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1.发明授权
公开(公告)号：US4786751A
公开(公告)日：1988-11-22
申请号：US797072
申请日：1985-11-12
IPC分类号： C08G18/00 , C07C67/00 , C07C241/00 , C07C265/04 , C07C265/10 , C07C265/12 , C07C265/14 , C08G18/10 , C08G18/72 , C08G18/74 , C08G18/76 , C09D175/00 , C07C71/00
CPC分类号： C07C265/12 , C08G18/74
摘要： Diisocyanates and isomeric mixtures of diisocyanates corresponding to the formula ##STR1## in which R.sub.1, R.sub.2, R.sub.3, m and n are as defined herein are made by phosgenating diamines corresponding to the formula ##STR2## in which R.sub.1, R.sub.2, R.sub.3, m and n are as defined herein at a temperature of from -20.degree. to 250.degree. C. These diisocyanates are particularly useful as starting materials for the production of polyurethanes by the isocyanate polyaddition process.
摘要翻译： R 1，R 2，R 3，m和n如本文所定义的对应于式“IMAGE”的二异氰酸酯的二异氰酸酯和异构体混合物通过对应于式“IMAGE”的二胺光气化制备，其中R 1，R 2，R 3，m和 n在-20℃至250℃的温度下定义。这些二异氰酸酯特别可用作通过异氰酸酯加聚方法生产聚氨酯的原料。
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公开(公告)号：US4720582A
公开(公告)日：1988-01-19
申请号：US523211
申请日：1983-08-15
IPC分类号： C07B61/00 , B01J23/00 , C07C67/00 , C07C209/00 , C07C209/36 , C07C209/72 , C07C211/49 , C08G18/32 , C07C87/52
CPC分类号： C08G18/3234
摘要： Diamines corresponding to the general formula ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 may be identical or different and represent hydrogen or straight- or branched-chain C.sub.1 -C.sub.12 alkyl groups, provided that two of the radicals,R.sup.1, R.sup.2 and R.sup.3, represent hydrogen, m and n each represent 0 or 1, provided that m+n=1; where m or n=0, the free valence is saturated by hydrogen, optionally in the form of isomeric mixtures, and optionally containing up to 35%, by weight, of the corresponding perhydrogenated diamines, and up to 10%, by weight, of the corresponding unhydrogenated aromatic diamines.Also, a process for preparing these diamines by catalytically-hydrogenating the corresponding aromatic diamines with 3 moles of hydrogen per mole of diamine, or catalytically-hydrogenating the corresponding dinitro compounds with 9 moles of hydrogen per mole of dinitro compound.
摘要翻译： 对应于通式“IMAGE”的二胺，其中R 1，R 2和R 3可以相同或不同，表示氢或直链或支链C 1 -C 12烷基，条件是基团R 1，R 2和R 3中的两个表示 氢，m和n各自表示0或1，条件是m + n = 1; 其中m或n = 0，任选地以异构混合物形式的氢饱和，并且任选地含有至多35重量％的相应的过氢化二胺，以及至多10重量％的 相应的未氢化芳族二胺。 另外，通过用相对于每摩尔二胺的3摩尔氢催化氢化相应的芳族二胺或每摩尔二硝基化合物以9摩尔氢催化氢化相应的二硝基化合物来制备这些二胺的方法。
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公开(公告)号：US4675437A
公开(公告)日：1987-06-23
申请号：US728357
申请日：1985-04-29
IPC分类号： C07C265/14 , C07C67/00 , C07C241/00 , C07C263/10 , C07C265/10 , C08G18/75 , G03G21/00 , C07C119/045
CPC分类号： C07C265/10 , C08G18/758
摘要： Cycloaliphatic triisocyanates or isomer mixtures of such triisocyanates corresponding to the formula ##STR1## in which R represents hydrogen or a C.sub.1 -C.sub.4 alkyl group are produced by phosgenating the corresponding cycloaliphatic triamines or isomer mixtures of such triamines or a salt thereof.These triisocyanates are useful in the production of polyisocyanate addition products, particularly polyurethane coatings and lacquers.
