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公开(公告)号：US08339025B2
公开(公告)日：2012-12-25
申请号：US12787800
申请日：2010-05-26
申请人： Toshitaka Nakamura , Hironaka Fujii , Hiroaki Miyagawa , Rajesh Mukherjee , Bin Zhang , Amane Mochizuki
发明人： Toshitaka Nakamura , Hironaka Fujii , Hiroaki Miyagawa , Rajesh Mukherjee , Bin Zhang , Amane Mochizuki
CPC分类号： C09K11/7774 , B82Y30/00 , C04B35/44 , C04B35/6268 , C04B35/6342 , C04B2235/3217 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/3418 , C04B2235/441 , C04B2235/443 , C04B2235/5445 , C04B2235/5454 , C04B2235/6581 , C04B2235/764 , C04B2235/9653 , C04B2235/9661 , H01L33/502 , H01L33/505
摘要： Some embodiments provide luminescent ceramics which have a lower amount of dopant than conventional luminescent ceramics. In some embodiments, the luminescent ceramic comprises a host material comprising a rare earth element and at least one rare earth dopant, wherein the rare earth dopant may be about 0.01% to 0.5% of the rare earth atoms present in the material. Some embodiments provide luminescent ceramic comprising: a polycrystalline phosphor represented by the formula (A1-xEx)3B5O12. Some embodiments provide a light-emitting device comprising a luminescent ceramic disclosed herein.
摘要翻译： 一些实施例提供具有比常规发光陶瓷更少量的掺杂剂的发光陶瓷。 在一些实施方案中，发光陶瓷包括含有稀土元素和至少一种稀土掺杂剂的主体材料，其中稀土掺杂剂可以是材料中存在的稀土原子的约0.01％至0.5％。 一些实施方案提供发光陶瓷，其包括：由式（A1-xEx）3B5O12表示的多晶磷光体。 一些实施方案提供包含本文公开的发光陶瓷的发光装置。
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公开(公告)号：US20120218736A1
公开(公告)日：2012-08-30
申请号：US13402668
申请日：2012-02-22
申请人： Bin Zhang , Amane Mochizuki , Toshitaka Nakamura , Guang Pan , Hiroaki Miyagawa , Hironaka Fujii
发明人： Bin Zhang , Amane Mochizuki , Toshitaka Nakamura , Guang Pan , Hiroaki Miyagawa , Hironaka Fujii
CPC分类号： E21B41/00 , B32B18/00 , C04B35/44 , C04B35/50 , C04B2235/3217 , C04B2235/3218 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/3418 , C04B2235/5409 , C04B2235/6025 , C04B2235/6562 , C04B2235/6565 , C04B2235/6581 , C04B2235/6586 , C04B2235/764 , C04B2235/9646 , C04B2235/9653 , C04B2237/343 , C04B2237/582 , C09K11/7774 , E21B43/11852 , E21B47/18 , H01L33/502
摘要： Disclosed herein are phosphor compositions having high gadolinium concentrations. Some embodiments include a thermally stable ceramic body comprising an emissive layer, wherein said emissive layer comprises a compound represented by the formula (A1-x-zGdxDz)3B5O12, wherein: D is a first dopant selected from the group consisting of Nd, Er, Eu, Mn, Cr, Yb, Sm, Tb, Ce, Pr, Dy, Ho, Lu and combinations thereof; A is selected from the group consisting of Y, Lu, Ca, La, Tb, and combinations thereof; B is selected from the group consisting of Al, Mg, Si, Ga, In, and combinations thereof; x is in the range of about 0.20 and about 0.80; and z is in the range of about 0.001 and about 0.10. Also disclosed are thermally stable ceramic bodies that can include the composition of formula I. Methods of making the ceramic body and a lighting device including the ceramic body are also disclosed.
