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    Process for the production of acrylic acid
    1.
    发明授权
    Process for the production of acrylic acid 有权
    丙烯酸生产工艺

    公开(公告)号：US07294741B2

    公开(公告)日：2007-11-13

    申请号：US10498852

    申请日：2002-12-13

    申请人： Gunther Bub ,  Jurgen Mosler ,  Dietrich Maschmeyer ,  Andreas Sabbagh ,  Roland Fornika ,  Matthias Peuckert

    发明人： Gunther Bub ,  Jurgen Mosler ,  Dietrich Maschmeyer ,  Andreas Sabbagh ,  Roland Fornika ,  Matthias Peuckert

    IPC分类号： C07C51/16

    CPC分类号： C07C51/252 ,  C07C57/04

    摘要： The present invention relates to a process for the production of acrylic acid (AA) comprising the steps wherein: a) a 1st gas mixture comprising propylene, oxygen, an inert gas and steam is subjected to a 1st catalytic oxidation reaction stage thereby converting the propylene in the presence of a catalyst mainly into acrolein being contained in a 2nd gas mixture from said 1st catalytic oxidation reaction, b) said 2nd gas mixture from the 1st catalytic oxidation reaction stage is subjected to a 2nd catalytic oxidation reaction stage thereby converting the acrolein in the presence of a catalyst mainly into AA, being contained in a product gas, c) said product gas is subjected to a quench tower, wherein said AA is recovered as an aqueous solution comprising said AA being contained in the process water, wherein a process vent gas is obtained at the top of said quench tower, wherein, said 1st gas mixture has a steam/propylene ratio of >0.3 and

    摘要翻译： 本发明涉及一种生产丙烯酸（AA）的方法，包括以下步骤：a）将包含丙烯，氧气，惰性气体和蒸汽的第一气体混合物进行第一催化氧化反应阶段，由此将丙烯 在主催化剂存在下，由所述第一催化氧化反应产生的第二气体混合物中含有丙烯醛，b）将来自第一催化氧化反应阶段的所述第二气体混合物进行第二催化氧化反应阶段，由此将丙烯醛转化为 催化剂主要以AA形式存在于产物气体中，c）将所述产物气体进行骤冷塔，其中所述AA作为包含所述AA的水溶液被回收，所述水溶液包含在工艺用水中，其中过程 在所述骤冷塔的顶部获得排出气体，其中所述第一气体混合物具有> 0.3和<2的蒸汽/丙烯比，并且所述处理水的量为 s或等于从骤冷塔抽出的所述水溶液中的水量。

    Process for the production of acrylic acid
    2.
    发明申请
    Process for the production of acrylic acid 有权
    丙烯酸生产工艺

    公开(公告)号：US20050171380A1

    公开(公告)日：2005-08-04

    申请号：US10498852

    申请日：2002-12-13

    申请人： Gunther Bub ,  Jurgen Mosler ,  Dietrich Maschmeyer ,  Andreas Sabbagh ,  Roland Fornika ,  Matthias Peuckert

    发明人： Gunther Bub ,  Jurgen Mosler ,  Dietrich Maschmeyer ,  Andreas Sabbagh ,  Roland Fornika ,  Matthias Peuckert

    IPC分类号： B01J23/30 ,  B01J8/04 ,  B01J23/88 ,  B01J35/04 ,  C07B61/00 ,  C07C51/235 ,  C07C51/25 ,  C07C51/48 ,  C07C57/055 ,  C07C51/16

    CPC分类号： C07C51/252 ,  C07C57/04

    摘要： The present invention relates to a process for the production of acrylic acid (AA) comprising the steps wherein: a) a 1st gas mixture comprising propylene, oxygen, an inert gas and steam is subjected to a 1st catalytic oxidation reaction stage thereby converting the propylene in the presence of a catalyst mainly into acrolein being contained in a 2nd gas mixture from said 1st catalytic oxidation reaction, b) said 2nd gas mixture from the 1st catalytic oxidation reaction stage is subjected to a 2nd catalytic oxidation reaction stage thereby converting the acrolein in the presence of a catalyst mainly into AA, being contained in a product gas, c) said product gas is subjected to a quench tower, wherein said AA is recovered as an aqueous solution comprising said AA being contained in the process water, wherein a process vent gas is obtained at the top of said quench tower, wherein, said 1st gas mixture has a steam/propylene ratio of >0.3 and

