公开(公告)号：US20150343434A1

公开(公告)日：2015-12-03

申请号：US14759610

申请日：2014-01-03

Applicant: Ekambaram SAMBANDAN ,  Rajesh MUKHERJEE ,  Takuya FUKUMURA ,  Amane MOCHIZUKI ,  NITTO DENKO CORPORATION

Inventor： Ekambaram Sambandan ,  Rajesh Mukherjee ,  Takuya Fukumura ,  Amane Mochizuki

IPC: B01J37/02 ,  B01J37/08 ,  B01J21/12 ,  B01J35/00 ,  B01J31/22 ,  B01J27/25

CPC classification number: B01J37/0215 ,  B01J21/063 ,  B01J21/12 ,  B01J23/14 ,  B01J27/24 ,  B01J27/25 ,  B01J31/2239 ,  B01J35/004 ,  B01J37/0217 ,  B01J37/0219 ,  B01J37/08 ,  B01J37/086 ,  C01B21/0828 ,  C01G23/053 ,  C01P2002/30 ,  C01P2002/54 ,  C01P2002/72 ,  C04B41/009 ,  C04B41/5041 ,  C04B2111/00827 ,  C04B35/185 ,  C04B14/16 ,  C04B28/02 ,  C04B41/4537 ,  C04B41/505

Abstract: A method for forming an oxide coated substrate comprising heating a pre-coating mixture in the presence of a substrate to synthesize an oxide coating on the substrate. The pre-coating mixture comprises a solubilized reducing additive, a solubilized oxidizing additive, and the substrate. The heating is conducted at a temperature sufficiently high enough to exothermically react the solubilized reducing additive and solubilized oxidizing additive and low enough to control the phase and composition of the oxide.

Abstract translation: 一种形成氧化物涂覆的基材的方法，包括在基材存在下加热预涂混合物以在基材上合成氧化物涂层。 预涂混合物包含溶解的还原添加剂，溶解的氧化添加剂和底物。 加热在足够高的温度下进行，以使溶解的还原添加剂和溶解的氧化添加剂放热反应，并足够低以控制氧化物的相和组成。

公开(公告)号：US08697479B2

公开(公告)日：2014-04-15

申请号：US13510590

申请日：2010-11-17

Applicant: Rajesh Mukherjee ,  Hironaka Fujii ,  Toshitaka Nakamura ,  Amane Mochizuki

Inventor： Rajesh Mukherjee ,  Hironaka Fujii ,  Toshitaka Nakamura ,  Amane Mochizuki

IPC: H01L21/00

CPC classification number: B22F9/26 ,  B22F1/0018 ,  B22F2999/00 ,  B82Y30/00 ,  H01L33/502 ,  B22F2202/13

Abstract: Some embodiments disclosed herein are related to methods of preparing a nanoparticle composition comprising: providing an aerosol comprising a plurality of droplets of a precursor solution comprising at least one nanoparticle precursor and an expansive component; passing the aerosol through a plasma; and collecting a nanoparticle composition product from the carrier gas which has exited the plasma. Some embodiments relate to nanoparticle compositions provided by this process. Some embodiments relate to light-emitting diodes or light emitting devices comprising these compositions.

Abstract translation: 本文公开的一些实施方案涉及制备纳米颗粒组合物的方法，其包括：提供包含多个包含至少一种纳米颗粒前体和膨胀组分的前体溶液的液滴的气溶胶; 使气溶胶通过等离子体; 并从已经离开等离子体的载气中收集纳米颗粒组合物产物。 一些实施方案涉及由该方法提供的纳米颗粒组合物。 一些实施方案涉及包含这些组合物的发光二极管或发光装置。

公开(公告)号：US08283843B2

公开(公告)日：2012-10-09

申请号：US13016665

申请日：2011-01-28

Applicant: Guang Pan ,  Hironaka Fujii ,  Hiroaki Miyagawa ,  Rajesh Mukherjee ,  Bin Zhang ,  Toshitaka Nakamura ,  Amane Mochizuki

Inventor： Guang Pan ,  Hironaka Fujii ,  Hiroaki Miyagawa ,  Rajesh Mukherjee ,  Bin Zhang ,  Toshitaka Nakamura ,  Amane Mochizuki