摘要翻译： 本文公开了具有高钆浓度的荧光体组合物。 一些实施方案包括包含发光层的热稳定陶瓷体，其中所述发射层包含由式（A1-x-zGdxDz）3B5O12表示的化合物，其中：D是选自Nd，Er， Eu，Mn，Cr，Yb，Sm，Tb，Ce，Pr，Dy，Ho，Lu及其组合; A选自Y，Lu，Ca，La，Tb及其组合; B选自Al，Mg，Si，Ga，In及其组合; x在约0.20和约0.80的范围内; z在约0.001至约0.10的范围内。 还公开了可以包括式I的组合物的热稳定陶瓷体。还公开了制造陶瓷体的方法和包括陶瓷体的照明装置。
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3.发明申请METHOD OF MANUFACTURING PHOSPHOR TRANSLUCENT CERAMICS AND LIGHT EMITTING DEVICES 有权制造磷光透明陶瓷和发光器件的方法公开(公告)号：US20120119148A1
公开(公告)日：2012-05-17
申请号：US13358344
申请日：2012-01-25
IPC分类号： C09K11/78
CPC分类号： C09K11/7774 , C04B35/44 , C04B35/634 , C04B35/638 , C04B2235/3217 , C04B2235/3225 , C04B2235/3229 , C04B2235/443 , C04B2235/5454 , C04B2235/6562 , C04B2235/6582 , C04B2235/662 , C04B2235/663 , C04B2235/664 , C04B2235/764 , C04B2235/768
摘要： Disclosed herein is a method of increasing the luminescence efficiency of a translucent phosphor ceramic. Other embodiments are methods of manufacturing a phosphor translucent ceramic having increased luminescence. Another embodiment is a light emitting device comprising a phosphor translucent ceramic made by one of these methods.
摘要翻译： 本文公开了提高半透明磷光体陶瓷的发光效率的方法。 其他实施例是制造具有增加的发光的荧光体半透明陶瓷的方法。 另一个实施例是包括通过这些方法之一制成的荧光体半透明陶瓷的发光器件。
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公开(公告)号：US08169136B2
公开(公告)日：2012-05-01
申请号：US12389207
申请日：2009-02-19
申请人： Toshitaka Nakamura , Hironaka Fujii , Hiroaki Miyagawa , Rajesh Mukherjee , Bin Zhang , Amane Mochizuki
发明人： Toshitaka Nakamura , Hironaka Fujii , Hiroaki Miyagawa , Rajesh Mukherjee , Bin Zhang , Amane Mochizuki
CPC分类号： C09K11/7774 , B82Y30/00 , C04B35/44 , C04B35/62675 , C04B35/6268 , C04B35/63416 , C04B35/6342 , C04B2235/3206 , C04B2235/3217 , C04B2235/3222 , C04B2235/3225 , C04B2235/3229 , C04B2235/3418 , C04B2235/3427 , C04B2235/5454 , C04B2235/656 , C04B2235/6581 , C04B2235/80 , C04B2235/9653 , C04B2235/9661 , H01L25/0753 , H01L33/502 , H01L2924/0002 , H05B33/14 , H01L2924/00
摘要： A light emitting device comprising a light emitting component that emits light with a first peak wavelength, and at least one sintered ceramic plate over the light emitting component is described. The at least one sintered ceramic plate is capable of absorbing at least a portion of the light emitted from said light emitting component and emitting light of a second peak wavelength, and has a total light transmittance at the second peak wavelength of greater than about 40%. A method for improving the luminance intensity of a light emitting device comprising providing a light emitting component and positioning at least one translucent sintered ceramic plate described above over the light emitting component is also disclosed.
