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公开(公告)号:US08747756B2
公开(公告)日:2014-06-10
申请号:US13381152
申请日:2010-07-01
申请人: Rolf Feller , Hanns-Ingolf Paul , Paul Wagner , John Lovegrove , Jörg Kirchhoff , Joachim Ritter , Ricarda Leiberich , Udo Wiesner
发明人: Rolf Feller , Hanns-Ingolf Paul , Paul Wagner , John Lovegrove , Jörg Kirchhoff , Joachim Ritter , Ricarda Leiberich , Udo Wiesner
CPC分类号: C08F2/01 , B01J19/1887 , B01J19/20 , B01J2219/00094 , B01J2219/00159 , B01J2219/00166 , B01J2219/00189 , B01J2219/00247 , B01J2219/182 , B01J2219/187
摘要: The present invention relates to a reactor (10) and a process for continuous polymerization, where the reactor (10) has an essentially tubular reactor housing (16). The reactor housing (16) has a drive (38) which runs along the geometric central axis (12) in the flow direction (22) and is configured as a central shaft. A rotatably arranged scraper or wiper (36) is provided within the reactor housing (16); the scraper or wiper (36) has at least one scraper or wiper blade (42) to run along an interior side (44) of the reactor housing (16). The rotational movement of the scraper or wiper (36) results in radial mixing of a stream within the reactor housing (16) which dominates gravity effects and, by virtue of shaping of the scrapers or wipers, optionally makes plug flow or backflow within the reactor (10) possible. This allows the reaction conditions in the axial direction of the reactor housing (16) to be predicted and individually suitable reaction conditions to be set and controlled along the reactor housing, so that, in particular, a desired molecular weight distribution can be set.
摘要翻译: 本发明涉及反应器(10)和连续聚合方法,其中反应器(10)具有基本上管状的反应器壳体(16)。 反应器壳体(16)具有在流动方向(22)上沿几何中心轴线(12)延伸并被构造为中心轴的驱动器(38)。 在反应器壳体(16)内设置有可旋转地布置的刮刀(36)。 刮刀或擦拭器(36)具有至少一个沿着反应器壳体(16)的内侧(44)延伸的刮刀或刮片(42)。 刮刀或擦拭器(36)的旋转运动导致反应器壳体(16)内的流的径向混合,其支配重力作用,并且借助于刮板或刮水器的成形,可任选地使反应器内的塞流或回流 (10)可能。 这允许预测反应器壳体(16)的轴向方向的反应条件,并且可以沿着反应器壳体设置和控制各自适当的反应条件,使得特别地可以设定所需的分子量分布。
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公开(公告)号:US09068031B2
公开(公告)日:2015-06-30
申请号:US13995246
申请日:2011-12-29
申请人: Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Joachim Ritter , Ricarda Leiberich , Jörg Kirchhoff , Udo Wiesner
发明人: Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Joachim Ritter , Ricarda Leiberich , Jörg Kirchhoff , Udo Wiesner
IPC分类号: C08F2/01 , B01J19/18 , C08F136/08 , B01J19/20 , C08F210/12
CPC分类号: C08F136/08 , B01J19/18 , B01J19/1812 , B01J19/1887 , B01J19/20 , B01J2219/00094 , B01J2219/0011 , B01J2219/00159 , B01J2219/00166 , B01J2219/00189 , B01J2219/00245 , B01J2219/00254 , B01J2219/182 , C08F210/12 , C08F236/08 , C08F2/01
摘要: The present invention relates to a reactor (10) and a process for continuous polymerization, where the reactor (10) has an essentially tubular reactor housing (16). The reactor housing (16) has a drive (38) which runs along the geometric central axis (12) in the flow direction (22) and is configured as a central shaft. A rotatably arranged scraper or wiper (36) is provided within the reactor housing (16); the scraper or wiper (36) has at least one scraper or wiper blade (42) to run along an interior side (44) of the reactor housing (16). The rotational movement of the scraper or wiper (36) results in radial mixing of a stream within the reactor housing (16) which dominates gravity effects and, by virtue of shaping of the scrapers or wipers, optionally makes plug flow or a loop flow or backflow within the reactor (10) or else via an additional external pumped circulation system (23) possible. This allows the reaction conditions in the axial direction of the reactor housing (16) to be predicted and individually suitable reaction conditions to be set and controlled along the reactor housing, so that, in particular, a desired molecular weight distribution can be set.
