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    Aqueous polyurethane dispersions from solvent-free prepolymers using sulfonate diols
    1.
    发明授权
    Aqueous polyurethane dispersions from solvent-free prepolymers using sulfonate diols 失效
    使用磺酸二醇的无溶剂预聚物的水性聚氨酯分散体

    公开(公告)号：US4108814A

    公开(公告)日：1978-08-22

    申请号：US777206

    申请日：1977-03-14

    申请人： Helmut Reiff ,  Wolfgang Wenzel ,  Jurgen Grammel ,  Dieter Dieterich

    发明人： Helmut Reiff ,  Wolfgang Wenzel ,  Jurgen Grammel ,  Dieter Dieterich

    IPC分类号： C08G18/08 ,  C08G18/38 ,  C08G18/50 ,  C08G18/12 ,  C08G18/84

    CPC分类号： C08G18/5072 ,  C08G18/0828 ,  C08G18/3855 ,  C08G2170/80

    摘要： This invention relates to a process for the production of water dispersible polyurethanes by reacting polyisocyanates with sulphonate group containing diols. The sulphonate diols have the general formula: ##STR1## WHEREIN A and B, which may be the same or different, each represents a divalent aliphatic hydrocarbon group containing from 1 to 6 carbon atoms,R represents hydrogen, an aliphatic hydrocarbon group containing 1 to 4 carbon atoms or a phenyl group,X.sup.(+) represents an alkali metal cation or ammonium group which may be substitutedn and m, which may be the same or different, each represents an integer between 0 and 30 inclusive,o and p, represent 0 or 1, andq represents an integer of 0 or 2.Sufficient amounts of this diol are used to provide the final polymer with a sulphonate group content of about 0.1 to 6 wt.%. In a preferred embodiment, a prepolymer is formed in substance with the sulphonate bearing diol, the polyisocyanate and optionally other reactive hydrogen bearing compounds. The prepolymer is then chain extended with water and water soluble polyamines. This second stage may take place in water and the polyamines may carry sulphonate groups.

    摘要翻译： 本发明涉及通过使多异氰酸酯与含有磺酸酯基团的二醇反应制备水分散性聚氨酯的方法。 磺酸二醇具有以下通式：其中A和B可以相同或不同，各自表示含有1至6个碳原子的二价脂族烃基，R表示氢，含有1至6个碳原子的脂族烃基 4个碳原子或苯基，X（+）表示可以被取代的N和M的碱金属阳离子或铵基团，可以是相同或不同的，每个表示0和30之间的整数，O和P， 代表0或1，Q表示0或2的整数。

    Aromatic diisocyanates containing N,N-disubstituted sulfonamide groups and processes for their production
    3.
    发明授权
    Aromatic diisocyanates containing N,N-disubstituted sulfonamide groups and processes for their production 失效
    含有N，N-二取代磺酰胺基团的芳族二异氰酸酯及其制备方法

    公开(公告)号：US4496491A

    公开(公告)日：1985-01-29

    申请号：US401036

    申请日：1982-07-22

    申请人： Richard Kopp ,  Gerhard Grogler ,  Helmut Reiff ,  Dieter Dieterich

    发明人： Richard Kopp ,  Gerhard Grogler ,  Helmut Reiff ,  Dieter Dieterich

    IPC分类号： C08G18/00 ,  C07C67/00 ,  C07C241/00 ,  C07C265/14 ,  C07D295/26 ,  C08G18/77 ,  C07C119/048

    CPC分类号： C07D295/26 ,  C08G18/775

    摘要： Diisocyanates corresponding to the formula ##STR1## in which R.sup.1, R.sup.2, R.sup.3, R.sup.4, R.sup.5 and R.sup.6 (an isocyanate-containing radical) are as defined herein are made by several processes. These diisocyanates may be made by phosgenating the diamine in which the diisocyanate is based. They may also be produced by treating the bis-urethane of the tertiary alcohol corresponding to the diisocyanate with phosgene. Such diisocyanates may also be made by treating a specific type of bis-urea with hydrogen chloride. The diisocyanates corresponding to the above-given formula are particularly useful in the production of polyurethanes having good flame-proof and mechanical properties.