摘要翻译： 一种发光装置，其包括发射具有第一峰值波长的光的发光部件和在发光部件上方的至少一个烧结陶瓷板。 所述至少一个烧结陶瓷板能够吸收从所述发光组件发射的光的至少一部分并发射第二峰值波长的光，并且在第二峰值波长处的总光线透射率大于约40％ 。 还公开了一种用于提高发光器件的亮度强度的方法，包括提供发光部件并且将上述至少一个半透明烧结陶瓷板定位在发光部件上。
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公开(公告)号：US08137587B2
公开(公告)日：2012-03-20
申请号：US12388936
申请日：2009-02-19
IPC分类号： C09K11/08
CPC分类号： C09K11/7774 , C04B35/44 , C04B35/634 , C04B35/638 , C04B2235/3217 , C04B2235/3225 , C04B2235/3229 , C04B2235/443 , C04B2235/5454 , C04B2235/6562 , C04B2235/6582 , C04B2235/662 , C04B2235/663 , C04B2235/664 , C04B2235/764 , C04B2235/768
摘要： Disclosed herein is a method of increasing the luminescence efficiency of a translucent phosphor ceramic. Other embodiments are methods of manufacturing a phosphor translucent ceramic having increased luminescence. Another embodiment is a light emitting device comprising a phosphor translucent ceramic made by one of these methods.
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公开(公告)号：US20100207512A1
公开(公告)日：2010-08-19
申请号：US12389177
申请日：2009-02-19
CPC分类号： C09K11/7774 , C04B35/44 , C04B35/634 , C04B2235/3217 , C04B2235/3225 , C04B2235/3229 , C04B2235/3418 , C04B2235/441 , C04B2235/443 , C04B2235/5409 , C04B2235/5454 , C04B2235/6562 , C04B2235/6582 , C04B2235/664 , C04B2235/764 , C04B2235/77 , H01L33/502 , H01L33/507
摘要： One embodiment provides a method for fabricating a translucent phosphor ceramic compact comprising: heating a precursor powder to at least about 1000° C. under a reducing atmosphere to provide a pre-conditioned powder, forming an intermediate compact comprising the pre-conditioned powder and a flux material, and heating the intermediate compact under a vacuum to a temperature of at least about 1400° C. In another embodiment, the compact may be a cerium doped translucent phosphor ceramic compact comprising yttrium, aluminum, oxygen, and cerium sources. Another embodiment may be a light emitting device having the phosphor translucent ceramic provided as described herein.
摘要翻译： 一个实施例提供了一种制造半透明磷光体陶瓷压块的方法，包括：在还原气氛下将前体粉末加热至至少约1000℃，以提供预调节的粉末，形成包含预调节粉末的中间成型体和 助熔剂材料，并在真空下将中间成型体加热到至少约1400℃的温度。在另一个实施方案中，压块可以是包含钇，铝，氧和铈源的铈掺杂的半透明磷光体陶瓷压块。 另一个实施例可以是具有如本文所述提供的荧光体半透明陶瓷的发光器件。
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公开(公告)号：US08968600B2
公开(公告)日：2015-03-03
申请号：US13402668
申请日：2012-02-22
申请人： Bin Zhang , Amane Mochizuki , Toshitaka Nakamura , Guang Pan , Hiroaki Miyagawa , Hironaka Fujii
发明人： Bin Zhang , Amane Mochizuki , Toshitaka Nakamura , Guang Pan , Hiroaki Miyagawa , Hironaka Fujii
IPC分类号： C09K11/77 , E21B41/00 , E21B43/1185 , E21B47/18 , B32B18/00 , C04B35/44 , C04B35/50 , H01L33/50
CPC分类号： E21B41/00 , B32B18/00 , C04B35/44 , C04B35/50 , C04B2235/3217 , C04B2235/3218 , C04B2235/3224 , C04B2235/3225 , C04B2235/3229 , C04B2235/3418 , C04B2235/5409 , C04B2235/6025 , C04B2235/6562 , C04B2235/6565 , C04B2235/6581 , C04B2235/6586 , C04B2235/764 , C04B2235/9646 , C04B2235/9653 , C04B2237/343 , C04B2237/582 , C09K11/7774 , E21B43/11852 , E21B47/18 , H01L33/502
摘要： Disclosed herein are phosphor compositions having high gadolinium concentrations. Some embodiments include a thermally stable ceramic body comprising an emissive layer, wherein said emissive layer comprises a compound represented by the formula (A1-x-zGdxDz)3B5O12, wherein: D is a first dopant selected from the group consisting of Nd, Er, Eu, Mn, Cr, Yb, Sm, Tb, Ce, Pr, Dy, Ho, Lu and combinations thereof; A is selected from the group consisting of Y, Lu, Ca, La, Tb, and combinations thereof; B is selected from the group consisting of Al, Mg, Si, Ga, In, and combinations thereof; x is in the range of about 0.20 to about 0.80; and z is in the range of about 0.001 to about 0.10. Also disclosed are thermally stable ceramic bodies that can include the composition of formula I. Methods of making the ceramic body and a lighting device including the ceramic body are also disclosed.
