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    Naphthalene alkylation process
    1.
    发明授权
    Naphthalene alkylation process 失效
    萘烷基化方法

    公开(公告)号：US5034563A

    公开(公告)日：1991-07-23

    申请号：US505392

    申请日：1990-04-06

    申请人： Henry Ashjian ,  Quang N. Le ,  David O. Marler ,  Joosup Shim ,  Stephen S. Wong

    发明人： Henry Ashjian ,  Quang N. Le ,  David O. Marler ,  Joosup Shim ,  Stephen S. Wong

    IPC分类号： C07C2/66

    CPC分类号： C07C2/66 ,  C07C2529/08 ,  C07C2529/70

    摘要： Long chain alkyl substituted naphthalenes are produced by the alkylation of naphthalene with an olefin or other alkylating agent possessing at least 6 carbon atoms, usually 12 to 20 carbon atoms, in the presence of an alkylation catalyst comprising a zeolite which contains cations having a radius of at least 2.5 .ANG.. Cations of this size may be provided by hydrated cations such as hydrated ammonium, sodium or potassium cations or by organoammonium cations such as tetraalkylammonium cations. The zeolite is usually a large pore size ze USY. The presence of the bulky cations in the zeolite increases the selectivity of the catalyst for the production of long chain mono-alkyl substituted naphthalenes in preference to more highly substituted products.

    摘要翻译： 长链烷基取代的萘是通过在含有至少6个碳原子，通常12至20个碳原子的烯烃或其它烷基化剂的烷基化催化剂的存在下，在包含含有阳离子的沸石的烷基化催化剂的存在下， 至少2.5 ANGSTROM。 这种大小的阳离子可由水合阳离子如水合铵，钠或钾阳离子或有机铵阳离子如四烷基铵阳离子提供。 沸石通常是大孔尺寸的USY。 沸石中大体积阳离子的存在增加了催化剂对于生产长链单烷基取代的萘的选择性，优于更高取代的产物。

    Synthetic lubricants
    4.
    发明授权
    Synthetic lubricants 失效
    合成润滑剂

    公开(公告)号：US5008460A

    公开(公告)日：1991-04-16

    申请号：US358108

    申请日：1989-05-30

    申请人： William E. Garwood ,  Quang N. Le ,  Joosup Shim ,  Stephen S. Wong

    发明人： William E. Garwood ,  Quang N. Le ,  Joosup Shim ,  Stephen S. Wong

    IPC分类号： C10G50/02 ,  C10G69/12

    CPC分类号： C10G50/02 ,  C10G69/126

    摘要： Synthetic lubricating oils having a predetermined alkylaromatic structure are prepared from a mixture of mono- or dialkenyl benzene with an aliphatic olefin by free-radical reaction in the presence of ditertiary-butyl peroxide, for example. Equivalent napthalene derivatives may be substituted for the dialkenyl benzene. The oils that are formed exhibit a high Viscosity Index, and a low pour point. The viscosity of the synthetic lube stock produced may be controlled by changing the amount of peroxide used.

    摘要翻译： 具有预定烷基芳族结构的合成润滑油例如由二叔丁基过氧化物存在下，由单 - 或二烯基苯与脂族烯烃的混合物通过自由基反应制备。 等价萘衍生物可代替二苯基苯。 所形成的油表现出高粘度指数和低倾点。 可以通过改变所用过氧化物的量来控制所生产的合成润滑油的粘度。

    Stabilization of polyalpha-olefins
    5.
    发明授权
    Stabilization of polyalpha-olefins 失效
    聚α-烯烃的稳定化

    公开(公告)号：US5107049A

    公开(公告)日：1992-04-21

    申请号：US593171

    申请日：1990-10-05

    申请人： Quang N. Le ,  Joosup Shim ,  Stephen S. Wong

    发明人： Quang N. Le ,  Joosup Shim ,  Stephen S. Wong

    IPC分类号： B01J29/04 ,  C07C2/12 ,  C07C2/66 ,  C07C37/14 ,  C07C51/347

    CPC分类号： C07C51/347 ,  B01J29/04 ,  C07C2/12 ,  C07C2/66 ,  C07C37/14 ,  C07C2529/06 ,  C07C2529/70

    摘要： The thermal stability of poly alpha-olefin (PAO) lubricant basestocks are improved by reacting an aromatic compound with the alpha-olefin oligomer. The PAO materials are prepared by oligomerization of olefins such as 1-decene in the presence of a Lewis acid oligomerization catalyst. The resulting lubricant basestock product exhibits high viscosity, viscosity index and low pour point in addition to the unique enhancement in thermal stability. The reaction between the PAO and the aromatic is carried out in the presence of a solid, cyrstalline alkylation catalyst identified by a specific X-ray diffraction pattern. The preferred catalyst for this purpose is the material known as MCM-22.

