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公开(公告)号：US4198534A
公开(公告)日：1980-04-15
申请号：US905126
申请日：1978-05-12
IPC分类号： C07C2/22 , A61K8/30 , A61K8/31 , A61K8/81 , A61Q1/00 , A61Q1/12 , A61Q19/00 , C07C1/00 , C07C2/08 , C07C9/22 , C07C67/00 , C07C9/14 , C07C3/10
摘要： A cosmetic base material which consists of a synthetic saturated aliphatic hydrocarbon having 24 to 36 carbon atoms, wherein the proton ratio of methyl group to methylene group, that is, CH.sub.3 /CH.sub.2, within the hydrocarbon chain is in the range of from 0.25 to 0.6 and the pour point is in the range of from -55.degree. C. to 10.degree. C.
摘要翻译： 一种由具有24至36个碳原子的合成饱和脂族烃组成的化妆品基料，其中烃链中的甲基与亚甲基的质子比（即CH 3 / CH 2）在0.25至0.6的范围内 倾点在-55℃至10℃的范围内。
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公开(公告)号：US4214112A
公开(公告)日：1980-07-22
申请号：US24205
申请日：1979-03-27
IPC分类号： C08F4/00 , C07C1/00 , C07C2/22 , C07C11/02 , C07C67/00 , C08F4/06 , C08F4/14 , C08F8/00 , C08F10/00 , C08F10/14 , C07C3/18
CPC分类号： C07C2/22 , C07C2521/02 , C07C2527/125 , C07C2527/126 , C07C2531/02 , C07C2531/26
摘要： A process for producing an olefin oligomer comprising polymerizing olefin having not less than 6 carbon atoms in the presence of a catalyst consisting essentially of (a) aluminum halide, (b) polyhydric alcohol derivative of which alcohol the hydrogen atoms of the entire hydroxyl groups are substituted with either one or both of alkyl and acyl groups and (c) a nickel compound or cobalt compound is provided. Thus, an olefin oligomer having a narrow distribution of the polymerization degree and good properties can be obtained with a high selectivity by using a catalyst capable of being easily handled.
摘要翻译： 1.一种烯烃低聚物的制造方法，其特征在于，在催化剂的存在下，在（a）卤化铝，（b）多元醇衍生物，全部羟基的氢原子为醇的多元醇衍生物的催化剂的存在下聚合具有不少于6个碳原子的烯烃， 被烷基和酰基中的一个或两个取代，和（c）提供镍化合物或钴化合物。 因此，通过使用能够容易地处理的催化剂，可以通过高选择性获得聚合度分布窄，性能好的烯烃低聚物。
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公开(公告)号：US4219691A
公开(公告)日：1980-08-26
申请号：US936043
申请日：1978-08-23
IPC分类号： C08F4/00 , C07C1/00 , C07C2/22 , C07C11/02 , C07C67/00 , C08F4/06 , C08F10/00 , C08F10/14 , C07C3/18
CPC分类号： C08F10/14
摘要： Disclosed is a process for producing olefin oligomer from olefins having not less than 6 carbon atoms in the presence of a reaction mixture of an aluminum halide and a secondary or tertiary alcohol in the stated equivalent proportions. The olefin oligomers thus obtained have a high kinematic viscosity, a low pour point, a high viscosity index and a good shear stability.
摘要翻译： 公开了一种在卤化铝和仲醇或叔醇的反应混合物存在下以所述等量比例生产烯烃低聚物的方法，该方法由具有不少于6个碳原子的烯烃制备。 由此获得的烯烃低聚物具有高运动粘度，低倾点，高粘度指数和良好的剪切稳定性。
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公开(公告)号：US4006199A
公开(公告)日：1977-02-01
申请号：US677158
申请日：1976-04-15
IPC分类号： C10M107/10 , A61K8/30 , B01J31/00 , C07C1/00 , C07C2/22 , C07C11/02 , C07C67/00 , C08F4/00 , C08F4/06 , C08F10/00 , C08F10/14 , C08F210/14 , C10M105/04 , C10N20/04 , C10N30/00 , C10N30/02 , C10N40/04 , C10N40/30 , C10N60/02 , C07C3/18
CPC分类号： C08F210/14
摘要： Liquid polyolefin oil having a kinematic viscosity of about 500 centistokes or more at 100.degree. F, a high viscosity index, a good shearing stability and a low pour point can be prepared by polymerizing an olefin having 6 or more carbon atoms in the presence of a catalyst mixture of (a) a dicarbonyl compound selected from a group consisting of acyclic or cyclic diketones and ketoesters and (b) an aluminum halide in an amount of 0.7 - 5 mole per one carbonyl group or ester bond of said dicarbonyl compound. Said catalyst mixture may contain an alkyl halide.