摘要翻译： 本文公开了具有高钆浓度的荧光体组合物。 一些实施方案包括包含发光层的热稳定陶瓷体，其中所述发射层包含由式（A1-x-zGdxDz）3B5O12表示的化合物，其中：D是选自Nd，Er， Eu，Mn，Cr，Yb，Sm，Tb，Ce，Pr，Dy，Ho，Lu及其组合; A选自Y，Lu，Ca，La，Tb及其组合; B选自Al，Mg，Si，Ga，In及其组合; x在约0.20至约0.80的范围内; z在约0.001至约0.10的范围内。 还公开了可以包括式I的组合物的热稳定陶瓷体。还公开了制造陶瓷体的方法和包括陶瓷体的照明装置。
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公开(公告)号：US20120194066A1
公开(公告)日：2012-08-02
申请号：US13436676
申请日：2012-03-30
申请人： Toshitaka Nakamura , Hironaka Fujii , Hiroaki Miyagawa , Rajesh Mukherjee , Bin Zhang , Amane Mochizuki
发明人： Toshitaka Nakamura , Hironaka Fujii , Hiroaki Miyagawa , Rajesh Mukherjee , Bin Zhang , Amane Mochizuki
IPC分类号： H01J1/62
CPC分类号： C09K11/7774 , B82Y30/00 , C04B35/44 , C04B35/62675 , C04B35/6268 , C04B35/63416 , C04B35/6342 , C04B2235/3206 , C04B2235/3217 , C04B2235/3222 , C04B2235/3225 , C04B2235/3229 , C04B2235/3418 , C04B2235/3427 , C04B2235/5454 , C04B2235/656 , C04B2235/6581 , C04B2235/80 , C04B2235/9653 , C04B2235/9661 , H01L25/0753 , H01L33/502 , H01L2924/0002 , H05B33/14 , H01L2924/00
摘要： A light emitting device comprising a light emitting component that emits light with a first peak wavelength, and at least one sintered ceramic plate over the light emitting component is described. The at least one sintered ceramic plate is capable of absorbing at least a portion of the light emitted from said light emitting component and emitting light of a second peak wavelength, and has a total light transmittance at the second peak wavelength of greater than about 40%. A method for improving the luminance intensity of a light emitting device comprising providing a light emitting component and positioning at least one translucent sintered ceramic plate described above over the light emitting component is also disclosed.
摘要翻译： 一种发光装置，其包括发射具有第一峰值波长的光的发光部件和在发光部件上方的至少一个烧结陶瓷板。 所述至少一个烧结陶瓷板能够吸收从所述发光组件发射的光的至少一部分并发射第二峰值波长的光，并且在第二峰值波长处的总光线透射率大于约40％ 。 还公开了一种用于提高发光器件的亮度强度的方法，包括提供发光部件并且将上述至少一个半透明烧结陶瓷板定位在发光部件上。
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公开(公告)号：US08123981B2
公开(公告)日：2012-02-28
申请号：US12389177
申请日：2009-02-19
CPC分类号： C09K11/7774 , C04B35/44 , C04B35/634 , C04B2235/3217 , C04B2235/3225 , C04B2235/3229 , C04B2235/3418 , C04B2235/441 , C04B2235/443 , C04B2235/5409 , C04B2235/5454 , C04B2235/6562 , C04B2235/6582 , C04B2235/664 , C04B2235/764 , C04B2235/77 , H01L33/502 , H01L33/507
摘要： One embodiment provides a method for fabricating a translucent phosphor ceramic compact comprising: heating a precursor powder to at least about 1000° C. under a reducing atmosphere to provide a pre-conditioned powder, forming an intermediate compact comprising the pre-conditioned powder and a flux material, and heating the intermediate compact under a vacuum to a temperature of at least about 1400° C. In another embodiment, the compact may be a cerium doped translucent phosphor ceramic compact comprising yttrium, aluminum, oxygen, and cerium sources. Another embodiment may be a light emitting device having the phosphor translucent ceramic provided as described herein.