摘要翻译: 本发明涉及反应器(10)和连续聚合方法,其中反应器(10)具有基本上管状的反应器壳体(16)。 反应器壳体(16)具有在流动方向(22)上沿几何中心轴线(12)延伸并被构造为中心轴的驱动器(38)。 在反应器壳体(16)内设置有可旋转地布置的刮刀(36)。 刮刀或擦拭器(36)具有至少一个沿着反应器壳体(16)的内侧(44)延伸的刮刀或刮片(42)。 刮刀或擦拭器(36)的旋转运动导致在反应器壳体(16)内的流的径向混合,其支配重力作用,并且借助于刮板或刮水器的成形,可选地使塞子流或环流或 反应器(10)内的回流,或经由另外的外部泵送循环系统(23)。 这允许预测反应器壳体(16)的轴向方向的反应条件,并且可以沿着反应器壳体设置和控制各自适当的反应条件,使得特别地可以设定所需的分子量分布。
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公开(公告)号:US20120302706A1
公开(公告)日:2012-11-29
申请号:US13381152
申请日:2010-07-01
申请人: Rolf Feller , Hanns-Ingolf Paul , Paul Wagner , John Lovegrove , Jörg Kirchhoff , Joachim Ritter , Ricarda Leiberich , Udo Wiesner
发明人: Rolf Feller , Hanns-Ingolf Paul , Paul Wagner , John Lovegrove , Jörg Kirchhoff , Joachim Ritter , Ricarda Leiberich , Udo Wiesner
CPC分类号: C08F2/01 , B01J19/1887 , B01J19/20 , B01J2219/00094 , B01J2219/00159 , B01J2219/00166 , B01J2219/00189 , B01J2219/00247 , B01J2219/182 , B01J2219/187
摘要: The present invention relates to a reactor (10) and a process for continuous polymerization, where the reactor (10) has an essentially tubular reactor housing (16). The reactor housing (16) has a drive (38) which runs along the geometric central axis (12) in the flow direction (22) and is configured as a central shaft. A rotatably arranged scraper or wiper (36) is provided within the reactor housing (16); the scraper or wiper (36) has at least one scraper or wiper blade (42) to run along an interior side (44) of the reactor housing (16). The rotational movement of the scraper or wiper (36) results in radial mixing of a stream within the reactor housing (16) which dominates gravity effects and, by virtue of shaping of the scrapers or wipers, optionally makes plug flow or backflow within the reactor (10) possible. This allows the reaction conditions in the axial direction of the reactor housing (16) to be predicted and individually suitable reaction conditions to be set and controlled along the reactor housing, so that, in particular, a desired molecular weight distribution can be set.
摘要翻译: 本发明涉及反应器(10)和连续聚合方法,其中反应器(10)具有基本上管状的反应器壳体(16)。 反应器壳体(16)具有在流动方向(22)上沿几何中心轴线(12)延伸并被构造为中心轴的驱动器(38)。 在反应器壳体(16)内设置有可旋转地布置的刮刀(36)。 刮刀或擦拭器(36)具有至少一个沿着反应器壳体(16)的内侧(44)延伸的刮刀或刮片(42)。 刮刀或擦拭器(36)的旋转运动导致反应器壳体(16)内的流的径向混合,其支配重力作用,并且借助于刮板或刮水器的成形,可任选地使反应器内的塞流或回流 (10)可能。 这允许预测反应器壳体(16)的轴向方向的反应条件,并且可以沿着反应器壳体设置和控制各自适当的反应条件,使得特别地可以设定所需的分子量分布。
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公开(公告)号:US20140148561A1
公开(公告)日:2014-05-29
申请号:US13995246
申请日:2011-12-29
申请人: Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Joachim Ritter , Ricarda Leiberich , Jörg Kirchhoff , Udo Wiesner
发明人: Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Joachim Ritter , Ricarda Leiberich , Jörg Kirchhoff , Udo Wiesner
IPC分类号: C08F136/08 , B01J19/18
CPC分类号: C08F136/08 , B01J19/18 , B01J19/1812 , B01J19/1887 , B01J19/20 , B01J2219/00094 , B01J2219/0011 , B01J2219/00159 , B01J2219/00166 , B01J2219/00189 , B01J2219/00245 , B01J2219/00254 , B01J2219/182 , C08F210/12 , C08F236/08 , C08F2/01
摘要: The present invention relates to a reactor (10) and a process for continuous polymerization, where the reactor (10) has an essentially tubular reactor housing (16). The reactor housing (16) has a drive (38) which runs along the geometric central axis (12) in the flow direction (22) and is configured as a central shaft. A rotatably arranged scraper or wiper (36) is provided within the reactor housing (16); the scraper or wiper (36) has at least one scraper or wiper blade (42) to run along an interior side (44) of the reactor housing (16). The rotational movement of the scraper or wiper (36) results in radial mixing of a stream within the reactor housing (16) which dominates gravity effects and, by virtue of shaping of the scrapers or wipers, optionally makes plug flow or a loop flow or backflow within the reactor (10) or else via an additional external pumped circulation system (23) possible. This allows the reaction conditions in the axial direction of the reactor housing (16) to be predicted and individually suitable reaction conditions to be set and controlled along the reactor housing, so that, in particular, a desired molecular weight distribution can be set.
