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    Processes for preparing mono-dispersed particles
    2.
    发明授权
    Processes for preparing mono-dispersed particles 失效
    制备单分散颗粒的方法

    公开(公告)号：US4925704A

    公开(公告)日：1990-05-15

    申请号：US206863

    申请日：1988-06-13

    申请人： Goro Sato ,  Michio Komatsu ,  Hiroyasu Nishida ,  Yoshichika Tanaka ,  Tsuguo Koyanagi ,  Kei Mihara

    发明人： Goro Sato ,  Michio Komatsu ,  Hiroyasu Nishida ,  Yoshichika Tanaka ,  Tsuguo Koyanagi ,  Kei Mihara

    IPC分类号： C01B13/32 ,  C01B33/16 ,  C01G23/053 ,  C01G25/02 ,  G02F1/1339

    CPC分类号： C01B33/163 ,  C01B13/32 ,  C01G23/053 ,  C01G25/02 ,  G02F1/13392 ,  C01P2004/03 ,  C01P2004/32 ,  C01P2004/52 ,  C01P2004/61 ,  C01P2004/62 ,  C01P2006/22 ,  C01P2006/60 ,  Y10T428/2998

    摘要： In a process for preparing spherical particles of a metal oxide or hydroxide having a particle size of from 0.1 to 10 .mu.m by adding a corresponding metal alkoxide to a dispersion of water-alcohol system having dispersed therein a metal oxide or hydroxide as a seed, under alkaline conditions and allowing a decomposition product from said metal alkoxide to attach onto said seed to effect particle growth of the seed, the improvement which comprises maintaining said dispersion at a substantially constant pH within the range between 10 and 13 during the addition of the metal alkoxide to said dispersion and the subsequent particle growth of the seed, thereby to prepare mono-dispersed particles substantially free from particle aggregation having a sharp particle size distribution of a standard deviation of not greater than 0.5. The white particles so prepared may be, after separation, heat treated to provide black particles. The white or black particles may be coated with a synthetic resin in the surface. The products are useful particularly as spacers for liquid crystal display devices.

    摘要翻译： 在通过向其中分散有金属氧化物或氢氧化物作为种子的水 - 醇体系的分散体中加入相应的金属醇盐来制备粒径为0.1至10μm的金属氧化物或氢氧化物的球形颗粒的方法中， 在碱性条件下并允许来自所述金属醇盐的分解产物附着在所述种子上以实现种子的颗粒生长，其改进包括在添加金属期间将所述分散体保持在10至13之间的基本恒定的pH值在10和13之间的范围内 所述分散体和随后的种子颗粒生长，从而制备基本上不具有标准偏差不大于0.5的尖锐粒度分布的颗粒聚集的单分散颗粒。 如此制备的白色颗粒可以在分离后进行热处理以提供黑色颗粒。 白色或黑色颗粒可以在表面上涂覆合成树脂。 该产品特别用作液晶显示装置的间隔物。

    Coating liquids for forming conductive coatings
    6.
    发明授权
    Coating liquids for forming conductive coatings 失效
    涂层液形成导电涂料

    公开(公告)号：US5078915A

    公开(公告)日：1992-01-07

    申请号：US298607

    申请日：1988-10-11

    申请人： Goro Sato ,  Michio Komatsu ,  Toshiharu Hirai ,  Yoneji Abe ,  Keiichi Mihara

    发明人： Goro Sato ,  Michio Komatsu ,  Toshiharu Hirai ,  Yoneji Abe ,  Keiichi Mihara

    IPC分类号： B32B15/00 ,  C03C17/23 ,  C03C17/25

    CPC分类号： C03C17/25 ,  C03C17/23 ,  C03C2217/23 ,  C03C2218/11

    摘要： In accordance with the present invention, there are provided coating liquids for forming conductive coatings, which comprise (i) a zirconium oxysalt, (ii) a conductive substance and, if necessary, (iii) at least one member selected from non-sedimentary silica dispersion and silicon alkoxide or its derivative. The coating liquids, when coated on substrates, form thereon transparent conductive coatings which are excellent in transparency, scratch resistance, permanence properties and adhesion to the substrates and, moreover, excellent in antistatic effect. In particular, when the coating liquids for forming conductive coatings mentioned above are coated by the spray method on appropriate substrates followed by drying and/or heating, there are obtained face-plates for display devices, which have excellent regular reflection reducing effect (non-glare) and antistatic effect.