摘要翻译： 对应于其中R表示氢或C1-C4烷基的式“IMAGE”的这种三异氰酸酯的环脂族三异氰酸酯或异构体混合物是通过对这种三胺或其盐的相应的脂环族三胺或异构体混合物进行光气化而产生的。 这些三异氰酸酯可用于制备多异氰酸酯加成产物，特别是聚氨酯涂料和漆。
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公开(公告)号：US4603189A
公开(公告)日：1986-07-29
申请号：US728351
申请日：1985-04-29
IPC分类号： C08G18/00 , C07C67/00 , C07C241/00 , C07C263/10 , C07C265/12 , C07C265/14 , C08G18/72 , C08G18/74 , C09D175/00
CPC分类号： C07C265/12 , C08G18/74
摘要： Triisocyanates and isomeric mixtures of triisocyanates corresponding to the formula ##STR1## in which R represents hydrogen or an alkyl group having from 1 to 4 carbon atoms are made by phosgenating the corresponding triamine. These triisocyanates are particularly useful in the production of polyurethanes, especially polyurethane lacquer coats.
摘要翻译： 对应于其中R表示氢或具有1至4个碳原子的烷基的式“IMAGE”的三异氰酸酯的三异氰酸酯和异构体混合物通过对相应的三胺进行光气化而制备。 这些三异氰酸酯特别可用于生产聚氨酯，特别是聚氨酯漆包衣。
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5.发明授权Cycloaliphatic diisocyanates, optionally in the form of isomeric mixtures and a process for their preparation 失效任选呈异构混合物形式的环脂族二异氰酸酯及其制备方法
公开(公告)号：US4879409A
公开(公告)日：1989-11-07
申请号：US35417
申请日：1987-04-07
IPC分类号： C08G18/00 , C07C67/00 , C07C69/00 , C07C241/00 , C07C263/10 , C07C265/10 , C07C265/14 , C08G18/73 , C08G18/75
CPC分类号： C07C265/10 , C08G18/758
摘要： A diisocyanate corresponding to the formula ##STR1## in which R.sup.1, R.sup.2, R.sup.3, m and n are as defined herein is prepared by phosgenating a diamine corresponding to the formula ##STR2## in which R.sup.1, R.sup.2, R.sup.3, m and n are as defined herein. The diisocyanate may contain C.sub.1 -C.sub.12 -monoalkyl-substituted methylene-bis-(cyclohexylisocyanate)isomers in an amount of up to 40 wt. %. These new diisocyanates which are liquid at room temperature and compatible with polyols are particularly useful in the production of polyurethanes.
摘要翻译： R 1，R 2，R 3，m和n如本文所定义的对应于式“IMAGE”的二异氰酸酯通过将对应于其中R 1，R 2，R 3，m和n如下的式“IMAGE”的二胺光气化 本文定义。 异氰酸酯可以含有至多40重量％的C1-C12-单烷基取代的亚甲基 - 双（环己基异氰酸酯）异构体。 ％。 这些在室温下为液体并与多元醇相容的新型二异氰酸酯特别可用于生产聚氨酯。
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6.发明授权Cycloaliphatic diisocyanates optionally in the form of isomer mixtures and a process for their production 失效任选以异构体混合物形式的环脂族二异氰酸酯及其制备方法
公开(公告)号：US4879408A
公开(公告)日：1989-11-07
申请号：US35571
申请日：1987-04-07
IPC分类号： C08G18/00 , C07C67/00 , C07C69/00 , C07C241/00 , C07C263/10 , C07C265/10 , C07C265/14 , C08G18/73 , C08G18/75 , C08G18/76
CPC分类号： C07C265/10 , C08G18/758
摘要： Diisocyanates and isomer mixtures of diisocyanates corresponding to the formula ##STR1## in which R.sup.1, R.sup.2, m and n are as defined herein are produced by phosgenating diamines and isomer mixtures of diamines corresponding to the formula ##STR2## in which R.sup.1, R.sup.2, m and n are as defined herein. These diisocyanates which are liquid at room temperature and highly compatible with polyols are particularly useful in the production of polyurethanes.
