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    2-amino-4-trichloropyridine derivatives
    1.
    发明授权
    2-amino-4-trichloropyridine derivatives 失效
    2-氨基-4-三氯吡啶衍生物

    公开(公告)号：US5216171A

    公开(公告)日：1993-06-01

    申请号：US681254

    申请日：1991-04-08

    申请人： Helmut Hagen ,  Hans Ziegler ,  Juergen Pfister ,  Gerhard Nilz ,  Gisela Lorenz ,  Juergen Dressel

    发明人： Helmut Hagen ,  Hans Ziegler ,  Juergen Pfister ,  Gerhard Nilz ,  Gisela Lorenz ,  Juergen Dressel

    IPC分类号： C05G3/08 ,  C07D213/74 ,  C07D213/75 ,  C07D213/76 ,  C07D401/04 ,  C07F9/58

    CPC分类号： C07D213/74 ,  C07D213/75 ,  C07D213/76 ,  C07D401/04 ,  C07F9/588 ,  Y02P60/218 ,  Y10S106/90

    摘要： 2-Amino-4-trichloromethylpyridines of the general formula I ##STR1## where R.sup.1 is hydrogen or C.sub.1 -C.sub.8 -alkyl,R.sup.2 is C.sub.1 -C.sub.8 -alkyl, C.sub.5 -C.sub.8 -cycloalkyl, C.sub.2 -C.sub.4 -alkenyl or phenyl, benzyl or phenylsulfonyl,--CX--R.sup.3, --SO.sub.2 R.sup.3 or --PX(OR.sup.4).sub.2 orR.sup.1 and R.sup.2 together form .dbd.CR.sup.5 R.sup.6 or --CO--Z--CO--,X is oxygen or sulfur,R.sup.3 is C.sub.1 -C.sub.20 -alkyl, C.sub.2 -C.sub.6 -alkenyl, amino, C.sub.1 -C.sub.6 -alkylamino, di-C.sub.1 -C.sub.6 -alkylamino, morpholino, piperidino, pyrazolidino or C.sub.1 -C.sub.8 -alkylcarbonylamino, substituted or unsubstituted phenylamino or benzylamino,R.sup.4 is C.sub.1 -C.sub.8 -alkyl, C.sub.1 -C.sub.8 -haloalkyl or substituted or unsubstituted phenyl,R.sup.5 is hydrogen, C.sub.1 -C.sub.4 -alkyl, or substituted or unsubstituted phenyl,R.sup.6 is substituted or unsubstituted phenyl,Z is substituted or unsubstituted ethylene which may be part of a substituted or unsubstituted cycloalkyl or cycloalkylene radical, substituted or unsubstituted ethenylene which may be part of a substituted or unsubstituted aromatic or heteroaromatic ring, and Z is not part of an unsubstituted phenyl radical, agriculturally useful salts thereof, processes for their preparation and the use thereof as nitrification inhibitors.

    摘要翻译： 通式I的2-氨基-4-三氯甲基吡啶其中R1是氢或C1-C8-烷基，R2是C1-C8-烷基，C5-C8-环烷基，C2-C4-烯基或苯基，苄基 或苯基磺酰基，-CX-R3，-SO2R3或-PX（OR4）2或R1和R2一起形成= CR5R6或-CO-Z-CO-，X是氧或硫，R3是C1-C20-烷基，C2- C 1 -C 6 - 烯基，氨基，C 1 -C 6 - 烷基氨基，二-C 1 -C 6烷基氨基，吗啉代，哌啶子基，吡唑烷基或C 1 -C 8烷基羰基氨基，取代或未取代的苯基氨基或苄基氨基，R 4是C 1 -C 8烷基， 卤代烷基或取代或未取代的苯基，R 5是氢，C 1 -C 4烷基或取代或未取代的苯基，R 6是取代或未取代的苯基，Z是可以是取代或未取代的环烷基或环亚烷基的一部分的取代或未取代的乙烯 取代或未取代的亚乙烯基，其可以是取代或未取代的芳族或杂芳族环的一部分，Z不是未取代的苯基的一部分，农业 其文化上有用的盐，其制备方法及其作为硝化抑制剂的用途。

