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    Process for regeneration of ionic liquid catalyst
    2.
    发明授权
    Process for regeneration of ionic liquid catalyst 有权
    离子液体催化剂再生方法

    公开(公告)号：US09346042B2

    公开(公告)日：2016-05-24

    申请号：US14369215

    申请日：2012-12-28

    申请人： SHELL OIL COMPANY ,  CHINA UNIVERSITY OF PETROLEUM

    发明人： Rui Zhang ,  Zhichang Liu ,  Chunming Xu ,  Xianghai Meng ,  Peter Anton August Klusener

    IPC分类号： B01J38/64 ,  B01J31/40 ,  B01J31/02 ,  B01J38/66

    CPC分类号： B01J31/4069 ,  B01J31/0279 ,  B01J31/40 ,  B01J38/66 ,  B01J2231/44 ,  C07C2/58 ,  C07C2527/125 ,  C10G29/205 ,  Y02P20/584 ,  C07C9/16

    摘要： The present invention relates to a regeneration process for producing a regenerated ionic liquid catalyst from solids formed in an ionic liquid alkylation process wherein a first ionic liquid is used as a catalyst which is a composite ionic liquid comprising ammonium cations, and anions being composite coordinate anions derived from two or more metal salts, the regeneration process comprising (a) removing the solids from the reaction zone of the alkylation process; and (b) subsequently treating the solids with a second ionic liquid made from an ammonium salt as cation, and an aluminum salt as anion which is the same as the aluminum salt present in the first ionic liquid.

    摘要翻译： 本发明涉及一种用于在离子液体烷基化方法中形成的固体生产再生离子液体催化剂的再生方法，其中使用第一离子液体作为催化剂，其为包含铵阳离子的复合离子液体，阴离子为复合配位阴离子 衍生自两种或更多种金属盐，再生方法包括（a）从烷基化方法的反应区除去固体; 和（b）随后用由铵盐形成的第二离子液体作为阳离子处理固体，和作为阴离子的铝盐与第一离子液体中存在的铝盐相同。

    PROCESS FOR REGENERATION OF IONIC LIQUID CATALYST
    3.
    发明申请
    PROCESS FOR REGENERATION OF IONIC LIQUID CATALYST 有权
    离子液体催化剂再生方法

    公开(公告)号：US20150231624A1

    公开(公告)日：2015-08-20

    申请号：US14369215

    申请日：2012-12-28

    申请人： SHELL OIL COMPANY ,  CHINA UNIVERSITY OF PETROLEUM

    发明人： Rui Zhang ,  Zhichang Liu ,  Chunming Xu ,  Xianghai Meng ,  Peter Anton August Klusener

    IPC分类号： B01J31/40 ,  B01J38/66 ,  B01J31/02

    CPC分类号： B01J31/4069 ,  B01J31/0279 ,  B01J31/40 ,  B01J38/66 ,  B01J2231/44 ,  C07C2/58 ,  C07C2527/125 ,  C10G29/205 ,  Y02P20/584 ,  C07C9/16

    摘要： The present invention relates to a regeneration process for producing a regenerated ionic liquid catalyst from solids formed in an ionic liquid alkylation process wherein a first ionic liquid is used as a catalyst which is a composite ionic liquid comprising ammonium cations, and anions being composite coordinate anions derived from two or more metal salts, wherein at least one metal salt is an aluminium salt and any further metal salt is a salt of a metal selected from the group consisting of Group IB elements of the Periodic Table, Group IIB elements of the Periodic Table and transition elements of the Periodic Table, the regeneration process comprising (a) removing the solids from the reaction zone of the alkylation process; and (b) subsequently treating the solids with a second ionic liquid made from an ammonium salt as cation, and an aluminium salt as anion which is the same as the aluminium salt present in the first ionic liquid. The process of the invention provides means to more efficiently run an ionic liquid alkylation process with less impact on the environment than processes known from the prior art.