摘要翻译： 对应于其中R 1，R 2，m和n如本文所定义的式“IMAGE”的二异氰酸酯的二异氰酸酯和异构体混合物通过对应于式“IMAGE”的二胺和二胺异构体混合物的光气化产生，其中R 1，R 2，m 和n如本文所定义。 这些在室温下为液体并与多元醇高度相容的二异氰酸酯特别可用于生产聚氨酯。
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7.发明授权Process for the preparation of N- and O-substituted diurethanes and/or polyurethanes 失效用于制备N-和O-取代的二氨基甲酸酯和/或聚氨酯的方法
公开(公告)号：US4593117A
公开(公告)日：1986-06-03
申请号：US678430
申请日：1984-12-05
IPC分类号： C07C269/04 , C07C67/00 , C07C209/00 , C07C209/62 , C07C211/44 , C07C239/00 , C07C271/12 , C07C271/24 , C07C271/26 , C07C271/28 , C07C271/44 , C08G18/70 , C07C125/073 , C07C125/077
CPC分类号： C08G18/701
摘要： Low molecular weight N- and O-substituted diurethanes and/or polyurethanes are prepared by reacting a diamine and/or polyamine containing a primary amino group with an N-aryl-0-alkyl urethane in the presence of at least one high boiling alcohol. This reaction may be carried out at a temperature of from 180.degree. to 350.degree. C. and a pressure of approximately 0.1 to 1,500 mbar. The arylamine corresponding to the N-ary-0-alkyl urethane which forms during this reaction is continuously removed from the reaction mixture.
摘要翻译： 在至少一种高沸点醇的存在下，使含有伯氨基的二胺和/或多胺与N-芳基-O-烷基氨基甲酸酯反应制备低分子量N-和O-取代的二氨基甲酸酯和/或聚氨酯。 该反应可以在180℃至350℃的温度和约0.1至1,500毫巴的压力下进行。 对应于在该反应期间形成的N-芳基 - 烷基氨基甲酸酯的芳基胺从反应混合物中连续除去。
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8.发明授权Fractionation and purification of mixtures of aromatic polyamines and use thereof 失效分离和纯化芳族多胺的混合物及其用途
公开(公告)号：US5672737A
公开(公告)日：1997-09-30
申请号：US623285
申请日：1996-03-28
申请人： Hartmut Knofel , Michael Brockelt
发明人： Hartmut Knofel , Michael Brockelt
IPC分类号： C08J3/00 , C07C209/72 , C07C209/84 , C07C209/86 , C07C211/34 , C07C211/50 , C07C263/10 , C07C265/14 , C08G18/32
CPC分类号： C07C209/86
摘要： The invention relates to a process for the fractionation and purification of mixtures of aromatic polyamines and to the use thereof.
摘要翻译： 本发明涉及芳族多胺混合物的分级和纯化方法及其用途。
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9.发明授权Fractionation and purification of aromatic polyamine mixtures and the use thereof 失效芳族多胺混合物的分级和纯化及其用途
公开(公告)号：US5679840A
公开(公告)日：1997-10-21
申请号：US623240
申请日：1996-03-28
申请人： Hartmut Knofel , Michael Brockelt
发明人： Hartmut Knofel , Michael Brockelt
IPC分类号： C07C209/72 , C07C209/84 , C07C209/86 , C07C211/34 , C07C211/50 , C07C263/10 , C07C265/14 , C08G59/50
CPC分类号： C07C209/86 , C07C209/84
摘要： The invention relates to a process for the fractionation and purification of aromatic polyamine mixtures and their use.
摘要翻译： 本发明涉及芳族多胺混合物的分级和纯化方法及其用途。
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公开(公告)号：US5359141A
公开(公告)日：1994-10-25
申请号：US863938
申请日：1992-04-06
IPC分类号： B01J27/02 , B01J27/10 , B01J27/16 , B01J31/02 , B01J31/04 , C07B61/00 , C07C209/78 , C07C209/82 , C07C211/50 , C07C209/84
CPC分类号： C07C209/78 , Y02P20/584
摘要： The invention relates to an improved process for the production of polynuclear aromatic polyamines by condensation of aniline with formaldehyde in the presence of water and acidic catalysts and working up of the reaction mixture by extraction with a hydrophobic solvent, the acid catalyst accumulating in the aqueous phase of the extraction step being reused.
摘要翻译： 本发明涉及通过在水和酸性催化剂的存在下苯胺与甲醛缩合制备多核芳族多胺的改进方法，并通过用疏水性溶剂萃取反应混合物进行处理，酸催化剂在水相中积聚 的提取步骤被重复使用。
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