    Cyanoquinoline compounds
    2.
    发明授权
    Cyanoquinoline compounds 失效
    氰基喹啉化合物

    公开(公告)号：US5565408A

    公开(公告)日：1996-10-15

    申请号：US423325

    申请日：1995-04-17

    申请人： Helmut Hagen ,  Juergen Pfister ,  Gunter Brill ,  Gerhard Nilz ,  Bruno Wuerzer ,  Karl-Otto Westphalen

    发明人： Helmut Hagen ,  Juergen Pfister ,  Gunter Brill ,  Gerhard Nilz ,  Bruno Wuerzer ,  Karl-Otto Westphalen

    IPC分类号： A01N43/42 ,  A01N25/32 ,  C07D215/48 ,  C07D215/50 ,  C07D215/54 ,  C07D215/56 ,  C07D401/04 ,  C07D401/06 ,  C07D401/12 ,  C07D401/14 ,  C07D413/04 ,  C07D413/14 ,  C07D417/04 ,  C07D215/28 ,  A01N43/40 ,  C07D215/26

    CPC分类号： C07D401/04 ,  A01N25/32 ,  C07D215/48 ,  C07D215/54 ,  C07D215/56 ,  C07D401/12

    摘要： Cyanoquinoline compounds Ia or Ib ##STR1## where R.sup.1 is CH.dbd.C(CN).sub.2 ; CH.dbd.N--N.dbd.CH--(5-quinolyl); methylsulfonyl; CH.dbd.NOH; halogen; hydroxyl; nitro; cyano; unsubstituted or substituted C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy or C.sub.1 -C.sub.4 -alkylthio, pyrrolidinyl; piperidinyl; morpholinyl; thiomorpholinyl; unsubstituted or substituted phenyl, phenoxy, phenylthio, phenyldithiolyl, phenylsulfonyl or pyrrolyl;m is 0, 1, 2 or 3;R.sup.2 is hydrogen; hydroxyl; halogen; C.sub.1 -C.sub.4 -alkoxy; --NR.sup.3 R.sup.4 ; --NR.sup.5 --CXR.sup.6 or --N.dbd.CR.sup.7 R.sup.8 ;R.sup.3 is hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 -alkyl;R.sup.4 is a radical R.sup.3 ; C.sub.1 -C.sub.4 -alkylamino; di-C.sub.1 -C.sub.4 -alkylamino; substituted C.sub.1 -C.sub.4 -alkyl; CH.dbd.N--(3-cyano-2-quinolinyl); or R.sup.3 and R.sup.4 together form C.sub.4 - or C.sub.3 -alkylene which may be interrupted by a hetero atom, or unsubstituted or substituted 1,3-butadienyl;R.sup.5 and R.sup.7 are each hydrogen or C.sub.1 -C.sub.4 -alkyl;R.sup.6 and R.sup.8 are each a radical R.sup.5 ; substituted C.sub.1 -C.sub.4 -alkyl; C.sub.3 -C.sub.7 -cycloalkyl; C.sub.1 -C.sub.4 -alkoxycarbonyl; unsubstituted or substituted phenyl or unsubstituted or substituted amino, andX is oxygen or sulfur,processes for their preparation and herbicides which contain them.

    摘要翻译： 氰基喹啉化合物Ia或Ib其中R 1是CH = C（CN）2; CH = N-N = CH-（5-喹啉基）; 甲基磺酰基; CH = NOH; 卤素; 羟; 硝基 氰基; 未取代或取代的C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基或C 1 -C 4 - 烷硫基，吡咯烷基; 哌啶基; 吗啉基 硫代吗啉基; 未取代或取代的苯基，苯氧基，苯硫基，苯基二硫代基，苯基磺酰基或吡咯基; m为0,1,2或3; R2是氢; 羟; 卤素; C1-C4-烷氧基; -NR3R4; -NR5-CXR6或-N = CR7R8; R3是氢或未取代的或取代的C1-C4-烷基; R4是一个基团R3; C 1 -C 4烷基氨基; 二-C 1 -C 4烷基氨基; 取代的C 1 -C 4 - 烷基; CH = N-（3-氰基-2-喹啉基）; 或者R 3和R 4一起形成可以被杂原子间隔的C4-或C3-亚烷基，或未取代或取代的1,3-丁二烯基; R5和R7各自为氢或C1-C4-烷基; R6和R8各自为基团R5; 取代的C 1 -C 4 - 烷基; C 3 -C 7 - 环烷基; C 1 -C 4烷氧基羰基; 未取代或取代的苯基或未取代或取代的氨基，X为氧或硫，其制备方法和含有它们的除草剂。