    摘要翻译： 本发明涉及一种用于在离子液体烷基化方法中形成的固体生产再生离子液体催化剂的再生方法，其中使用第一离子液体作为催化剂，其为包含铵阳离子的复合离子液体，阴离子为复合配位阴离子 衍生自两种或更多种金属盐，其中至少一种金属盐是铝盐，并且任何另外的金属盐是选自元素周期表第IB族元素，元素周期表IIB族元素的金属盐 和周期表的过渡元素，再生过程包括（a）从烷基化方法的反应区除去固体; 和（b）随后用由铵盐形成的第二离子液体作为阳离子处理固体，和作为阴离子的铝盐与第一离子液体中存在的铝盐相同。 本发明的方法提供了比现有技术已知的方法更有效地运行对环境的影响较小的离子液体烷基化方法的方法。

    Process for passivation by a nitrogen-containing compound of a zeolitic catalyst, in particular a hydrocracking catalyst
    6.
    发明申请
    Process for passivation by a nitrogen-containing compound of a zeolitic catalyst, in particular a hydrocracking catalyst 有权
    通过沸石催化剂，特别是加氢裂化催化剂的含氮化合物钝化的方法

    公开(公告)号：US20140042057A1

    公开(公告)日：2014-02-13

    申请号：US13610250

    申请日：2012-09-11

    申请人： Pierre Dufresne ,  Mickael Bremaud ,  Pauline Galliou ,  Sharath Kirumakki

    发明人： Pierre Dufresne ,  Mickael Bremaud ,  Pauline Galliou ,  Sharath Kirumakki

    IPC分类号： B01J29/04 ,  C10G47/16

    CPC分类号： B01J29/04 ,  B01J23/883 ,  B01J23/885 ,  B01J29/06 ,  B01J37/20 ,  B01J38/66 ,  C10G47/06 ,  C10G47/16 ,  C10G47/20

    摘要： The invention relates to a process for ex-situ treatment of a catalyst that contains at least one hydrogenating phase, and at least one amorphous silica-alumina or a zeolite that contains acid sites, whereby said process comprises: A stage for introducing nitrogen by contact at a temperature that is less than 100° C., with at least one basic nitrogen-containing compound that is ammonia or a compound that can be decomposed into ammonia, with said compound being introduced at a rate of 0.5-10% by weight (expressed in terms of N), and A sulfurization/activation stage with a gas that contains hydrogen and hydrogen sulfide at a temperature of at least 250° C., with this stage being carried out before or after the stage for introducing said nitrogen-containing compound, and the catalyst that is obtained is optionally dried. This treatment allows a rapid, effective start-up on the hydrocracking unit.

    摘要翻译： 本发明涉及一种用于非原位处理含有至少一个氢化相的催化剂和至少一种含有酸性位点的无定形二氧化硅 - 氧化铝或沸石的方法，其中所述方法包括：通过接触引入氮的阶段 在低于100℃的温度下，使用至少一种碱性含氮化合物，其为氨或可分解成氨的化合物，所述化合物以0.5-10重量％的速率引入（ 以N表示）和A在含至少250℃的温度下含有氢和硫化氢的气体的硫化/活化阶段，该阶段在引入含氮的 将所得催化剂任选地干燥。 这种处理可以在加氢裂化装置上快速，有效启动。

    PROCESS FOR REGENERATING A CATALYST
    8.
    发明申请
    PROCESS FOR REGENERATING A CATALYST 有权
    再生催化剂的方法

    公开(公告)号：US20120165417A1

    公开(公告)日：2012-06-28

    申请号：US13333409

    申请日：2011-12-21

    申请人： Gerrit Leendert BEZEMER ,  Stephen NKRUMAH ,  Johannes Theodorus Maria SMITS

    发明人： Gerrit Leendert BEZEMER ,  Stephen NKRUMAH ,  Johannes Theodorus Maria SMITS

    IPC分类号： C07C1/04 ,  B01J38/66

    CPC分类号： B01J23/94 ,  B01J21/063 ,  B01J23/8892 ,  B01J37/0009 ,  B01J38/10 ,  B01J38/12 ,  B01J38/66 ,  C10G2/332 ,  C10G2300/70

    摘要： A process for regenerating one or more deactivated cobalt comprising Fischer-Tropsch catalyst particle(s), comprising the steps of: (i) oxidising the catalyst particle(s) at a temperature between 20 and 400° C.; (ii) treating the catalyst particle(s) for more than 5 minutes, (iii) drying the catalyst particle(s); and (iv) optionally reducing the catalyst particle(s) with hydrogen or a hydrogen comprising gas. This process may be preceded by a step in which Fischer-Tropsch product is removed from the catalyst particle(s). The treatment is performed using carbon dioxide and a liquid comprising ammonia.

