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1.发明申请METHODS AND APPARATUS FOR CROSSLINKING A SILICON CARBIDE FIBER PRECURSOR POLYMER 有权用于交联硅碳纤维前体聚合物的方法和装置公开(公告)号：US20150018448A1
公开(公告)日：2015-01-15
申请号：US13937298
申请日：2013-07-09
CPC分类号： C08G77/62 , B01J19/085 , B01J19/087 , B01J2219/0803 , B01J2219/0879 , B29C35/0866 , B29C2035/0877 , C04B35/571 , C04B35/62281 , C08G77/60 , C08J3/28 , D01D10/00 , D01F9/10 , D01F11/08 , D01F11/16 , D06M10/008
摘要： The present disclosure generally provides methods and apparatus for efficiently crosslinking silicon carbide fiber precursor polymers with electron beam radiation. The methods and apparatus utilize a platform containing silicon carbide fiber precursor polymer. The temperature of the platform is regulated while the silicon carbide fiber precursor polymer is irradiated to thereby regulate the temperature of the irradiated silicon carbide fiber precursor polymer thereon. In this way, the temperature of the irradiated silicon carbide fiber precursor polymer is regulated via the platform both during and after it is subjected to radiation. At least one of the platform and the e-beam radiation mechanism may be translated with respect to the other to irradiate different portions of the silicon carbide fiber precursor polymer and, ultimately, the entirety of the silicon carbide fiber precursor polymer contained on the platform.
摘要翻译： 本发明通常提供了用电子束辐射有效交联碳化硅纤维前体聚合物的方法和装置。 该方法和装置利用含有碳化硅纤维前体聚合物的平台。 调节平台的温度，同时照射碳化硅纤维前体聚合物，从而调节照射的碳化硅纤维前体聚合物的温度。 以这种方式，照射的碳化硅纤维前体聚合物的温度在经受辐射之后和之后通过平台调节。 平台和电子束辐射机构中的至少一个可以相对于另一平台和电子束辐射机构平移以照射碳化硅纤维前体聚合物的不同部分，最终照射包含在平台上的整个碳化硅纤维前体聚合物。
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2.发明申请METHOD FOR CURING OF GREEN POLYSILAZANE-BASED SILICON CARBIDE PRECURSOR FIBERS 有权用于固化绿色聚硅氧烷碳化物前体纤维的方法公开(公告)号：US20150247265A1
公开(公告)日：2015-09-03
申请号：US14193158
申请日：2014-02-28
IPC分类号： D01F11/08
CPC分类号： D01F11/08 , C04B35/571 , C04B35/62281 , C04B35/6269 , C04B35/62844 , C04B2235/444 , C04B2235/483 , C04B2235/5264 , C04B2235/666 , C08G77/62 , C08J3/243 , C08J2383/16 , D01D10/02 , D01F6/94 , D01F9/10 , D10B2331/30
摘要： Disclosed herein are methods of curing silicon carbide precursor polymer fibers, such as polysilazanes, using moisture and free radical generators, such as peroxides. Also disclosed are methods of forming, curing, and using silicon carbide precursor polymers that contain alkenyl groups and free radical generators, such as peroxides.
摘要翻译： 本文公开了使用水分和自由基发生剂如过氧化物固化碳化硅前体聚合物纤维如聚硅氮烷的方法。 还公开了形成，固化和使用含有烯基的碳化硅前体聚合物和自由基发生剂如过氧化物的方法。
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3.发明申请METHODS OF USING BORON-CONTAINING ADDITIVES AS SILICON CARBIDE CROSSLINKING AGENTS 有权使用含硼添加剂作为碳化硅交联剂的方法公开(公告)号：US20140353868A1
公开(公告)日：2014-12-04
申请号：US13905732
申请日：2013-05-30
CPC分类号： C08G77/54 , C01B32/956 , C04B35/62281 , C04B35/62295 , C04B35/6269 , C04B2235/3409 , C04B2235/483 , C04B2235/5264 , C04B2235/9661 , C08G77/60 , C08G77/62 , D01F9/10
摘要： The present disclosure generally relates to methods of using boron-containing additives for crosslinking polysilazane green fibers, which are precursors to silicon carbide fibers. These methods provide a controllable process for crosslinking silicon carbide fibers while providing a simple way for the introduction of boron as a sintering aid into the polymer structure.
摘要翻译： 本公开一般涉及使用含硼添加剂交联聚硅氮烷绿纤维的方法，聚硅氮烷绿纤维是碳化硅纤维的前体。 这些方法提供了一种用于交联碳化硅纤维的可控制法，同时提供了将硼作为烧结助剂引入聚合物结构中的简单方法。
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