    2,3-substituted 1,8-naphthyridines, their preparation and their use as antidotes
    3.
    发明授权
    2,3-substituted 1,8-naphthyridines, their preparation and their use as antidotes 失效
    2,3-取代的1,8-萘啶，其制备及其作为抗体使用

    公开(公告)号：US5059240A

    公开(公告)日：1991-10-22

    申请号：US486867

    申请日：1990-03-01

    申请人： Helmut Hagen ,  Juergen Pfister ,  Hans Ziegler ,  Bruno Wuerzer ,  Karl-Otto Westphalen

    发明人： Helmut Hagen ,  Juergen Pfister ,  Hans Ziegler ,  Bruno Wuerzer ,  Karl-Otto Westphalen

    IPC分类号： A01N25/32 ,  A01N43/90 ,  C07D471/04 ,  C07D471/14

    CPC分类号： C07D471/04 ,  A01N25/32 ,  C07D471/14

    摘要： 2,3-substituted 1,8-naphthyridines of the general formula I ##STR1## where: R is hydrogen or C.sub.1 -C.sub.4 -alkyl (n=1 or 2)R.sup.1 is amino or substituted amino,XR.sup.5, where X is oxygen or sulfur and R.sup.5 is hydrogen, C.sub.1 -C.sub.12 -alkyl, C.sub.1 -C.sub.4 -alkoxycarbonyl-((C.sub.1 -C.sub.4)-alkyl, C.sub.5 -C.sub.8 -cycloakyl, substituted or unsubstituted phenyl, substituted or unsubstituted phenyl-(C.sub.1 -C.sub.3)-alkyl,halogen,isothiorhonium halide,C.sub.1 -C.sub.12 -alkyl,C.sub.1 -C.sub.4 -alkoxycarbonyl-C.sub.1 -C.sub.4 -alkyl,substituted or unsubstituted phenyl or phenyl-(C.sub.1 -C.sub.3)-alkyl,R.sup.2 is C.sub.1 -C.sub.4 -alkyl, cyano, carboxyl or a group ##STR2## where X is oxygen or sulfur,B is C.sub.1 -C.sub.6 -alkyl, C.sub.1 -C.sub.6 -alkoxy or alkylthio, amino, mono- or dialkylamino, where each alkyl radical is of 1 to 4 carbon atoms, morpholino, piperidyl, chlorine, bromine or substituted or unsubstituted phenyl,D is C.sub.1 -C.sub.4 alkyl or NH.sub.2 andR.sup.6 is hydrogen, C.sub.1 -C.sub.8 -alkyl or alkylcarbonyl,or R.sup.1 and R.sup.2 together are --NH--N.dbd.C(CH.sub.2)--,and their environmentally tolerated saltswith the proviso that R.sup.2 is not cyano, carboxyl or a carboxamido or carboxylic ester group when R.sup.1 is methyl, hydroxyl or amino (NH.sub.2), processes for their manufacture, and herbicidal agents containing a naphthyridine I as safener and at least one herbicidal active ingredient selected from the group consisting ofa) 2-(4-heteroaryloxy)- or 2-(4-aryloxy)-phenoxyacetic acid derivatives andb) cyclohexenone derivatives.

