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1.发明申请公开(公告)号：US20150197688A1
公开(公告)日：2015-07-16
申请号：US14411332
申请日：2013-06-25
发明人： Mario Such , Gerhard Schoetz , Andreas Langner
CPC分类号： C09K11/7706 , C01B33/18 , C03B19/066 , C03B2201/06 , C03B2201/32 , C03B2201/34 , C03B2201/36 , C03C1/006 , C03C3/06 , C03C3/061 , C03C4/12 , C03C2201/06 , C03C2201/3488 , C03C2201/36 , C09K11/025
摘要： The invention relates to a method for producing a doped SiO2 slurry in which an SiO2 suspension is brought into interaction with at least one doping solution, wherein the SiO2 suspension and/or the doping solution act on one another in the form of an atomised spray, the average droplet diameter of which is in the range between 10 μm and 100 μm. The invention further relates to the use of an SiO2 slurry doped by the atomised spray method for the production of doped quartz glass, particularly for the production of laser-active quartz glass.
摘要翻译： 本发明涉及一种制备掺杂SiO 2浆料的方法，其中SiO 2悬浮液与至少一种掺杂溶液相互作用，其中SiO 2悬浮液和/或掺杂溶液以雾化喷雾的形式彼此作用， 其平均液滴直径在10μm和100μm之间的范围内。 本发明还涉及通过雾化喷雾方法掺杂的SiO 2浆料用于生产掺杂石英玻璃的用途，特别是用于生产激光活性石英玻璃。
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公开(公告)号：US20150086462A1
公开(公告)日：2015-03-26
申请号：US14397484
申请日：2013-04-25
发明人： Mario Such , Gerhard Schoetz , Andreas Langner
IPC分类号： C01B33/18
CPC分类号： C01B33/18 , C03B19/108 , C03C1/026
摘要： The invention relates to a process for producing SiO2 granules by freezing and re-thawing an SiO2 suspension, wherein a separation of liquid and sediment composed of agglomerated SiO2 particles occurs in the course of thawing, the liquid removed is decanted and the residual moisture in the sediment is removed by a drying step with formation of the SiO2 granules. According to the invention, an auxiliary comprising alkali metal-free bases in the form of nitrogen hydrides is added to the suspension to set the pH greater than 7.
摘要翻译： 本发明涉及一种通过冷冻和再融化SiO 2悬浮液来生产SiO 2颗粒的方法，其中在解冻过程中发生由附聚的SiO 2颗粒组成的液体和沉积物的分离，将去除的液体倾倒并将残留的水分 通过形成SiO 2颗粒的干燥步骤除去沉淀物。 根据本发明，向悬浮液中加入包含氮化氢形式的不含碱金属的碱的辅助剂，使pH大于7。
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3.发明申请QUARTZ GLASS TUBE AS A SEMI-FINISHED PRODUCT FOR AN OPTICAL COMPONENT AND METHOD FOR PRODUCING SAID QUARTZ GLASS TUBE 审中-公开QUARTZ玻璃管作为光学部件的半精加工产品和生产标准石英玻璃管的方法公开(公告)号：US20150017440A1
公开(公告)日：2015-01-15
申请号：US14372734
申请日：2013-01-17
发明人： Gerhard Schötz , Karsten Bräuer , Richard Schmidt , Peter Bauer , Andreas Schultheis , Clemens Schmitt , Andreas Langner
IPC分类号： C03B37/012
CPC分类号： C03B37/01211 , C03B37/01222 , C03B37/01228 , C03B37/0124 , C03B37/01291 , C03B37/01426 , C03B2201/12 , C03B2201/31 , C03B2203/04 , C03B2203/12 , C03B2203/23 , C03B2203/31 , C03B2203/32 , C03B2203/34 , Y02P40/57 , Y10T428/2935
摘要： A quartz glass tube as a semi-finished product for an optical component that has an inner bore extending along a tube centre axis for the acceptance of a core rod and a tube wall limited by an inner casing surface and an outer casing surface is already known; within said tube wall an inner region made of a first quartz glass and an outer region made of a second quartz glass with a different index of refraction surrounding the inner region contact one another at a contact surface which runs around the centre axis. In order to provide a quartz glass on this basis that facilitates the production of optical components for special applications such as laser-activated optical components in wand or fibre form, the invention states that the contact surface has a non-round course in the radial cross-section and the inner casing surface has a circular course.