IPC: H01J5/16

CPC classification number: C09K11/7774 ,  B32B18/00 ,  C04B35/44 ,  C04B35/62665 ,  C04B35/62675 ,  C04B35/6268 ,  C04B35/632 ,  C04B35/63488 ,  C04B35/638 ,  C04B2235/3225 ,  C04B2235/3229 ,  C04B2235/3418 ,  C04B2235/441 ,  C04B2235/443 ,  C04B2235/444 ,  C04B2235/5409 ,  C04B2235/5445 ,  C04B2235/6025 ,  C04B2235/652 ,  C04B2235/6562 ,  C04B2235/6567 ,  C04B2235/658 ,  C04B2235/6581 ,  C04B2235/6582 ,  C04B2235/6587 ,  C04B2235/663 ,  C04B2235/9653 ,  C04B2235/9661 ,  C04B2237/343 ,  C04B2237/565 ,  C04B2237/582 ,  C04B2237/64 ,  C04B2237/704 ,  C04B2237/76 ,  H01L33/502 ,  H01L33/505

Abstract: A ceramic composite laminate includes a wavelength-converting layer and a non-emissive layer, wherein the ceramic composite laminate has a wavelength conversion efficiency (WCE) of at least 0.650. The ceramic composite laminate can also include a wavelength-converting ceramic layer comprising an emissive material and a scattering material, wherein the laminated composite has a total transmittance of between about 40% to about 85%. The wavelength-converting layer may be formed from plasma YAG:Ce powder.

Abstract translation: 陶瓷复合层叠体包括波长转换层和非发射层，其中陶瓷复合层压体的波长转换效率（WCE）至少为0.650。 陶瓷复合层压体还可以包括包含发射材料和散射材料的波长转换陶瓷层，其中层压复合材料的总透射率为约40％至约85％。 波长转换层可以由等离子体YAG：Ce粉末形成。

公开(公告)号：US20120068213A1

公开(公告)日：2012-03-22

申请号：US13235147

申请日：2011-09-16

Applicant: Bin Zhang ,  Guang Pan ,  Hiroaki Miyagawa ,  Hironaka Fujii ,  Rajesh Mukherjee ,  Toshitaka Nakamura

Inventor： Bin Zhang ,  Guang Pan ,  Hiroaki Miyagawa ,  Hironaka Fujii ,  Rajesh Mukherjee ,  Toshitaka Nakamura

IPC: H01L33/50 ,  B32B37/14 ,  B32B37/06 ,  B32B19/00 ,  B32B3/00

CPC classification number: C09K11/7774 ,  B32B18/00 ,  C01F17/0025 ,  C01P2002/84 ,  C01P2006/12 ,  C04B35/44 ,  C04B35/6261 ,  C04B35/6265 ,  C04B35/62665 ,  C04B35/62685 ,  C04B35/63488 ,  C04B35/638 ,  C04B2235/3217 ,  C04B2235/3222 ,  C04B2235/3225 ,  C04B2235/3229 ,  C04B2235/5409 ,  C04B2235/6025 ,  C04B2235/6562 ,  C04B2235/6581 ,  C04B2235/6587 ,  C04B2235/661 ,  C04B2235/663 ,  C04B2235/764 ,  C04B2235/9653 ,  C04B2237/341 ,  C04B2237/343 ,  C04B2237/562 ,  C04B2237/565 ,  C04B2237/704 ,  H01L33/505 ,  Y10T428/265

Abstract: A laminated composite includes a wavelength-converting layer and a non-emissive blocking layer, wherein the emissive layer includes a garnet host material and an emissive guest material, and the non-emissive blocking layer includes a non-emissive blocking material. The metallic element constituting the non-emissive blocking material has an ionic radius which is less than about 80% of an ionic radius of an A cation element when the garnet or garnet-like host material is expressed as A3B5O12 and/or an element constituting the emissive guest material, and the non-emissive blocking layer is substantially free of the emissive guest material migrated through an interface between the emissive layer and the non-emissive blocking layer.