    摘要翻译： PCT No.PCT / JP88 / 00122 Sec。 371日期：1988年10月11日 102（e）日期1988年10月11日PCT提交1988年2月9日PCT公布。 公开号WO88 / 06331 日本1988年8月25日。根据本发明，提供了用于形成导电涂层的涂料液体，其包含（i）锆氧基钾，（ii）导电物质，如果需要，（iii）至少一种 成员选自非沉积二氧化硅分散体和硅烷醇盐或其衍生物。 涂布液在基材上涂布时，在其上形成透明性，耐擦伤性，耐久性和对基材的粘合性优异的抗静电效果的透明导电性涂料。 特别地，当将用于形成上述导电涂层的涂布液通过喷涂方法涂覆在适当的基材上，然后进行干燥和/或加热时，获得具有优异的正常反射减少效果的显示装置用面板， 眩光）和抗静电效果。

    Substrate having a transparent coating thereon
    7.
    发明授权
    Substrate having a transparent coating thereon 失效
    基材在其上具有透明涂层

    公开(公告)号：US5256484A

    公开(公告)日：1993-10-26

    申请号：US746406

    申请日：1991-08-16

    申请人： Goro Sato ,  Michio Komatsu ,  Toshiharu Hirai ,  Yoneji Abe ,  Keiichi Mihara

    发明人： Goro Sato ,  Michio Komatsu ,  Toshiharu Hirai ,  Yoneji Abe ,  Keiichi Mihara

    IPC分类号： C03C17/23 ,  C03C17/25 ,  B32B17/06

    CPC分类号： C03C17/23 ,  C03C17/25 ,  C03C2217/23 ,  C03C2218/11 ,  Y10T428/31598 ,  Y10T428/31609

    摘要： In accordance with the present invention, there are provided coating liquids for forming conductive coatings, which comprise (i) a zirconium oxysalt, (ii) a conductive substance and, if necessary, (iii) at least one member selected from non-sedimentary silica dispersion and silicon alkoxide or its derivative. The coating liquids, when coated on substrate, form thereon transparent conductive coatings which are excellent in transparency, scratch resistance, permanence properties and adhesion to the substrates and, moreover, excellent in antistatic effect. In particular, when the coating liquids for forming conductive coatings mentioned above are coated by the spray method on appropriate substrates followed by drying and/or heating, there are obtained face-plates for display devices, which have excellent regular reflection reducing effect (non-glare) and antistatic effect.

    摘要翻译： 根据本发明，提供了用于形成导电涂层的涂布液，其包括（i）锆氧化锡，（ii）导电物质，如果需要，（iii）至少一种选自非沉积二氧化硅 分散体和烷氧基硅烷或其衍生物。 涂布液在基材上涂布时，在透明性，耐刮擦性，耐久性和对基材的粘附性上具有优异的抗静电效果的透明导电性涂料。 特别地，当将用于形成上述导电涂层的涂布液通过喷涂方法涂覆在适当的基材上，然后进行干燥和/或加热时，获得具有优异的正常反射减少效果的显示装置用面板， 眩光）和抗静电效果。

    Coating liquids for forming conductive coatings
    8.
    发明授权
    Coating liquids for forming conductive coatings 失效
    用于形成导电涂层的涂料液体

    公开(公告)号：US5270072A

    公开(公告)日：1993-12-14

    申请号：US746403

    申请日：1991-08-16

    申请人： Goro Sato ,  Michio Komatsu ,  Toshiharu Hirai ,  Yoneji Abe ,  Keiichi Mihara

    发明人： Goro Sato ,  Michio Komatsu ,  Toshiharu Hirai ,  Yoneji Abe ,  Keiichi Mihara

    IPC分类号： C03C17/23 ,  C03C17/25 ,  B05D5/12

    CPC分类号： C03C17/25 ,  C03C17/23 ,  C03C2217/23 ,  C03C2218/11

    摘要： In accordance with the present invention, there are provided coating liquids for forming conductive coatings, which comprise (i) a zirconium oxysalt, (ii) a conductive substance and, if necessary, (iii) at least one member selected from non-sedimentary silica dispersion and silicon alkoxide or its derivative. The coating liquids, when coated on substrates, form thereon transparent conductive coatings which are excellent in transparency, scratch resistance, permanence properties and adhesion to the substrates and, moreover, excellent in antistatic effect. In particular, when the coating liquids for forming conductive coatings mentioned above are coated by the spray method on appropriate substrates followed by drying and/or heating, there are obtained face plates for display devices, which have excellent regular reflection reducing effect (non-glare) and antistatic effect.