摘要翻译： 作为用于光学部件的半成品的石英玻璃管是具有沿着管中心轴延伸以便接受芯棒的内孔和由内壳表面和外壳表面限制的管壁的半成品已知 ; 在所述管壁内，围绕内部区域的折射率不同的由第二石英玻璃制成的内部区域由第一石英玻璃制成的外部区域和围绕中心轴线的接触表面彼此接触。 为了在此基础上提供石英玻璃，有助于生产用于特殊应用的光学部件，例如以棒或纤维形式的激光激活光学部件，本发明指出接触表面具有径向十字形的非圆形过程 并且内壳表面具有圆形过程。
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4.发明授权公开(公告)号：US09296639B2
公开(公告)日：2016-03-29
申请号：US14420572
申请日：2013-08-08
发明人： Gerhard Schoetz , Karsten Bräuer , Richard Schmidt , Peter Bauer , Andreas Schultheis , Paul Bödiger , Andreas Langner
IPC分类号： C03B37/012
CPC分类号： C03B37/01291 , C03B2201/12 , C03B2203/12
摘要： The invention relates to a plasma deposition process for producing an optical preform, which is characterized by a cladding glass layer having a non-round internal cross-section together with high fluorine doping and axially and radially specified dopant distribution, which in the simplest case is as uniform as possible. For this purpose, a two-stage method is proposed, wherein a substrate body having a non-round cross-section is first reshaped into a coated substrate body having a circular cross-section in that a POD filling layer made of quartz glass having the nominal fluorine concentration is deposited onto a present filling surface and rounded by grinding, and then in the second stage of the method a POD sheathing glass layer made of fluorine-doped quartz glass and having a circular-ring-shaped cross-section is deposited.
摘要翻译： 本发明涉及一种用于制造光学预型件的等离子体沉积工艺，其特征在于具有非圆形内部横截面的包层玻璃层以及高氟掺杂以及轴向和径向指定的掺杂剂分布，其最简单的情况是 尽可能统一。 为此，提出了一种两级方法，其中具有非圆形横截面的基底主体首先重新成形为具有圆形横截面的涂覆基底主体，其中由具有圆形横截面的石英玻璃制成的POD填充层具有 将标称氟浓度沉积在当前的填充表面上并通过研磨进行圆化，然后在该方法的第二阶段中沉积由氟掺杂的石英玻璃制成并具有圆环形横截面的POD护套玻璃层。
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公开(公告)号：US10851008B2
公开(公告)日：2020-12-01
申请号：US15938156
申请日：2018-03-28
发明人： Walter Lehmann , Mario Such , Thomas Kayser , Andreas Langner , Gerhard Schötz
摘要： A method for producing a component with portions of a rare earth metal-doped quartz glass, an intermediate product containing voids and consisting of a SiO2 raw material doped with rare earth metal is introduced into a sinter mold the interior of which is bordered by a carbonaceous mold wall, and is melted therein into the component by gas pressure sintering at a maximum temperature above 1500° C. A shield is arranged between the mold wall and the intermediate product. In order to indicate a modified gas pressure sintering method that ensures the production of rare earth metal-doped quartz glass with reproducible properties, a bulk material of amorphous SiO2 particles with a layer thickness of at least 2 mm is used as the shield, the softening temperature thereof being at least 20° C. higher than the softening temperature of the doped SiO2 raw material, and the bulk material being gas-permeable at the beginning of the melting of the intermediate product, and the bulk material sintering during melting into an outer layer that is gas-tight to a pressure gas.
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公开(公告)号：US20180282196A1
公开(公告)日：2018-10-04
申请号：US15938156
申请日：2018-03-28
发明人： Walter Lehmann , Mario Such , Thomas Kayser , Andreas Langner , Gerhard Schötz
摘要： A method for producing a component with portions of a rare earth metal-doped quartz glass, an intermediate product containing voids and consisting of a SiO2 raw material doped with rare earth metal is introduced into a sinter mold the interior of which is bordered by a carbonaceous mold wall, and is melted therein into the component by gas pressure sintering at a maximum temperature above 1500° C. A shield is arranged between the mold wall and the intermediate product. In order to indicate a modified gas pressure sintering method that ensures the production of rare earth metal-doped quartz glass with reproducible properties, a bulk material of amorphous SiO2 particles with a layer thickness of at least 2 mm is used as the shield, the softening temperature thereof being at least 20° C. higher than the softening temperature of the doped SiO2 raw material, and the bulk material being gas-permeable at the beginning of the melting of the intermediate product, and the bulk material sintering during melting into an outer layer that is gas-tight to a pressure gas.