摘要翻译: 本发明涉及反应器(10)和连续聚合方法,其中反应器(10)具有基本上管状的反应器壳体(16)。 反应器壳体(16)具有在流动方向(22)上沿几何中心轴线(12)延伸并被构造为中心轴的驱动器(38)。 在反应器壳体(16)内设置有可旋转地布置的刮刀(36)。 刮刀或擦拭器(36)具有至少一个沿着反应器壳体(16)的内侧(44)延伸的刮刀或刮片(42)。 刮刀或擦拭器(36)的旋转运动导致反应器壳体(16)内的流的径向混合,其支配重力作用,并且借助刮板或刮水器的成形,可选地使塞子流或环流或 反应器(10)内的回流,或经由另外的外部泵送循环系统(23)。 这允许预测反应器壳体(16)的轴向方向的反应条件,并且可以沿着反应器壳体设置和控制各自适当的反应条件,使得特别地可以设定所需的分子量分布。
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5.
公开(公告)号:US20130203943A1
公开(公告)日:2013-08-08
申请号:US13635954
申请日:2011-03-23
申请人: Jörg Kirchhoff , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Udo Wiesner
发明人: Jörg Kirchhoff , Adam Gronowski , John Lovegrove , Hanns-Ingolf Paul , Rolf Feller , Udo Wiesner
IPC分类号: C08F6/10
CPC分类号: C08F6/10 , B29C48/76 , B29C48/767 , C08C19/12 , C08F6/003 , C08F6/008 , C08L23/283
摘要: The present invention relates to water and solvent-free halogenated butyl rubber products as a process for the production thereof. The process comprises at least the steps of: a.) treating a fluid containing at least one halogenated butyl rubber and at least one volatile compound in at least one concentrator unit, b.) reheating the concentrated fluid and c.) feeding the reheated concentrated fluid into at least one extruder.
摘要翻译: 本发明涉及作为其生产方法的无水和无溶剂卤化丁基橡胶产品。 该方法至少包括以下步骤:a)在至少一个浓缩器单元中处理含有至少一种卤化丁基橡胶和至少一种挥发性化合物的流体,b)加热浓缩流体,c)将再加热的浓缩 流体进入至少一个挤出机。
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公开(公告)号:US09512240B2
公开(公告)日:2016-12-06
申请号:US13063227
申请日:2009-09-17
申请人: Jörg Kirchhoff , Werner Bäcker , Rolf Feller , Paul Wagner , John Lovegrove , Hanns-Ingolf Paul
发明人: Jörg Kirchhoff , Werner Bäcker , Rolf Feller , Paul Wagner , John Lovegrove , Hanns-Ingolf Paul
IPC分类号: B29C47/76 , C08C2/00 , C01B5/00 , C08F6/00 , B29C47/36 , B29C47/38 , B29C47/60 , B29C47/62 , B29B7/74
CPC分类号: C08C2/00 , B29B7/7485 , B29C47/364 , B29C47/38 , B29C47/6056 , B29C47/62 , C01B5/00 , C08F6/003 , C08L23/283
摘要: The present invention relates to water and solvent-free polymers, in particular water and solvent-free synthetic rubber products like non-halogenated and halogenated butyl rubber products as well as a process for the production thereof. The invention further relates to a device suitable to accomplish said process.
摘要翻译: 本发明涉及无水和无溶剂的聚合物,特别是无水和无溶剂的合成橡胶产品,如非卤化和卤化丁基橡胶产品,以及其生产方法。 本发明还涉及适合于完成所述过程的装置。
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公开(公告)号:US20130203942A1
公开(公告)日:2013-08-08
申请号:US13635803
申请日:2011-03-23
申请人: Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Jörg Kirchhoff , Werner Bäcker
发明人: Hanns-Ingolf Paul , Rolf Feller , Paul Wagner , John Lovegrove , Jörg Kirchhoff , Werner Bäcker
IPC分类号: C08F236/02
CPC分类号: C08C2/02 , B29B7/38 , B29B7/7461 , B29B7/7466 , B29B7/7495 , B29B7/82 , B29B7/845 , B29B9/065 , B29C48/03 , B29C48/37 , B29C48/38 , B29C48/385 , B29C48/39 , B29C48/395 , B29C48/57 , B29C48/575 , B29C48/767 , C08C2/00 , C08F6/003 , C08F236/02 , Y02P70/263 , C08L23/283
摘要: The present invention relates to water and solvent-free polymers, in particular water and solvent-free synthetic rubber products like non-halogenated and halogenated butyl rubber products as well as a process for the production thereof. The invention further relates to a device suitable to accomplish said process.