    摘要翻译： 通过使芳族化合物与α-烯烃低聚物反应来改善聚α-烯烃（PAO）润滑剂基础油料的热稳定性。 在路易斯酸低聚催化剂存在下，通过烯烃如1-癸烯的低聚制备PAO材料。 除了独特的热稳定性提高之外，所得润滑剂基础油产品显示出高粘度，粘度指数和低倾点。 PAO和芳族化合物之间的反应是在特定X射线衍射图谱鉴定的固体，Cyrstalline烷基化催化剂的存在下进行的。 用于该目的的优选催化剂是称为MCM-22的材料。

    Process for making a blended lubricant
    8.
    发明授权
    Process for making a blended lubricant 失效
    制造混合润滑剂的方法

    公开(公告)号：US5306416A

    公开(公告)日：1994-04-26

    申请号：US898365

    申请日：1992-06-15

    申请人： Quang N. Le ,  Stephen S. Wong

    发明人： Quang N. Le ,  Stephen S. Wong

    IPC分类号： C10G27/12 ,  C10M101/02 ,  C10M171/02 ,  C10G71/00 ,  C10M129/22

    CPC分类号： C10M171/02 ,  C10M101/02 ,  C10G2400/10 ,  C10M2203/10 ,  C10M2203/1006 ,  C10M2203/1025 ,  C10M2203/1045 ,  C10M2203/1065 ,  C10M2203/1085

    摘要： A blended mineral oil lubricant is made having a higher viscosity index than predicted by calculating the viscosity index from an ASTM standard method designated D 341-87 or by calculating the average of the actual VI based on the proportion of each component of the blend. The lubricant is treated with a peroxide compound, preferably an organic peroxide such as di-tertiary butyl peroxide to increase the viscosity index. The treated lubricant is blended with a lubricant of lower viscosity index to achieve a blended lubricant having an enhanced viscosity index. The lubricant charge stock and blending component can be a wax-derived lubricant fraction or a conventional light neutral or heavy neutral mineral oil.

    摘要翻译： 制备混合矿物油润滑剂，其具有比通过由标准D 341-87的ASTM标准方法计算粘度指数更高的粘度指数，或通过基于混合物各组分的比例计算实际VI的平均值。 润滑剂用过氧化物化合物，优选有机过氧化物如二叔丁基过氧化物处理以增加粘度指数。 将经处理的润滑剂与较低粘度指数的润滑剂混合以获得具有增强粘度指数的混合润滑剂。 润滑剂装料和共混组分可以是蜡衍生的润滑剂部分或常规的轻质中性或重质中性矿物油。

    Method of noble metal-zeolite catalyst activation with Bronsted acid compound
    9.
    发明授权
    Method of noble metal-zeolite catalyst activation with Bronsted acid compound 失效
    用布朗斯台德酸化合物对贵金属 - 沸石催化剂活化的方法

    公开(公告)号：US4826792A

    公开(公告)日：1989-05-02

    申请号：US193151

    申请日：1988-05-05

    申请人： Quang N. Le ,  Stephen S. Wong

    发明人： Quang N. Le ,  Stephen S. Wong

    IPC分类号： B01J29/90 ,  B01J38/60 ,  B01J38/66 ,  B01J29/38 ,  B01J23/96

    CPC分类号： B01J29/90 ,  B01J38/60 ,  B01J38/66 ,  Y10S502/517

    摘要： A method for reactivating noble metal-containing zeolites containing sulfur oxide poisoned noble metal such as oxygen regenerated platinum zeolite beta catalysts, by contacting the catalyst with an acidic aqueous solution having a pH below about 7. The solution contains a Bronsted acid compound having a dissociation constant ranging from about 1.times.10.sup.-14 to about 2.times.10.sup.-1.

    摘要翻译： 通过使催化剂与pH低于约7的酸性水溶液接触，使含有硫氧化物中毒的贵金属如贵金属贵金属如氧再生的铂沸石β催化剂再生的方法。该溶液含有具有解离性的布朗斯台德酸化合物 常数范围为约1×10-14至约2×10 -1。

    Lubricant production process with product viscosity control
    10.
    发明授权
    Lubricant production process with product viscosity control 失效
    润滑油生产过程与产品粘度控制

    公开(公告)号：US5037528A

    公开(公告)日：1991-08-06

    申请号：US517958

    申请日：1990-04-30

    申请人： William E. Garwood ,  Quang N. Le ,  Stephen S. Wong

    发明人： William E. Garwood ,  Quang N. Le ,  Stephen S. Wong

    IPC分类号： C10G65/04 ,  C10G67/04

    CPC分类号： C10G65/043 ,  C10G67/04

    摘要： High viscosity index, low pour point lubricants are produced by the oligomerization of a wax-derived lubricant fraction. The fraction may be produced from slack wax or de-oiled wax by hydroisomerization over zeolite beta or hydrocracking/isomerization over an amorphous catalyst followed by selective dewaxing, preferably by catalytic dewaxing over a highly shape selective zeolite such as ZSM-23. The preferred peroxides are ditertiary alkyl peroxides such as ditertiary butyl peroxide (DTBP) and are typically used at temperatures of 100.degree.-300.degree. C.

    摘要翻译： 高粘度指数，低倾点润滑剂是通过蜡衍生的润滑剂部分的低聚产生的。 馏分可以通过在沸石β上的加氢异构化或非晶态催化剂上的加氢裂化/异构化，然后进行选择性脱蜡，优选通过高度形状选择性沸石如ZSM-23的催化脱蜡来由松散蜡或脱油蜡产生。 优选的过氧化物是二叔烷基过氧化物，例如二叔丁基过氧化物（DTBP），通常在100-300℃的温度下使用