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公开(公告)号：US20170203995A1
公开(公告)日：2017-07-20
申请号：US15473425
申请日：2017-03-29
IPC分类号： C03B37/014 , C03B37/027
CPC分类号： C03B37/01426 , C03B37/01211 , C03B37/027 , C03B2201/12 , C03B2201/23 , Y02P40/57 , Y10T428/2935
摘要： The aim of the invention is to improve a generally known method for producing quartz glass doped with fluorine, wherein SiO2 particles are formed in the presence of fluorine by means of a plasma deposition process, deposited in layers on an outer envelope of a cylindrical quartz glass substrate body rotating about its longitudinal axis, and vitrified to form a layer of quartz glass with a fluorine content of at least 1.5 wt. %, in such a way that a quartz glass semifinished product with a high fluorine content, characterised by a high basic transmission in the UV wavelength range, is obtained. To this end, the substrate body has at least one reservoir layer of quartz glass at least in the region of the outer envelope thereof, having a minimum hydroxyl group content of 200 wt. ppm and/or a minimum hydrogen content of 1×1017 molecules/cm3, and the substrate body is either fully or partially removed following the deposition of the quartz glass layer doped with fluorine.
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公开(公告)号：US11952302B2
公开(公告)日：2024-04-09
申请号：US17395791
申请日：2021-08-06
发明人： Stefan Ochs , Thomas Kayser , Martin Trommer , Andreas Langner , Sascha Pihan , Kay Schuster , Michael Hünermann
CPC分类号： C03B19/143 , C03B19/1423 , C03B19/1453 , C03C3/06 , C03B2201/12 , C03B2207/30 , C03C2201/12 , C03C2203/40
摘要： A process for the production of a fluorinated quartz glass including the steps of generating SiO2 particles in a synthesis burner; depositing the resulting SiO2 particles into a body; and vitrifying the resulting body, wherein a fluorinating agent having a boiling point greater than or equal to −10° C. is supplied to the synthesis burner.
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公开(公告)号：US11512017B2
公开(公告)日：2022-11-29
申请号：US16804760
申请日：2020-02-28
发明人： Jacqueline Plass , Dörte Schönfeld , Clemens Schmitt , Alexander Laaz , Andreas Langner , Gerhard Schötz , Walter Lehmann , Michael Hünermann , Stefan Weidlich , Jürgen Schäfer
IPC分类号： C03B37/012
摘要： In known methods for producing a glass component, a void-containing intermediate product containing doped or non-doped SiO2 is inserted into a sheath tube composed of glass, which has a longitudinal axis and an inner bore, and is thermally treated therein. In order to subject the intermediate product to a thermal and/or reactive treatment that is reproducible and uniform in its effect from this starting point, it is proposed in one embodiment that into the sheath tube's inner bore a first gas-permeable gas diffuser is inserted which is displaceable along the sheath tube's longitudinal axis and is pressed against the intermediate product during the thermal treatment.
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公开(公告)号：US20200277217A1
公开(公告)日：2020-09-03
申请号：US16804760
申请日：2020-02-28
发明人： Jacqueline Plass , Dörte Schönfeld , Clemens Schmitt , Alexander Laaz , Andreas Langner , Gerhard Schötz , Walter Lehmann , Michael Hünermann , Stefan Weidlich , Jürgen Schäfer
IPC分类号： C03B37/012
摘要： In known methods for producing a glass component, a void-containing intermediate product containing doped or non-doped SiO2 is inserted into a sheath tube composed of glass, which has a longitudinal axis and an inner bore, and is thermally treated therein. In order to subject the intermediate product to a thermal and/or reactive treatment that is reproducible and uniform in its effect from this starting point, it is proposed in one embodiment that into the sheath tube's inner bore a first gas-permeable gas diffuser is inserted which is displaceable along the sheath tube's longitudinal axis and is pressed against the intermediate product during the thermal treatment.
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