ALPHA，欧米二酸和其酯公开(公告)号：US20120245375A1
公开(公告)日：2012-09-27
申请号：US13424548
申请日：2012-03-20
申请人： Peter HANNEN , Harald Haeger , Martin Roos
发明人： Peter HANNEN , Harald Haeger , Martin Roos
IPC分类号： C07C67/44
CPC分类号： C07C67/333 , C07C51/285 , C07C51/34 , C07C51/373 , C07C67/313 , C07C69/48 , C07C69/716 , C07C53/126 , C07C59/147 , C07C55/02
摘要： A process for preparing an alpha, omega-dicarboxylic acid or an ester thereof, which includes (a) subjecting at least one unsaturated fatty acid or fatty acid derivative to ozonolysis to obtain an ozonolysis reaction mixture; and (b) oxidizing the ozonolysis reaction mixture with an oxidizing agent in the presence of an acid catalyst to obtain an oxidized reaction mixture comprising at least one alpha, omega-dicarboxylic acid or ester; wherein the process is performed using a solvent and the acid catalyst has a pKa of less than or equal to zero, as measured at 25° C.
摘要翻译： 一种制备α，ω-二羧酸或其酯的方法，其包括（a）使至少一种不饱和脂肪酸或脂肪酸衍生物进行臭氧分解以获得臭氧分解反应混合物; 和（b）在酸催化剂存在下用氧化剂氧化臭氧分解反应混合物，得到包含至少一种α，ω-二羧酸或酯的氧化反应混合物; 其中所述方法使用溶剂进行，并且所述酸催化剂的pKa小于或等于零，如在25℃下测量的。
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9.发明申请METHOD FOR PRODUCING DODECA-2,10-DIENE-1,12-DICARBOXYLIC ACID OR 1,12-DODECANE-DICARBOXYLIC ACID BY WAY OF RING-OPENING CROSS METATHESIS (ROCM) OF CYCLOOCTENE WITH ACRYLIC ACID 有权通过旋转开环方式通过丙烯酸的环己烷的交联（ROCM）方法生产多卡那-2,10-二烯-1,12-二羧酸或1,12-十二烷基二羧酸的方法公开(公告)号：US20110015434A1
公开(公告)日：2011-01-20
申请号：US12922807
申请日：2009-04-16
申请人： Peter Hannen , Martin Roos , Harald Haeger
发明人： Peter Hannen , Martin Roos , Harald Haeger
IPC分类号： C07C51/36 , C07C51/347
摘要： The invention relates to a method for producing 1,2-dodeca-2,10-diene diacid and 1,12-dodecanoic acid whereby cyclooctene and acrylic acid are reacted with a ruthenium catalyst by way of a metathesis reaction at high substrate concentrations until the reaction takes place in substance, the resulting unsaturated dicarboxylic acid being precipitated and being hydrated in a second reaction step.
摘要翻译： 本发明涉及一种1,2-十二碳-2,10-二烯二酸和1,12-十二烷酸的制备方法，其中环辛烯和丙烯酸通过在高底物浓度下的复分解反应与钌催化剂反应，直到 反应发生在物质中，所得的不饱和二羧酸在第二反应步骤中沉淀并水合。
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10.发明授权Synthesis of alpha,omega-dicarboxylic acids and esters thereof from unsaturated fatty acid derivatives 失效从不饱和脂肪酸衍生物合成α，ω-二羧酸及其酯公开(公告)号：US08703993B2
公开(公告)日：2014-04-22
申请号：US13424548
申请日：2012-03-20
申请人： Peter Hannen , Harald Haeger , Martin Roos
发明人： Peter Hannen , Harald Haeger , Martin Roos
IPC分类号： C07C69/48
CPC分类号： C07C67/333 , C07C51/285 , C07C51/34 , C07C51/373 , C07C67/313 , C07C69/48 , C07C69/716 , C07C53/126 , C07C59/147 , C07C55/02
摘要： A process for preparing an alpha, omega-dicarboxylic acid or an ester thereof, which includes (a) subjecting at least one unsaturated fatty acid or fatty acid derivative to ozonolysis to obtain an ozonolysis reaction mixture; and (b) oxidizing the ozonolysis reaction mixture with an oxidizing agent in the presence of an acid catalyst to obtain an oxidized reaction mixture comprising at least one alpha, omega-dicarboxylic acid or ester; wherein the process is performed using a solvent and the acid catalyst has a pKa of less than or equal to zero, as measured at 25° C.
摘要翻译： 一种制备α，ω-二羧酸或其酯的方法，其包括（a）使至少一种不饱和脂肪酸或脂肪酸衍生物进行臭氧分解以获得臭氧分解反应混合物; 和（b）在酸催化剂存在下用氧化剂氧化臭氧分解反应混合物，得到包含至少一种α，ω-二羧酸或酯的氧化反应混合物; 其中所述方法使用溶剂进行，并且所述酸催化剂的pKa小于或等于零，如在25℃下测量的。
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