Abstract translation: 层压复合材料包括波​​长转换层和非发射阻挡层，其中发射层包括石榴石主体材料和发射客体材料，并且非发射阻挡层包括非发射阻挡材料。 构成非发射阻挡材料的金属元素的离子半径小于A阳离子元素的离子半径的约80％，当石榴石或石榴石状主体材料表示为A3B5O12和/或构成 发射客体材料和非发射阻挡层基本上不含通过发射层和非发射阻挡层之间的界面迁移的发射客体材料。

公开(公告)号：US20100301739A1

公开(公告)日：2010-12-02

申请号：US12787800

申请日：2010-05-26

Applicant: TOSHITAKA NAKAMURA ,  Hironaka Fujii ,  Hiroaki Miyagawa ,  Rajesh Mukherjee ,  Bin Zhang ,  Amane Mochizuki

Inventor： TOSHITAKA NAKAMURA ,  Hironaka Fujii ,  Hiroaki Miyagawa ,  Rajesh Mukherjee ,  Bin Zhang ,  Amane Mochizuki

IPC: H01J1/63 ,  C09K11/78

CPC classification number: C09K11/7774 ,  B82Y30/00 ,  C04B35/44 ,  C04B35/6268 ,  C04B35/6342 ,  C04B2235/3217 ,  C04B2235/3224 ,  C04B2235/3225 ,  C04B2235/3229 ,  C04B2235/3418 ,  C04B2235/441 ,  C04B2235/443 ,  C04B2235/5445 ,  C04B2235/5454 ,  C04B2235/6581 ,  C04B2235/764 ,  C04B2235/9653 ,  C04B2235/9661 ,  H01L33/502 ,  H01L33/505

Abstract: Some embodiments provide luminescent ceramics which have a lower amount of dopant than conventional luminescent ceramics. In some embodiments, the luminescent ceramic comprises a host material comprising a rare earth element and at least one rare earth dopant, wherein the rare earth dopant may be about 0.01% to 0.5% of the rare earth atoms present in the material. Some embodiments provide luminescent ceramic comprising: a polycrystalline phosphor represented by the formula (A1-xEx)3B5O12. Some embodiments provide a light-emitting device comprising a luminescent ceramic disclosed herein.

Abstract translation: 一些实施例提供具有比常规发光陶瓷更少量的掺杂剂的发光陶瓷。 在一些实施方案中，发光陶瓷包括含有稀土元素和至少一种稀土掺杂剂的主体材料，其中稀土掺杂剂可以是材料中存在的稀土原子的约0.01％至0.5％。 一些实施方案提供发光陶瓷，其包括：由式（A1-xEx）3B5O12表示的多晶磷光体。 一些实施方案提供包含本文公开的发光陶瓷的发光装置。

公开(公告)号：US20100301367A1

公开(公告)日：2010-12-02

申请号：US12788154

申请日：2010-05-26

Applicant: TOSHITAKA NAKAMURA ,  Hironaka Fujii ,  Hiroaki Miyagawa ,  Rajesh Mukherjee ,  Bin Zhang ,  Amane Mochizuki

Inventor： TOSHITAKA NAKAMURA ,  Hironaka Fujii ,  Hiroaki Miyagawa ,  Rajesh Mukherjee ,  Bin Zhang ,  Amane Mochizuki

IPC: H01L33/52

CPC classification number: H01L33/507 ,  H01L33/56 ,  H01L2933/0091

Abstract: Some embodiments provide a light-emitting device comprising: a light-emitting diode; a substantially transparent encapsulating material having a refractive index in the range of about 1.3 to about 1.8; a layer of low refractive index material having a refractive index in the range of about 1 to about 1.2; and a translucent ceramic phosphor having a refractive index in the range of about 1.6 to about 2.7, and is substantially dome-shaped with substantially uniform thickness. Some embodiments provide a light-emitting device comprising: a substrate; a light-emitting diode mounted on a surface of the substrate; and a substantially hemispheric cover mounted on the surface of the substrate so as to enclose the light emitting diode; wherein the substantially hemispheric cover comprises an outer layer, a middle layer, and an inner layer arranged concentrically, with the inner layer being nearest the light-emitting diode.

Abstract translation: 一些实施例提供一种发光器件，包括：发光二极管; 折射率在约1.3至约1.8范围内的基本透明的包封材料; 折射率在约1至约1.2范围内的低折射率材料层; 以及折射率在约1.6至约2.7范围内的半透明陶瓷荧光粉，并且基本上圆顶形，具有基本均匀的厚度。 一些实施例提供一种发光器件，其包括：衬底; 安装在所述基板的表面上的发光二极管; 以及安装在所述基板的表面上以包围所述发光二极管的大致半球形盖; 其中所述基本上半球形的盖子包括外层，中间层和同心布置的内层，所述内层最靠近所述发光二极管。