    摘要翻译： 其中R 1，R 2，R 3，R 4，R 5和R 6（含异氰酸酯的基团）如本文所定义的式“IMAGE”的二异氰酸酯通过几种方法制备。 这些二异氰酸酯可以通过使二异氰酸酯所基于的二胺光气化而制成。 它们也可以通过用光气处理对应于二异氰酸酯的叔醇的双 - 氨基甲酸酯来制备。 这种二异氰酸酯也可以通过用氯化氢处理特定类型的双脲来制备。 对应于上述给定配方的二异氰酸酯特别可用于生产具有良好的阻燃和机械性能的聚氨酯。

    Process for the production of plastic based on polyisocyanates
    4.
    发明授权
    Process for the production of plastic based on polyisocyanates 失效
    基于多异氰酸酯生产塑料的方法

    公开(公告)号：US4440901A

    公开(公告)日：1984-04-03

    申请号：US509910

    申请日：1983-07-01

    申请人： Helmut Reiff ,  Dieter Dieterich

    发明人： Helmut Reiff ,  Dieter Dieterich

    IPC分类号： C08G18/00 ,  C08G18/10 ,  C08G18/34 ,  C08G18/42 ,  C08G18/48 ,  C08G18/65 ,  C08G18/73 ,  C08G18/75

    CPC分类号： C08G18/75 ,  C08G18/10 ,  C08G18/34 ,  C08G18/4263 ,  C08G18/4887

    摘要： The present invention is directed to a process for the production of plastics based on an isocyanate-polyaddition product by(1) forming an isocyanate group-containing prepolymer from(a) a compound which has a molecular weight of from 146 to about 10,000, is substantially free from hydroxyl groups, contains at least two terminal carboxyl groups and optionally contains ether and/or ester groups,(b) excess quantities of an organic nonaromatic polyisocyanate which has at least one cyclohexane ring and exclusively contains aliphatically- and/or cycloaliphatically-bound isocyanate groups and(c) up to 10 equivalent percent, based on the isocyanate-reactive groups in component (a), of a compound which is monofunctional for the purposes of the isocyanate-addition reaction and,(2) reacting the product of step (1) with(d) a chain-lengthening agent such as water, a polyamine containing at least two primary and/or secondary amino groups or hydrazine or a derivative thereof containing at least two primary and/or secondary amino groups.

    摘要翻译： 本发明涉及通过（1）从（a）分子量为146至约10,000的化合物形成含异氰酸酯基的预聚物来生产基于异氰酸酯加聚产物的塑料的方法，是 基本上不含羟基，含有至少两个末端羧基并且任选地含有醚和/或酯基，（b）过量的有机非芳族聚异氰酸酯，其具有至少一个环己烷环并且仅含有脂族和/或脂环 结合异氰酸酯基团和（c）基于组分（a）中异氰酸酯反应性基团的异氰酸酯加成反应中单官能化合物的至多10当量％，和（2）使 步骤（1）与（d）链增长剂如水，含有至少两个伯和/或仲氨基的多胺或肼或其衍生物至少包含 两个伯和/或仲氨基。

    Inorganic-organic plastic
    6.
    发明授权
    Inorganic-organic plastic 失效
    无机 - 有机塑料