    摘要翻译： 具有通式I的2,3-取代的1,8-萘啶，其中：R是氢或C 1 -C 4 - 烷基（n = 1或2）R 1是氨基或取代的氨基，XR 5，其中X是氧 或（C 1 -C 4） - 烷基，C 5 -C 8 - 环烷基，取代或未取代的苯基，取代或未取代的苯基 - （C 1 -C 3） - 烷基，卤素，异卤卤化物，C 1 -C 12 - 烷基，C 1 -C 4 - 烷氧基羰基-C 1 -C 4烷基，取代或未取代的苯基或苯基 - （C 1 -C 3） - 烷基，R 2为C 1 -C 4烷基，氰基， 羧基或基团，其中X为氧或硫，B为C 1 -C 6 - 烷基，C 1 -C 6 - 烷氧基或烷硫基，氨基，单或二烷基氨基，其中每个烷基为1至4个碳原子，吗啉代 ，哌啶基，氯，溴或取代或未取代的苯基，D是C 1 -C 4烷基或NH 2，R 6是氢，C 1 -C 8 - 烷基或烷基羰基，或者R 1和R 2一起是-NH-N = C（CH 2） 其环境耐受性盐，条件是R2不是氰基，羧基或a 当R1是甲基，羟基或氨基（NH2）时，羧酰胺基或羧酸酯基，其制备方法和含有萘啶I作为安全剂的除草剂和至少一种除草活性成分，其选自a）2-（4 - 杂芳氧基） - 或2-（4-芳氧基） - 苯氧基乙酸衍生物和b）环己烯酮衍生物。

    Pyrrole derivatives useful as diazo and coupling components
    7.
    发明授权
    Pyrrole derivatives useful as diazo and coupling components 失效
    可用作重氮和偶联组分的吡咯衍生物

    公开(公告)号：US5003081A

    公开(公告)日：1991-03-26

    申请号：US461688

    申请日：1990-01-08

    申请人： Juergen Pfister ,  Matthias Wiesenfeldt ,  Karl-Heinz Etzbach

    发明人： Juergen Pfister ,  Matthias Wiesenfeldt ,  Karl-Heinz Etzbach

    IPC分类号： C07D207/325 ,  C07D207/337 ,  C07D207/34 ,  C07D207/36 ,  C07D207/38 ,  C07D401/04 ,  C07D403/06 ,  C07D405/06 ,  C07D409/04 ,  C07D417/06 ,  C09B55/00 ,  G03C1/58

    CPC分类号： C07D401/04 ,  C07D207/34 ,  C07D207/38 ,  C07D405/06 ,  G03C1/58

    摘要： Pyrrole derivatives of the formula ##STR1## or the tautomers thereof, where R.sup.1 is hydrogen, alkyl, alkenyl, alkynyl, cycloalkyl, phenyl, hetaryl or amino, it being possible for these radicals to be substituted,R.sup.2 is hydrogen, alkyl, benzyl, alkenyl, cycloalkyl or phenylR.sup.3 is hydrogen, alkyl, benzyl or alkenyl, or R.sup.2 and R.sup.3 together are ##STR2## where T.sup.1, T.sup.2 and T.sup.3 have the meanings mentioned in the description, or R.sup.2 and R.sup.3 together with the nitrogen connecting them are a heterocyclic radical,R.sup.4 is cyano, or carbamoyl or thiocarbamoyl, each of which can be substituted, or --C(NH.sub.2).dbd.N--OH,R.sup.5 is halogen, hydroxyl, alkanoyloxy or benzoyloxy andR.sup.6 is hydrogen, alkyl, phenyl, cyano, halogen, nitro, hydroxysulfonyl, alkanoyl, benzoyl or ##STR3## where T.sup.4 is alkyl or phenyl and T.sup.5 is the radical of an active methylene compound, hydroxyimino or the radical of a primary amine,with the proviso that R.sup.1, R.sup.2 and R.sup.3 are not all hydrogen, a process for the preparation of pyrrole derivatives (with R.sup.5 =hydroxyl) and the use of the novel products as diazo or coupling components are described.