公开(公告)号：US20100012478A1

公开(公告)日：2010-01-21

申请号：US12175389

申请日：2008-07-17

Applicant: TOSHITAKA NAKAMURA ,  RAJESH MUKHERJEE ,  BIN ZHANG ,  AMANE MOCHIZUKI

Inventor： TOSHITAKA NAKAMURA ,  RAJESH MUKHERJEE ,  BIN ZHANG ,  AMANE MOCHIZUKI

IPC: B01J19/12

CPC classification number: B01J19/126 ,  B01J2219/123 ,  B01J2219/1242 ,  B01J2219/1245 ,  B01J2219/1254 ,  B01J2219/1281 ,  B01J2219/1284 ,  B82Y30/00 ,  C01F17/0025 ,  C01P2002/34 ,  C01P2002/54 ,  C01P2004/64 ,  C01P2006/90

Abstract: A method of annealing inorganic particles using microwave is provided. The method comprises disposing a plurality of raw particles having poor room-temperature microwave coupling characteristics in a close proximity to a microwave-absorbing material, irradiating said microwave-absorbing material with microwave radiation to heat said microwave-absorbing material, and heating said plurality of raw particles for a period of time sufficient to obtain a plurality of annealed particles, wherein the plurality of annealed particles has a crystalline phase, and wherein said heating comprises transferring heat from said microwave-absorbing material to said plurality of raw particles.

Abstract translation: 提供了使用微波对无机颗粒进行退火的方法。 该方法包括在微波吸收材料附近配置具有差的室温微波耦合特性的多个原始颗粒，用微波辐射照射所述微波吸收材料以加热所述微波吸收材料，并加热所述多个 原料颗粒足以获得多个退火颗粒的时间段，其中所述多个退火颗粒具有结晶相，并且其中所述加热包括将热量从所述微波吸收材料转移到所述多个原料颗粒。

公开(公告)号：US08828531B2

公开(公告)日：2014-09-09

申请号：US13306797

申请日：2011-11-29

Applicant: Guang Pan ,  Hiroaki Miyagawa ,  Hironaka Fujii ,  Bin Zhang ,  Rajesh Mukherjee ,  Toshitaka Nakamura ,  Amane Mochizuki

Inventor： Guang Pan ,  Hiroaki Miyagawa ,  Hironaka Fujii ,  Bin Zhang ,  Rajesh Mukherjee ,  Toshitaka Nakamura ,  Amane Mochizuki

IPC: B32B3/26 ,  B32B18/00 ,  C09K11/00 ,  C09K11/80 ,  C09K11/77 ,  C04B35/638 ,  C04B35/44 ,  C04B35/626 ,  H01L33/50

CPC classification number: C09K11/7774 ,  B32B18/00 ,  C04B35/44 ,  C04B35/6261 ,  C04B35/62665 ,  C04B35/6268 ,  C04B35/638 ,  C04B38/00 ,  C04B2111/807 ,  C04B2235/3225 ,  C04B2235/3229 ,  C04B2235/3418 ,  C04B2235/441 ,  C04B2235/5409 ,  C04B2235/6025 ,  C04B2235/604 ,  C04B2235/6562 ,  C04B2235/6565 ,  C04B2235/6581 ,  C04B2235/661 ,  C04B2235/663 ,  C04B2235/75 ,  C04B2235/764 ,  C04B2235/9646 ,  C04B2235/9653 ,  C04B2235/9661 ,  C04B2237/343 ,  C04B2237/582 ,  C04B2237/586 ,  C04B2237/704 ,  C09K2211/182 ,  H01L33/502 ,  H01L33/505 ,  H01L51/52 ,  Y10T428/249953 ,  Y10T428/249961 ,  Y10T428/24997 ,  Y10T428/24999 ,  C04B38/0655

Abstract: Disclosed herein are emissive ceramic materials having a dopant concentration gradient along a thickness of a yttrium aluminum garnet (YAG) region. The dopant concentration gradient may include a maximum dopant concentration, a half-maximum dopant concentration, and a slope at or near the half-maximum dopant concentration. The emissive ceramics may, in some embodiments, exhibit high internal quantum efficiencies (IQE). The emissive ceramics may, in some embodiments, include porous regions. Also disclosed herein are methods of make the emissive ceramic by sintering an assembly having doped and non-doped layers.