摘要翻译： 一个实施例提供了一种制造半透明磷光体陶瓷压块的方法，包括：在还原气氛下将前体粉末加热至至少约1000℃，以提供预调节的粉末，形成包含预调节粉末的中间成型体和 助熔剂材料，并在真空下将中间成型体加热到至少约1400℃的温度。在另一个实施方案中，压块可以是包含钇，铝，氧和铈源的铈掺杂的半透明磷光体陶瓷压块。 另一个实施例可以是具有如本文所述提供的荧光体半透明陶瓷的发光器件。
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10.发明授权Emissive ceramic materials having a dopant concentration gradient and methods of making and using the same 有权具有掺杂剂浓度梯度的发光陶瓷材料及其制造和使用方法公开(公告)号：US08828531B2
公开(公告)日：2014-09-09
申请号：US13306797
申请日：2011-11-29
申请人： Guang Pan , Hiroaki Miyagawa , Hironaka Fujii , Bin Zhang , Rajesh Mukherjee , Toshitaka Nakamura , Amane Mochizuki
发明人： Guang Pan , Hiroaki Miyagawa , Hironaka Fujii , Bin Zhang , Rajesh Mukherjee , Toshitaka Nakamura , Amane Mochizuki
IPC分类号： B32B3/26 , B32B18/00 , C09K11/00 , C09K11/80 , C09K11/77 , C04B35/638 , C04B35/44 , C04B35/626 , H01L33/50
CPC分类号： C09K11/7774 , B32B18/00 , C04B35/44 , C04B35/6261 , C04B35/62665 , C04B35/6268 , C04B35/638 , C04B38/00 , C04B2111/807 , C04B2235/3225 , C04B2235/3229 , C04B2235/3418 , C04B2235/441 , C04B2235/5409 , C04B2235/6025 , C04B2235/604 , C04B2235/6562 , C04B2235/6565 , C04B2235/6581 , C04B2235/661 , C04B2235/663 , C04B2235/75 , C04B2235/764 , C04B2235/9646 , C04B2235/9653 , C04B2235/9661 , C04B2237/343 , C04B2237/582 , C04B2237/586 , C04B2237/704 , C09K2211/182 , H01L33/502 , H01L33/505 , H01L51/52 , Y10T428/249953 , Y10T428/249961 , Y10T428/24997 , Y10T428/24999 , C04B38/0655
摘要： Disclosed herein are emissive ceramic materials having a dopant concentration gradient along a thickness of a yttrium aluminum garnet (YAG) region. The dopant concentration gradient may include a maximum dopant concentration, a half-maximum dopant concentration, and a slope at or near the half-maximum dopant concentration. The emissive ceramics may, in some embodiments, exhibit high internal quantum efficiencies (IQE). The emissive ceramics may, in some embodiments, include porous regions. Also disclosed herein are methods of make the emissive ceramic by sintering an assembly having doped and non-doped layers.
摘要翻译： 本文公开了具有沿钇铝石榴石（YAG）区域的厚度的掺杂剂浓度梯度的发射陶瓷材料。 掺杂剂浓度梯度可以包括最大掺杂剂浓度，半最大掺杂剂浓度以及在半最大掺杂剂浓度处或附近的斜率。 在一些实施例中，发射陶瓷可表现出高的内部量子效率（IQE）。 在一些实施例中，发光陶瓷可以包括多孔区域。 本文还公开了通过烧结具有掺杂层和非掺杂层的组件来制造发光陶瓷的方法。
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