    摘要翻译： 一种用于再生一种或多种包含费 - 托催化剂颗粒的失活的钴的方法，包括以下步骤：（i）在20-400℃的温度下氧化催化剂颗粒; （ii）处理催化剂颗粒超过5分钟，（iii）干燥催化剂颗粒; 和（iv）任选地用氢或包含气体的氢还原催化剂颗粒。 此过程之前可以是从催化剂颗粒中除去费 - 托产物的步骤。 使用二氧化碳和包含氨的液体进行处理。

    Method of restoring catalytic activity to a spent hydrotreating catalyst, the resulting restored catalyst, and a method of hydroprocessing
    9.
    发明授权
    Method of restoring catalytic activity to a spent hydrotreating catalyst, the resulting restored catalyst, and a method of hydroprocessing 有权
    对废加氢处理催化剂恢复催化活性的方法，所得到的还原催化剂和加氢处理方法

    公开(公告)号：US08168557B2

    公开(公告)日：2012-05-01

    申请号：US12878825

    申请日：2010-09-09

    申请人： Josiane Marie-Rose Ginestra ,  James Dallas Seamans ,  Kenneth Scott Lee

    发明人： Josiane Marie-Rose Ginestra ,  James Dallas Seamans ,  Kenneth Scott Lee

    IPC分类号： B01J27/02 ,  B01J27/047 ,  B01J27/043 ,  B01J23/00 ,  B01J23/10 ,  C10G17/00 ,  C10G19/00 ,  C10G21/00 ,  C10G25/00 ,  C10G27/00 ,  C10G29/00 ,  C10G31/00

    CPC分类号： B01J27/02 ,  B01J23/94 ,  B01J37/20 ,  B01J38/12 ,  B01J38/48 ,  B01J38/50 ,  B01J38/66 ,  C10G45/04 ,  C10G45/34 ,  C10G45/46 ,  C10G45/60 ,  C10G47/02 ,  C10G49/02 ,  C10G2300/44 ,  C10G2300/70

    摘要： A method of restoring catalytic activity to a spent hydroprocessing catalyst that has a first carbon concentration. The concentration of carbon on the spent hydroprocessing catalyst is reduced to provide a carbon-reduced catalyst having a second carbon concentration that is less than the first carbon concentration. The carbon-reduced catalyst is exposed to a solution, comprising a chelating agent and a solvent, for an aging time period sufficient to provide for a restored catalytic activity thereby resulting in an aged catalyst having incorporated therein the chelating agent and the solvent. The aged catalyst is exposed to conditions, including a drying temperature, so as to remove from the aged catalyst a portion of the solvent without removing a significant portion of the chelating agent from the aged catalyst thereby resulting in a dried aged catalyst. The dried aged catalyst is then sulfur treated to thereby provide a restored catalyst. The restored catalyst and those catalysts made by the treatment method can be used in a hydroprocessing process comprising contacting the restored catalyst with a hydrocarbon feedstock under hydroprocessing conditions.

    摘要翻译： 对具有第一碳浓度的废加氢处理催化剂恢复催化活性的方法。 减少处于废加氢处理催化剂上的碳的浓度以提供具有小于第一碳浓度的第二碳浓度的碳减少催化剂。 将碳减少的催化剂暴露于包含螯合剂和溶剂的溶液中，老化时间段足以提供恢复的催化活性，从而导致其中掺入螯合剂和溶剂的老化催化剂。 将老化的催化剂暴露于包括干燥温度的条件下，以便从老化的催化剂中除去一部分溶剂，而不从老化的催化剂中除去大量的螯合剂，从而导致干燥的老化催化剂。 然后对干燥的老化催化剂进行硫处理，从而提供恢复的催化剂。 还原的催化剂和通过处理方法制备的那些催化剂可用于加氢处理方法，包括在加氢处理条件下将恢复的催化剂与烃原料接触。