Abstract translation: 本文公开了具有沿钇铝石榴石（YAG）区域的厚度的掺杂剂浓度梯度的发射陶瓷材料。 掺杂剂浓度梯度可以包括最大掺杂剂浓度，半最大掺杂剂浓度以及在半最大掺杂剂浓度处或附近的斜率。 在一些实施例中，发射陶瓷可表现出高的内部量子效率（IQE）。 在一些实施例中，发光陶瓷可以包括多孔区域。 本文还公开了通过烧结具有掺杂层和非掺杂层的组件来制造发光陶瓷的方法。

公开(公告)号：US08502442B2

公开(公告)日：2013-08-06

申请号：US13436676

申请日：2012-03-30

Applicant: Toshitaka Nakamura ,  Hironaka Fujii ,  Hiroaki Miyagawa ,  Rajesh Mukherjee ,  Bin Zhang ,  Amane Mochizuki

Inventor： Toshitaka Nakamura ,  Hironaka Fujii ,  Hiroaki Miyagawa ,  Rajesh Mukherjee ,  Bin Zhang ,  Amane Mochizuki

IPC: H01J1/62

CPC classification number: C09K11/7774 ,  B82Y30/00 ,  C04B35/44 ,  C04B35/62675 ,  C04B35/6268 ,  C04B35/63416 ,  C04B35/6342 ,  C04B2235/3206 ,  C04B2235/3217 ,  C04B2235/3222 ,  C04B2235/3225 ,  C04B2235/3229 ,  C04B2235/3418 ,  C04B2235/3427 ,  C04B2235/5454 ,  C04B2235/656 ,  C04B2235/6581 ,  C04B2235/80 ,  C04B2235/9653 ,  C04B2235/9661 ,  H01L25/0753 ,  H01L33/502 ,  H01L2924/0002 ,  H05B33/14 ,  H01L2924/00

Abstract: A light emitting device comprising a light emitting component that emits light with a first peak wavelength, and at least one sintered ceramic plate over the light emitting component is described. The at least one sintered ceramic plate is capable of absorbing at least a portion of the light emitted from said light emitting component and emitting light of a second peak wavelength, and has a total light transmittance at the second peak wavelength of greater than about 40%. A method for improving the luminance intensity of a light emitting device comprising providing a light emitting component and positioning at least one translucent sintered ceramic plate described above over the light emitting component is also disclosed.

Abstract translation: 一种发光装置，其包括发射具有第一峰值波长的光的发光部件和在发光部件上方的至少一个烧结陶瓷板。 所述至少一个烧结陶瓷板能够吸收从所述发光组件发射的光的至少一部分并发射第二峰值波长的光，并且在第二峰值波长处的总光线透射率大于约40％ 。 还公开了一种用于提高发光器件的亮度强度的方法，包括提供发光部件并且将上述至少一个半透明烧结陶瓷板定位在发光部件上。

公开(公告)号：US20120235203A1

公开(公告)日：2012-09-20

申请号：US13510590

申请日：2010-11-17

Applicant: Rajesh Mukherjee ,  Hironaka Fujii ,  Toshitaka Nakamura ,  Amane Mochizuki

Inventor： Rajesh Mukherjee ,  Hironaka Fujii ,  Toshitaka Nakamura ,  Amane Mochizuki

IPC: C01F17/00 ,  C09K11/80 ,  H01L33/50 ,  B82Y30/00 ,  B82Y40/00

CPC classification number: B22F9/26 ,  B22F1/0018 ,  B22F2999/00 ,  B82Y30/00 ,  H01L33/502 ,  B22F2202/13

Abstract: Some embodiments disclosed herein are related to methods of preparing a nanoparticle composition comprising: providing an aerosol comprising a plurality of droplets of a precursor solution comprising at least one nanoparticle precursor and an expansive component; passing the aerosol through a plasma; and collecting a nanoparticle composition product from the carrier gas which has exited the plasma. Some embodiments relate to nanoparticle compositions provided by this process. Some embodiments relate to light-emitting diodes or light emitting devices comprising these compositions.

Abstract translation: 本文公开的一些实施方案涉及制备纳米颗粒组合物的方法，其包括：提供包含多个包含至少一种纳米颗粒前体和膨胀组分的前体溶液的液滴的气溶胶; 使气溶胶通过等离子体; 并从已经离开等离子体的载气中收集纳米颗粒组合物产物。 一些实施方案涉及由该方法提供的纳米颗粒组合物。 一些实施方案涉及包含这些组合物的发光二极管或发光装置。