    公开(公告)号：US4142030A

    公开(公告)日：1979-02-27

    申请号：US795834

    申请日：1977-05-11

    申请人： Dieter Dieterich ,  Peter Markusch ,  Helmut Reiff

    发明人： Dieter Dieterich ,  Peter Markusch ,  Helmut Reiff

    IPC分类号： C04B28/00 ,  C04B28/24 ,  C08G18/08 ,  C08G18/30 ,  C08G18/38 ,  C08K3/34 ,  C08G18/32

    CPC分类号： C08G18/3895 ,  C04B28/003 ,  C04B28/24 ,  C08G18/0804 ,  C08G18/302 ,  C08K3/34

    摘要： An inorganic-organic plastic having improved strength, elasticity, dimensional stability with increase in temperature and flame resistace and adapted for use in filling cracks and cavities and for making materials useful in the building industry is prepared by (1) premixing (c) an organic compound having at least two reactive hydrogen and at least one non-ionic hydrophilic group with (b) an aqueous silicate and then mixing the resulting mixture with (a) an organic polyisocyanate or (2) mixing (a), (b) and (c) simultaneously and reacting the mixture thus obtained to form a colloidal xerosol.

    摘要翻译： 具有改善的强度，弹性，尺寸稳定性，温度升高和阻燃性并适用于填充裂纹和空腔以及用于制造建筑工业中有用的材料的无机 - 有机塑料是通过（1）预混合（c）有机 具有至少两个反应性氢和至少一个非离子亲水基团的化合物与（b）硅酸水溶液混合，然后将所得混合物与（a）有机多异氰酸酯或（2）混合（a），（b）和（ c）同时并使由此获得的混合物反应以形成胶态干燥剂。

    Leather tanning with oligourethanes
    7.
    发明授权
    Leather tanning with oligourethanes 失效
    皮革鞣制与低聚氨酯

    公开(公告)号：US4106897A

    公开(公告)日：1978-08-15

    申请号：US718489

    申请日：1976-08-30

    申请人： Harro Traubel ,  Helmut Reiff ,  Dieter Dieterich

    发明人： Harro Traubel ,  Helmut Reiff ,  Dieter Dieterich

    IPC分类号： C14C3/18

    CPC分类号： C14C3/18

    摘要： This invention is concerned with a method of tanning or retanning leather or pelts by treating them with an aqueous liquor containing water-soluble oligourethanes having ionic groups. The oligourethanes have a molecular weight of from 300 to 20,000 and they may be methylolated. The oligourethanes may be water-soluble owing to their ionic groups or they may contain hydrophilic segments to aid in their solubility in the aqueous liquor. The liquor may also contain up to an equal amount of formaldehyde or compounds which split off formaldehyde.

    摘要翻译： 本发明涉及通过用含有具有离子基团的水溶性低聚氨酯的含水液体处理皮革或毛皮来鞣制或复鞣的方法。 低聚氨酯的分子量为300至20,000，它们可以是羟甲基化的。 寡聚氨酯由于其离子基团而可能是水溶性的，或者它们可以含有亲水链段以帮助其在含水液体中的溶解度。 该液体还可含有相等量的甲醛或分解甲醛的化合物。

    Colored poly (urethane) urea powders
    9.
    发明授权
    Colored poly (urethane) urea powders 失效
    彩色聚氨酯脲粉

    公开(公告)号：US3970601A

    公开(公告)日：1976-07-20

    申请号：US573491

    申请日：1975-05-01

    申请人： Karl-Arnold Weber ,  Helmut Reiff ,  Dieter Dieterich

    发明人： Karl-Arnold Weber ,  Helmut Reiff ,  Dieter Dieterich

    IPC分类号： C08G18/08 ,  C09B69/10 ,  C08G18/00

    CPC分类号： C09B69/10 ,  C08G18/0804 ,  Y10T428/2998

    摘要： The instant invention relates to thermoplastic polyurea powders, optionally containing urethane groups, characterized byA. a smooth, substantially spherical or lenticular surface,B. an average particle diameter of 5 to 1,000.mu., preferably 10 to 200.mu.,C. a urea group content, and, optionally, a urethane group content, of 8 to 30% by weight,D. an ionic group content of 0.01-0.15 milliequivalents per gram of solids, preferably 0.02-0.1 milliequivalent per gram andE. 0.1 to 10% by weight, preferably 0.2 to 5% by weight, of an organic dye incorporated in the polymer molecule by way of at least one urethane and/or urea group,And the process of manufacture thereof.