    摘要翻译： 根据本发明，提供了用于形成导电涂层的涂布液，其包括（i）锆氧化锡，（ii）导电物质，如果需要，（iii）至少一种选自非沉积二氧化硅 分散体和烷氧基硅烷或其衍生物。 涂布液在基材上涂布时，在其上形成透明性，耐擦伤性，耐久性和对基材的粘合性优异的抗静电效果的透明导电性涂料。 特别地，当用上述形成导电涂层的涂布液通过喷涂方法在适当的基材上进行干燥和/或加热涂覆时，得到具有优异的均匀反射减少效果（非眩光）的显示装置用面板 ）和抗静电效果。

    Coating liquids for forming conductive coatings
    9.
    发明授权
    Coating liquids for forming conductive coatings 失效
    用于形成导电涂层的涂料液体

    公开(公告)号：US5273828A

    公开(公告)日：1993-12-28

    申请号：US746402

    申请日：1991-08-16

    申请人： Goro Sato ,  Michio Komatsu ,  Toshiharu Hirai ,  Yoneji Abe ,  Keiichi Mihara

    发明人： Goro Sato ,  Michio Komatsu ,  Toshiharu Hirai ,  Yoneji Abe ,  Keiichi Mihara

    IPC分类号： B32B15/00 ,  C03C17/23 ,  C03C17/25

    CPC分类号： C03C17/25 ,  C03C17/23 ,  C03C2217/23 ,  C03C2218/11

    摘要： In accordance with the present invention, there are provided coating liquids for forming conductive coatings, which comprise (i) a zirconium oxysalt, (ii) a conductive substance and, if necessary, (iii) at least one member selected from non-sedimentary silica dispersion and silicon alkoxide or its derivative. The coating liquids, when coated on substrates, form thereon transparent conductive coatings which are excellent in transparency, scratch resistance, permanence properties and adhesion to the substrates and, moreover, excellent in antistatic effect. In particular, when the coating liquids for forming conductive coatings mentioned above are coated by the spray method on appropriate substrates followed by drying and/or heating, there are obtained face-plates for display devices, which have excellent regular reflection reducing effect (non-glare) and antistatic effect.

    摘要翻译： 根据本发明，提供了用于形成导电涂层的涂布液，其包括（i）锆氧化锡，（ii）导电物质，如果需要，（iii）至少一种选自非沉积二氧化硅 分散体和烷氧基硅烷或其衍生物。 涂布液在基材上涂布时，在其上形成透明性，耐擦伤性，耐久性和对基材的粘合性优异的抗静电效果的透明导电性涂料。 特别地，当将用于形成上述导电涂层的涂布液通过喷涂方法涂覆在适当的基材上，然后进行干燥和/或加热时，获得具有优异的正常反射减少效果的显示装置用面板， 眩光）和抗静电效果。

    Transparent conductive ceramic-coated substrate processes for preparing same and uses thereof
    10.
    发明授权
    Transparent conductive ceramic-coated substrate processes for preparing same and uses thereof 失效
    透明导电陶瓷涂布基板的制备方法及其用途

    公开(公告)号：US5013607A

    公开(公告)日：1991-05-07

    申请号：US391604

    申请日：1989-06-08

    申请人： Goro Sato ,  Michio Komatsu ,  Toshiharu Hirai ,  Yoneji Abe ,  Noboru Senjyuu

    发明人： Goro Sato ,  Michio Komatsu ,  Toshiharu Hirai ,  Yoneji Abe ,  Noboru Senjyuu

    IPC分类号： C03C17/25 ,  C09D5/24

    CPC分类号： C03C17/25 ,  C09D5/24 ,  C03C2217/23 ,  C03C2218/11 ,  C03C2218/113 ,  Y10T428/31612 ,  Y10T428/31663

    摘要： Disclosed are transparent conductive ceramiccoated substrates having a surface resistance of 10.sup.3 -10.sup.11 .OMEGA./.quadrature., a total light transmission of at least 85% and a haze of less than 10%, said coated substrates being prepared by coating on the substrate a water organic solvent mixture type coating liquid containing dialkoxy-bisacetylacetonato zirconium, a partial hydrolysate of silicon alkoxide and a conductive substance, processes for preparing said coated substrates, and display and copy machine using said coated substrates.

    摘要翻译： PCT No.PCT / JP88 / 00793 Sec。 371日期：1989年6月8日 102（e）日期1989年6月8日PCT PCT 1988年8月10日PCT公布。 公开号WO89 / 03114 日期为1989年4月6日。公开的是透明导电陶瓷涂层基材，其表面电阻为103-1011欧米茄/平方厘米，总透光率至少为85％，雾度小于10％，所述涂覆的基材通过涂布 在基材上，含有二烷氧基 - 双乙酰丙酮酸锆的部分水解有机溶剂混合物型涂料液，硅氧烷和导电物质的部分水解产物，制备所述涂覆的基材的方法，以及使用所述涂覆的基材的显示和复印机。