    摘要翻译： 其中R 1是氢，烷基，烯基，炔基，环烷基，苯基，杂芳基或氨基，这些基团可以被取代，R 2是氢，烷基，苄基， 烯基，环烷基或苯基R3是氢，烷基，苄基或烯基，或者R2和R3一起是“IMAGE”，其中T1，T2和T3具有说明书中提及的含义，或者R 2和R 3与连接它们的氮一起是 杂环基，R 4为氰基或氨基甲酰基或硫代氨基甲酰基，各自可被取代，或-C（NH 2）= N-OH，R 5为卤素，羟基，烷酰氧基或苯甲酰氧基，R 6为氢，烷基，苯基，氰基， 卤素，硝基，羟基磺酰基，烷酰基，苯甲酰基或者其中T4是烷基或苯基，T5是活性亚甲基化合物，羟基亚氨基或伯胺基团的基团，条件是R1，R2和R3不是 所有氢，一种制备吡咯衍生物的方法（R5 = 羟基），并且描述了新产物作为重氮或偶联组分的用途。

    PROCESS FOR PRODUCING ELECTRODES FOR SOLAR CELLS
    8.
    发明申请
    PROCESS FOR PRODUCING ELECTRODES FOR SOLAR CELLS 有权
    用于生产太阳能电池的电极的方法

    公开(公告)号：US20110151614A1

    公开(公告)日：2011-06-23

    申请号：US12999329

    申请日：2009-06-09

    申请人： Rene Lochtman ,  Norbert Wagner ,  Juergen Kaczun ,  Juergen Pfister

    发明人： Rene Lochtman ,  Norbert Wagner ,  Juergen Kaczun ,  Juergen Pfister

    IPC分类号： H01L31/18

    CPC分类号： H01L31/022425 ,  Y02E10/50

    摘要： The invention relates to a process for producing electrodes for solar cells, the electrode being configured as an electrically conductive layer on a substrate (1) for solar cells, in which, in a first step, a dispersion comprising electrically conductive particles is transferred from a carrier (7) to the substrate (1) by irradiating the dispersion with a laser (9) and, in a second step, the dispersion transferred to the substrate (1) is dried and/or hardened to form the electrically conductive layer.

    摘要翻译： 本发明涉及一种用于制造太阳能电池用电极的方法，该电极被构造为用于太阳能电池的基板（1）上的导电层，其中在第一步骤中，将包含导电颗粒的分散体从 载体（7）通过用激光（9）照射分散体到基板（1），并且在第二步骤中，转移到基板（1）的分散体被干燥和/或硬化以形成导电层。

    Preparation of hydroxyanthraquinones
    9.
    发明授权
    Preparation of hydroxyanthraquinones 失效
    羟基四氢呋喃的制备

    公开(公告)号：US5081270A

    公开(公告)日：1992-01-14

    申请号：US599975

    申请日：1990-10-19

    申请人： Juergen Pfister ,  Michael Schiessl ,  Rainer Nachtrab

    发明人： Juergen Pfister ,  Michael Schiessl ,  Rainer Nachtrab

    IPC分类号： B01J27/08 ,  B01J19/20 ,  C07B61/00 ,  C07C46/00 ,  C07C46/02 ,  C07C50/34 ,  C07C50/38

    CPC分类号： C07C50/38 ,  B01J19/20 ,  C07C46/00 ,  C07C50/34

    摘要： 1-Hydroxyanthraquinones are prepared in an improved process by reacting phthalic anhydride or derivatives thereof with phenol derivatives in the presence of a Lewis acid as catalyst and in the presence or absence of a diluent, wherein the improvement comprises conducting the reaction in a self-cleaning apparatus having a mixing effect, at a temperature of from 120.degree. C. to 300.degree. C. for from 5 to 1,000 seconds, the self-cleaning apparatus having a mixing effect subjecting the reactants to a shear gradient of from 50 to 20,000 sec.sup.-1 with an energy input of from 0.01 to 0.2 kwh/kg of reactants.

    摘要翻译： 通过邻苯二甲酸酐或其衍生物与苯酚衍生物在路易斯酸作为催化剂的存在下和在存在或不存在稀释剂的情况下反应制备1-羟基蒽醌，其中改进包括在自清洁中进行反应 具有混合效果的装置，在120℃至300℃的温度下为5至1,000秒，所述自清洁装置具有将反应物的剪切梯度为50至20,000秒的混合效果， 1，能量输入为0.01至0.2千瓦时/ kg的反应物。