    摘要翻译： 本发明涉及任选地含有氨基甲酸酯基团的热塑性聚脲粉末，其特征在于A.A SMOOTH，主要的球形或透明表面，B.平均颗粒直径为5至1,000μm，优选10至200μm，尿素组 内容和可选择的URETHANE集团内容，按重量计，8至30％，D.固体含量为0.01-0.15百万分之一的离子组含量，优选0.02-0.1百万分之一百克，E. 0.1至10％ 重量，优选0.2至5％重量，有机染料以聚合物分子的方式通过至少一个URURHANE和/或UREA集团的方式及其制造过程。

    Liquid organic polyisocyanates containing carboxyl and/or carboxylate groups
    10.
    发明授权
    Liquid organic polyisocyanates containing carboxyl and/or carboxylate groups 失效
    含羧基和/或羧酸酯基的液体有机多异氰酸酯

    公开(公告)号：US3959348A

    公开(公告)日：1976-05-25

    申请号：US527389

    申请日：1974-11-26

    申请人： Helmut Reiff ,  Peter Markusch ,  Dieter Dieterich

    发明人： Helmut Reiff ,  Peter Markusch ,  Dieter Dieterich

    IPC分类号： C09K17/00 ,  C04B38/02 ,  C07C67/00 ,  C07C239/00 ,  C07C269/02 ,  C08G18/08 ,  C08G18/34 ,  C08G18/38 ,  C08G18/42 ,  C08G18/80 ,  C09K17/30 ,  C07C119/048 ,  C07C155/02

    CPC分类号： C08G18/0823 ,  C08G18/348 ,  C08G18/3876 ,  C08G18/3895 ,  C08G18/4263 ,  C08G18/8003 ,  C08G18/8048

    摘要： Liquid organic polyisocyanates containing carboxyl and/or carboxylate groups are prepared by reacting liquid multicomponent mixtures of aromatic polyisocyanates having an isocyanato content of about 10 to about 20% by weight and a viscosity of about 8 cP to about 10,000 cP at 25.degree.C withA. a compound which contains carboxylate groups and hydrogen atoms which are reactive with isocyanate groups; orB. a hydroxycarboxylic or mercaptocarboxylic acid, wherebyBa. at least partial conversion of the carboxyl group into the corresponding carboxylate group by neutralization with a base is carried out simultaneously with or after the isocyanate addition reaction orBb. the hydroxycarboxylic acid or mercaptocarboxylic acid is of the kind in which the carboxyl groups are much less reactive with the isocyanate groups than are the hydroxyl or mercapto groups, the quantitative proportion of the reactants being so chosen that the products of the process have an isocyanate content of 10 to 40% by weight and a carboxyl or carboxylate group content of 0.1 to 10% by weight. The polyisocyanates can be used to make inorganic-organic plastics.

    摘要翻译： 含有羧基和/或羧酸酯基团的液体有机多异氰酸酯是通过使具有约10至约20重量％的异氰酸酯基含量的芳族多异氰酸酯的液体多组分混合物与25℃下的约8cP至约10,000cP的粘度与A 含有与异氰酸酯基团反应的羧酸酯基团和氢原子的化合物; 或B.羟基羧基或邻甲氧基苯甲酸，其中BA。 通过与基质中和的羧基相对于羧酸酯基团的至少部分转化与异氰酸酯添加反应或BB同时进行。 羟基羧基酸或羧甲氧基酸是这样的种类，其中羧酸基团与异羟基化合物没有反应，而不是羟基或甘油聚糖组，反应物的定量比例表明该方法的产物具有异氰酸酯的含量 10-40重量％，羧基或羧酸酯基含量为0.1〜10重量％。 多异氰酸酯可用于制备无机 - 有机塑料。