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    Products of the condensation of phenolmonosulfonic acids, dihydroxydiphenyl sulfones, urea and formaldehyde
    4.
    发明授权
    Products of the condensation of phenolmonosulfonic acids, dihydroxydiphenyl sulfones, urea and formaldehyde 失效
    苯二酚酸，二羟基二苯基硫醚，尿素和甲醛的浓缩产物

    公开(公告)号：US5155164A

    公开(公告)日：1992-10-13

    申请号：US696912

    申请日：1991-05-08

    申请人： Hermann Graf ,  Adolf Stuebinger ,  Klaus Lorenz ,  Ortwin Schaffer ,  Karl Stork

    发明人： Hermann Graf ,  Adolf Stuebinger ,  Klaus Lorenz ,  Ortwin Schaffer ,  Karl Stork

    IPC分类号： C08G14/02

    CPC分类号： C08G14/02

    摘要： Products of the condensation of phenolmonosulfonic acids, dihydroxydiphenyl sulfones, urea and formaldehyde can be obtained by(A) preparing a homogeneous reaction mixture in sulfuric acid from the phenolmonosulfonic acid and dihydroxydiphenyl sulfone in the molar ratio of from 3:1 to 10:1, with the proviso that the water content of the mixture is not more than 10% of the total weight of the components, and the mixture contains from 0.3 to 1.5 moles of sulfuric acid per mole of dihydroxydiphenyl sulfone, at from 100.degree. to 180.degree. C.,(B) subsequently, at from 40.degree. to 90.degree. C., carrying out a precondensation with 1 to 2 moles of formaldehyde and 0.5 to 1.5 moles of urea per mole of phenol units present in aqueous medium,(C) partially neutralizing the reaction mixture,(D) adding to the partially neutralized reaction mixture 0 to 0.5 mole of phenol per mole of phenol units present and then 0.1 to 0.8 mole of formaldehyde per mole of phenol units then present,(E) further condensing at from 40.degree. to 90.degree. C.,(F) shifting the pH of the reaction mixture into the neutral range and(G) subsequently acidifying with a weak acid.

    摘要翻译： 苯酚磺酸，二羟基二苯基砜，脲和甲醛缩合的产物可以通过以下方法获得：（A）在苯磺酸和二羟基二苯基砜的硫酸中以3:1至10:1的摩尔比制备均匀的反应混合物， 条件是混合物的水含量不超过组分总重量的10％，并且混合物含有0.3至1.5摩尔硫酸/摩尔二羟基二苯基砜，在100至180℃ （B）随后在40℃至90℃下，每1摩尔含水介质中的苯酚单元进行1至2摩尔甲醛和0.5至1.5摩尔脲的预缩合，（C）部分中和 反应混合物中，（D）向部分中和的反应混合物中加入每摩尔苯酚单元0至0.5摩尔苯酚，然后存在每摩尔苯酚单元0.1至0.8摩尔甲醛，（E）进一步冷凝 在40℃至90℃下，（F）将反应混合物的pH转移到中性范围，（G）随后用弱酸酸化。

    Substituted sulfobenzene and triazine-containing reactive dyes
    6.
    发明授权
    Substituted sulfobenzene and triazine-containing reactive dyes 失效
    取代的磺基苯和三嗪的活性染料

    公开(公告)号：US4801693A

    公开(公告)日：1989-01-31

    申请号：US88533

    申请日：1987-08-20

    申请人： Ortwin Schaffer ,  Manfred Patsch

    发明人： Ortwin Schaffer ,  Manfred Patsch

    IPC分类号： C09B62/01 ,  C09B62/03 ,  C09B62/04 ,  C09B62/09 ,  C09B62/25 ,  C09B62/44 ,  C09B62/513 ,  D06P3/10 ,  D06P3/66

    CPC分类号： C09B62/043 ,  C09B62/09 ,  C09B62/25 ,  C09B62/4415 ,  C09B62/513

    摘要： Novel compounds of the general formula I ##STR1## where A is a fiber-reactive radical of the triazine, pyrimidine or vinylsulfone series, D is a radical of a sulfo-containing diazo component of the aniline or aminonaphthalene series, K is the radical of a coupling component of the aminohydroxynaphthalene series, X is fluorine, chlorine, bromine, C.sub.1 -C.sub.4 -alkyl, trifluoromethyl, C.sub.1 -C.sub.4 -alkoxy, phenoxy, hydroxysulfonyl, carboxyl, acetyl, propionyl, methylsulfonyl, ethylsulfonyl, phenylsulfonyl, C.sub.1 -C.sub.4 -alkoxycarbonyl, phenoxysulfonyl or unsubstituted or substituted carbamyl or sulfamyl, and Y is fluorine, chlorine, bromine, C.sub.1 -C.sub.4 -alkyl, trifluoromethyl, C.sub.1 -C.sub.4 -alkoxy, phenoxy, phenoxysulfonyl, acetyl, propionyl, methylsulfonyl, ethylsulfonyl, phenylsulfonyl, p-acetylaminophenylsulfonyl, hydroxysulfonyl, C.sub.1 -C.sub.4 -alkoxycarbonyl, hydroxycarbonyl or unsubstituted or substituted carbamyl or sulfamyl, are very useful for dyeing wool and hydroxyl-containing fibers, such as cellulose and in particular cotton.

    摘要翻译： 通式I的新型化合物其中A是三嗪，嘧啶或乙烯基砜系列的纤维反应性基团，D是苯胺或氨基萘系列的含磺基重氮组分的基团，K是基团 的氨基羟基萘系列的偶联组分，X为氟，氯，溴，C 1 -C 4 - 烷基，三氟甲基，C 1 -C 4 - 烷氧基，苯氧基，羟基磺酰基，羧基，乙酰基，丙酰基，甲基磺酰基，乙基磺酰基，苯基磺酰基， 烷氧基，苯氧基，苯氧基磺酰基，乙酰基，丙酰基，甲基磺酰基，乙基磺酰基，苯基磺酰基，苯基磺酰基，苯基磺酰基，苯基磺酰基， 乙酰氨基苯基磺酰基，羟基磺酰基，C 1 -C 4 - 烷氧基羰基，羟基羰基或未取代或取代的氨基甲酰基或亚磺酰基，对于染色羊毛和含羟基纤维如纤维素，特别是c otton。