    摘要翻译： 本发明涉及一种生产丙烯酸（AA）的方法，包括以下步骤：a）将包含丙烯，氧气，惰性气体和蒸汽的第一气体混合物进行第一催化氧化反应阶段，由此将丙烯 在主催化剂存在下，由所述第一催化氧化反应产生的第二气体混合物中含有丙烯醛，b）将来自第一催化氧化反应阶段的所述第二气体混合物进行第二催化氧化反应阶段，由此将丙烯醛转化为 催化剂主要以AA形式存在于产物气体中，c）将所述产物气体进行骤冷塔，其中所述AA作为包含所述AA的水溶液被回收，所述水溶液包含在所述工艺用水中， 在所述骤冷塔的顶部获得排出气体，其中所述第一气体混合物具有> 0.3和<2的蒸汽/丙烯比，并且所述处理水的量为 s或等于从骤冷塔抽出的所述水溶液中的水量。

    SUPERABSORBENT POLYMERS AND METHODS OF MAKING THE SAME
    6.
    发明申请
    SUPERABSORBENT POLYMERS AND METHODS OF MAKING THE SAME 有权
    超吸收聚合物及其制备方法

    公开(公告)号：US20120226003A1

    公开(公告)日：2012-09-06

    申请号：US13461220

    申请日：2012-05-01

    申请人： Torsten Balduf ,  Gunther Bub ,  Jurgen Mosler ,  Andreas Sabbagh ,  Jurgen Kohn ,  Arndt Selbach

    发明人： Torsten Balduf ,  Gunther Bub ,  Jurgen Mosler ,  Andreas Sabbagh ,  Jurgen Kohn ,  Arndt Selbach

    IPC分类号： C08F2/44 ,  C08F120/06

    CPC分类号： C08J3/00 ,  C07C51/43 ,  C07C57/04

    摘要： In some embodiments, a process for producing a polymer comprises (I) producing a pure (meth)acrylic acid comprising the steps of (a) synthesizing a crude (meth)acrylic acid phase; (b) distillatively working-up the crude (meth)acrylic acid phase to obtain a (meth)acrylic acid phase and a dimer phase comprising (meth)acrylic acid dimers or (meth)acrylic acid oligomers or both; (c) splitting at least a part of the (meth)acrylic acid dimers or of the (meth)acrylic acid oligomers or both from the dimer phase to obtain a (meth)acrylic acid-comprising low boiling phase and a high boiling phase comprising less (meth)acrylic acid than the low boiling phase; (d) separating at least a part of the (meth)acrylic acid from the low boiling phase to obtain a pure (meth)acrylic acid, and a residue; (II) polymerizing a monomer phase comprising the pure (meth)acrylic acid to obtain a polymer phase; and (III) working-up the polymer phase to obtain the polymer.

    摘要翻译： 在一些实施方案中，制备聚合物的方法包括（I）制备纯（甲基）丙烯酸，其包括以下步骤：（a）合成粗（甲基）丙烯酸相; （b）蒸馏处理粗（甲基）丙烯酸相以获得（甲基）丙烯酸相和包含（甲基）丙烯酸二聚体或（甲基）丙烯酸低聚物或二者的二聚体相; （c）从二聚体相分离至少一部分（甲基）丙烯酸二聚体或（甲基）丙烯酸低聚物或两者，得到包含（甲基）丙烯酸的低沸点相和高沸点相，包括 较少（甲基）丙烯酸低于低沸点相; （d）从低沸点相分离出至少一部分（甲基）丙烯酸，得到纯（甲基）丙烯酸，残渣; （II）使包含纯（甲基）丙烯酸的单体相聚合以获得聚合物相; 和（III）加工聚合物相以获得聚合物。

    WATER-ABSORBENT POLYMER STRUCTURES BASED ON RENEWABLE RESOURCES AND METHOD FOR PRODUCING SAID STRUCTURES
    8.
    发明申请
    WATER-ABSORBENT POLYMER STRUCTURES BASED ON RENEWABLE RESOURCES AND METHOD FOR PRODUCING SAID STRUCTURES 有权
    基于可再生资源的水吸收聚合物结构和生产结构的方法

    公开(公告)号：US20090023006A1

    公开(公告)日：2009-01-22

    申请号：US11817204

    申请日：2006-02-28

    申请人： Gunther Bub ,  Jurgen Mosler ,  Andreas Sabbagh ,  Franz-Felix Kuppinger ,  Franck Furno

