Process for fabricating fluorine-doped sol-gel article
    3.
    发明授权
    Process for fabricating fluorine-doped sol-gel article 失效
    氟掺杂溶胶凝胶制品的制备方法

    公开(公告)号:US06223563B1

    公开(公告)日:2001-05-01

    申请号:US09528382

    申请日:2000-03-17

    IPC分类号: C03B37016

    摘要: The invention reflects discovery of a liquid phase doping technique that, unlike previous techniques, exhibits very little fluorine depletion upon subsequent heating. The invention involves the steps of providing a silica sol comprising a tetraalkylammonium hydroxide and a di-, tri-, or tetraalkylammonium fluoride, the sol having pH of about 10 to about 14, adding a gelling agent to the sol to induce gelation, casting or extruding the sol to form a gel body, and then drying, heat treating, and sintering the body. Advantageously, the fluorine-containing compound is tetramethylammonium fluoride.

    摘要翻译: 本发明反映了液相掺杂技术的发现,其与以前的技术不同,在随后的加热中表现出非常少的氟耗尽。 本发明涉及提供包含四烷基氢氧化铵和二 - ,三 - 或四烷基氟化铵,pH约为10至约14的溶胶的二氧化硅溶胶的步骤,向溶胶中加入胶凝剂以诱导凝胶化,浇铸或 挤出溶胶以形成凝胶体,然后干燥,热处理和烧结体。 有利地,含氟化合物是四甲基氟化铵。

    Process of making biomaterials
    5.
    发明申请
    Process of making biomaterials 审中-公开
    制作生物材料的工艺

    公开(公告)号:US20080098771A1

    公开(公告)日:2008-05-01

    申请号:US11975143

    申请日:2007-10-17

    IPC分类号: C03B8/00

    摘要: An improved sol-gel process is disclosed for the making of large synthetic silica based bioactive materials objects crack-free. A series of ordered mesoporous SiO2—CaO—P2O5 sol-gel glasses which are highly bioactive are synthesized through a sol-gel process. The mesoporous glasses are highly bioactive compared with conventional ones, due to the increased textural characteristics, i.e. surface area. The bioactivity tests point out that the surface area, porosity, and 3D-structure become more important than chemical composition during the apatite crystallization stage in these materials, due to the very high textural parameters obtained. The product is intended to be used for tissue engineering applications.

    摘要翻译: 公开了一种改进的溶胶 - 凝胶方法,用于制造无合金二氧化硅的生物活性物质。 通过溶胶 - 凝胶合成了一系列具有高度生物活性的有序介孔SiO 2 -C 2 O 2 P 2 O 5 O 5溶胶凝胶玻璃 处理。 由于增加的结构特征,即表面积,介孔玻璃与常规玻璃相比具有高生物活性。 生物活性测试指出,由于获得的非常高的结构参数,表面积,孔隙率和3D结构在这些材料中的磷灰石结晶阶段期间比化学成分更重要。 该产品旨在用于组织工程应用。

    Flame hydrolysis process for the manufacture of glass bodies of doped silica glass
    6.
    发明申请
    Flame hydrolysis process for the manufacture of glass bodies of doped silica glass 审中-公开
    用于制造掺杂石英玻璃的玻璃体的火焰水解方法

    公开(公告)号:US20040250573A1

    公开(公告)日:2004-12-16

    申请号:US10826078

    申请日:2004-04-16

    IPC分类号: C03B019/06

    摘要: A process for manufacturing glass bodies of doped silicate glass is disclosed. The process involves flame hydrolysis, wherein precursors for the forming of the doped glass are fed together with fuel gases into a single burner. A first formed body is generated on a target. The doped silicate glass produced in this way offers a low density of defects and a small breadth of striae. Preferably the first formed body is subsequently formed into a second formed body having a larger breadth and a smaller length than the first formed body. Thereby, the breadth of striae and the density of defects in the doped silica glass is further reduced.

    摘要翻译: 公开了一种用于制造掺杂硅酸盐玻璃的玻璃体的方法。 该方法涉及火焰水解,其中用于形成掺杂玻璃的前体与燃料气体一起进料到单个燃烧器中。 在目标上产生第一成形体。 以这种方式生产的掺杂硅酸盐玻璃提供低密度的缺陷和小的条纹。 优选地,第一成形体随后形成具有比第一成形体更大的宽度和更小的长度的第二成形体。 因此,掺杂石英玻璃中的条纹宽度和缺陷密度进一步降低。

    Glass composition and method for producing glass article
    9.
    发明申请
    Glass composition and method for producing glass article 失效
    玻璃制品的玻璃组合物和方法

    公开(公告)号:US20070197366A1

    公开(公告)日:2007-08-23

    申请号:US10576291

    申请日:2004-10-19

    IPC分类号: C03C3/00 C03B5/16

    摘要: The glass composition of the present invention is an inorganic glass composition in which the volume ratio of helium with a mass number of 3 to helium with a mass number of 4, namely 3He/4He in the glass (0° C., 1 atm) is smaller than the volume ratio 3He/4He in the atmosphere. The method of producing a glass article of the present invention includes the steps of: melting a glass raw material by heating; homogenizing molten glass; forming the molten glass into a desired shape; and cooling the shaped glass to room temperature, in which helium with a certain mass ratio is dissolved in the glass material so that the glass article of the present invention is obtained.

    摘要翻译: 本发明的玻璃组合物是将质量数为4的氦质量数为3的氦的体积比为3的无机玻璃组合物,即He / 玻璃(0℃,1大气压)中的He小于He气体中的He / 4 He体积比。 本发明的玻璃制品的制造方法包括以下步骤:通过加热熔化玻璃原料; 均质化熔融玻璃; 将所述熔融玻璃形成为期望的形状; 将成形玻璃冷却至室温,将具有一定质量比的氦溶解在玻璃材料中,得到本发明的玻璃制品。

    Bragg grating optical fiber
    10.
    发明授权
    Bragg grating optical fiber 失效
    布拉格光栅光纤

    公开(公告)号:US06993241B2

    公开(公告)日:2006-01-31

    申请号:US10658606

    申请日:2003-09-08

    IPC分类号: G02B6/16 G02B6/34

    摘要: The present invention provides an optical fiber providing high photosensitivity in the absence of hydrogen loading as well as a low numerical aperture. One aspect of the present invention relates to an optical fiber including a core, the core comprising silica doped with at least about 6 mol % germania and at least about 0.9 wt % fluorine; and a cladding surrounding the core. The optical fiber of the present invention is suitable for the production of fiber Bragg gratings.

    摘要翻译: 本发明提供了一种在不存在氢负载和低数值孔径下提供高光敏性的光纤。 本发明的一个方面涉及一种包括芯的光纤,所述芯包括掺杂有至少约6mol%的氧化锗和至少约0.9wt%的氟的二氧化硅; 以及围绕芯的包层。 本发明的光纤适用于制造光纤布拉格光栅。