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公开(公告)号:US20120043687A1
公开(公告)日:2012-02-23
申请号:US13063227
申请日:2009-09-17
申请人: Jörg Kirchhoff , Werner Bäcker , Rolf Feller , Paul Wagner , John Lovegrove , Hanns-Ingolf Paul
发明人: Jörg Kirchhoff , Werner Bäcker , Rolf Feller , Paul Wagner , John Lovegrove , Hanns-Ingolf Paul
IPC分类号: B29B9/02 , C08F210/16 , B29C47/76 , C08F236/12 , C08F236/16 , C08F236/08 , C08F6/10 , C08F236/10
CPC分类号: C08C2/00 , B29B7/7485 , B29C47/364 , B29C47/38 , B29C47/6056 , B29C47/62 , C01B5/00 , C08F6/003 , C08L23/283
摘要: The present invention relates to water and solvent-free polymers, in particular water and solvent-free synthetic rubber products like non-halogenated and halogenated butyl rubber products as well as a process for the production thereof. The invention further relates to a device suitable to accomplish said process.
摘要翻译: 本发明涉及无水和无溶剂的聚合物,特别是无水和无溶剂的合成橡胶产品,如非卤化和卤化丁基橡胶产品,以及其生产方法。 本发明还涉及适合于完成所述过程的装置。
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9.
公开(公告)号:US09469697B2
公开(公告)日:2016-10-18
申请号:US13635810
申请日:2011-03-21
申请人: Hanns-Ingolf Paul , Paul Wagner , Rolf Feller , Jörg Kirchhoff , John Lovegrove , Florian Forner , Michael Klimpel , Peter Weuta , Sven Brandau
发明人: Hanns-Ingolf Paul , Paul Wagner , Rolf Feller , Jörg Kirchhoff , John Lovegrove , Florian Forner , Michael Klimpel , Peter Weuta , Sven Brandau
摘要: The present invention relates to specific water and solvent-free nitrile rubbers having specific functional groups and/or end groups, a process for the production thereof and the use thereof. This process involves removing volatile compounds from a fluid (F) containing (1) at least one nitrile rubber and (2) at least one volatile compound, wherein the process comprises at least the steps of a.) treating the fluid (F) in at least one conversation unit, b.) retreating the concentrated fluid from step a.) in at least one retreating unit and c.) feeding the retreated concentrated fluid from step b.) into at least one retreating unit.
摘要翻译: 本发明涉及具有特定官能团和/或端基的具体的无水和无溶剂丁腈橡胶,其制备方法及其用途。 该方法包括从含有(1)至少一种丁腈橡胶和(2)至少一种挥发性化合物的流体(F)中除去挥发性化合物,其中该方法至少包括以下步骤:a。)将 至少一个通话单元,b)将至少一个后退单元中的步骤a。)中的浓缩流体退回,以及c)将从后续处理的浓缩流体从步骤b。进给至至少一个后退单元。
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10.
公开(公告)号:US20130211031A1
公开(公告)日:2013-08-15
申请号:US13635810
申请日:2011-03-21
申请人: Matthias Soddemann , Werner Obrecht , Franz-Josef Mersmann , Hanns-Ingolf Paul , Paul Wagner , Rolf Feller , Thomas Köenig , Jörg Kirchhoff , Werner Bäcker , John Lovegrove
发明人: Matthias Soddemann , Werner Obrecht , Franz-Josef Mersmann , Hanns-Ingolf Paul , Paul Wagner , Rolf Feller , Thomas Köenig , Jörg Kirchhoff , Werner Bäcker , John Lovegrove
IPC分类号: C08C2/02
摘要: The present invention relates to specific water and solvent-free nitrile rubbers having specific functional groups and/or end groups, a process for the production thereof and the use thereof. This process involves removing volatile compounds from a fluid (F) containing (1) at least one nitrile rubber and (2) at least one volatile compound, wherein the process comprises at least the steps of a.) treating the fluid (F) in at least one conversation unit, b.) retreating the concentrated fluid from step a.) in at least one retreating unit and c.) feeding the retreated concentrated fluid from step b.) into at least one retreating unit.
摘要翻译: 本发明涉及具有特定官能团和/或端基的具体的无水和无溶剂丁腈橡胶,其制备方法及其用途。 该方法包括从含有(1)至少一种丁腈橡胶和(2)至少一种挥发性化合物的流体(F)中除去挥发性化合物,其中该方法至少包括以下步骤:a。)将 至少一个通话单元,b)将至少一个后退单元中的步骤a。)中的浓缩流体退回,以及c)将从后续处理的浓缩流体从步骤b。进给至至少一个后退单元。
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