    发明人： Gunther Bub ,  Jurgen Mosler ,  Andreas Sabbagh ,  Franz-Felix Kuppinger ,  Franck Furno

    IPC分类号： B32B27/28 ,  C08F20/06 ,  C07C57/04 ,  C12M1/34

    CPC分类号： C08F4/30 ,  C08F2/00 ,  C12P7/40 ,  C12P7/42 ,  Y10T428/31855

    摘要： The present invention relates to a process for the production of polymers, such as water-absorbing polymer structures, by radical polymerization of acrylic acid, whereby the acrylic acid has been obtained by a synthesis process which comprises as a process step the splitting of an organic material by means of an enzyme or at least one component of an enzyme. The invention also relates to the water-absorbing polymers obtainable by this process, water-absorbing polymers which are based to at least about 25 wt % upon partially neutralized acrylic acid, a composite, a process for the production of a composite, the composite obtainable by this production, the use of acrylic acid in the production of polymers, preferably in the production of water-absorbing polymer structures, a device for the production of acrylic acid, and a process for the production of acrylic acid.

    摘要翻译： 本发明涉及通过丙烯酸的自由基聚合制备聚合物如吸水聚合物结构的方法，由此通过合成方法获得丙烯酸，其包括作为工艺步骤将有机物分解 材料通过酶或至少一种酶组分。 本发明还涉及通过该方法可获得的吸水聚合物，在部分中和的丙烯酸上基于至少约25重量％的吸水聚合物，复合材料，制备复合材料的方法，可获得的复合材料 通过这种生产，在生产聚合物中使用丙烯酸，优选在生产吸水聚合物结构，生产丙烯酸的装置和生产丙烯酸的方法。

    Superabsorbent polymers and methods of making the same
    10.
    发明授权
    Superabsorbent polymers and methods of making the same 有权
    超吸收性聚合物及其制造方法

    公开(公告)号：US08445617B2

    公开(公告)日：2013-05-21

    申请号：US13668899

    申请日：2012-11-05

    申请人： Torsten Balduf ,  Gunther Bub ,  Jurgen Mosler ,  Andreas Sabbagh ,  Jurgen Kohn ,  Arndt Selbach

    发明人： Torsten Balduf ,  Gunther Bub ,  Jurgen Mosler ,  Andreas Sabbagh ,  Jurgen Kohn ,  Arndt Selbach

    IPC分类号： C08F220/06 ,  C08L33/02

    CPC分类号： C08J3/00 ,  C07C51/43 ,  C07C57/04

    摘要： The invention relates to producing a superabsorbent polymer comprising (I) producing a (meth)acrylic acid comprising the steps of (a) synthesizing a crude (meth)acrylic acid phase; (b) distillatively working-up the crude (meth)acrylic acid phase to obtain a (meth)acrylic acid phase and a dimer phase comprising (meth)acrylic acid dimers and/or (meth)acrylic acid oligomers; (c) splitting at least a part of the (meth)acrylic acid dimers or of the (meth)acrylic acid oligomers or both from the dimer phase to obtain a (meth)acrylic acid-comprising a low boiling phase and a high boiling phase comprising less (meth)acrylic acid than the low boiling phase; (d) separating at least a part of the (meth)acrylic acid from the low boiling phase by forming crystals to obtain a pure (meth)acrylic acid, and a residue; (II) polymerizing a monomer phase comprising the pure (meth)acrylic acid to obtain a polymer phase; and (III) working-up the polymer phase to obtain the polymer.

    摘要翻译： 本发明涉及制备超吸收性聚合物，其包括（I）生产（甲基）丙烯酸，其包括以下步骤：（a）合成粗制（甲基）丙烯酸相; （b）蒸馏处理粗（甲基）丙烯酸相以获得（甲基）丙烯酸相和包含（甲基）丙烯酸二聚体和/或（甲基）丙烯酸低聚物的二聚体相; （c）从二聚体相分解至少一部分（甲基）丙烯酸二聚体或（甲基）丙烯酸低聚物或两者，得到包含低沸点相和高沸点相的（甲基）丙烯酸 包括比低沸点相少的（甲基）丙烯酸; （d）通过形成晶体从低沸点相分离出至少一部分（甲基）丙烯酸，得到纯的（甲基）丙烯酸和残余物; （II）使包含纯（甲基）丙烯酸的单体相聚合以获得聚合物相; 和（III）加工聚合物相以获得聚合物。