摘要翻译： 在100°F下具有约500厘沲或更高的运动粘度，高粘度指数，良好剪切稳定性和低倾点的液体聚烯烃油可以通过在存在下存在下聚合具有6个或更多个碳原子的烯烃来制备 （a）选自无环或环状二酮和酮酯的二羰基化合物的催化剂混合物和（b）每个羰基或所述二羰基化合物的酯键为0.7-5摩尔量的卤化铝。 所述催化剂混合物可以含有烷基卤化物。
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公开(公告)号：US3947507A
公开(公告)日：1976-03-30
申请号：US446017
申请日：1974-02-26
申请人： Hiroshi Isa , Hiroshi Mandai , Toshiyuki Ukigai , Anri Tominaga , Ryozo Taniyasu , Masuzo Nagayama
发明人： Hiroshi Isa , Hiroshi Mandai , Toshiyuki Ukigai , Anri Tominaga , Ryozo Taniyasu , Masuzo Nagayama
CPC分类号： C07C2/30 , C08F10/00 , C07C2527/08 , C07C2527/125 , C07C2527/126 , C07C2527/135 , C07C2531/12 , C07C2531/26
摘要： A method for producing a liquid olefin polymer which comprises polymerizing an .alpha.-olefin having 6 - 14 carbon atoms or mixtures thereof, in the presence of a catalyst consisting of an alkali metal hydride, a halide of an element selected from boron and aluminum and a titanium halide, or a catalyst in which metallic lithium or sodium is added to those catalyst ingredients.
摘要翻译： 一种制备液体烯烃聚合物的方法，其包括在由碱金属氢化物，选自硼和铝的元素的卤化物和选自硼和铝的催化剂的存在下，将具有6-14个碳原子的α-烯烃或其混合物聚合， 卤化钛或其中向这些催化剂成分中加入金属锂或钠的催化剂。
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公开(公告)号：US4031158A
公开(公告)日：1977-06-21
申请号：US707614
申请日：1976-07-22
IPC分类号： C08F4/00 , C07C1/00 , C07C2/22 , C07C11/02 , C07C67/00 , C08F4/06 , C08F10/00 , C08F10/14 , C10M107/10 , C10N30/02 , C10N40/08 , C10N40/12 , C10N40/25 , C10N60/02 , C07C3/18
CPC分类号： C08F10/14
摘要： A method of preparing a polyolefin oil in the present invention comprises polymerizing an olefin having 6 or more carbon atoms in the presence of a mixture of a polyhydric alcohol derivative and an aluminum halide, said derivative being obtained by replacing hydrogen atoms of all the hydroxyl groups of the polyhydric alcohol by alkyl groups having 1-20 carbon atoms. The thus prepared polyolefin oil scarcely contains halogen, and it has a wide range of use such as, for instance, a lubricant, a cosmetic base, a textile finishing agent, etc.
摘要翻译： 在本发明中制备聚烯烃油的方法包括在多元醇衍生物和卤化铝的混合物的存在下聚合具有6个或更多个碳原子的烯烃，所述衍生物是通过取代所有羟基的氢原子 的多元醇通过具有1-20个碳原子的烷基。 由此制备的聚烯烃油几乎不含有卤素，并且具有广泛的用途，例如润滑剂，化妆品基质，纺织整理剂等。
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公开(公告)号：US3997622A
公开(公告)日：1976-12-14
申请号：US652426
申请日：1976-01-26
申请人： Hiroshi Isa , Toshiyuki Ukigai , Anri Tominaga , Michito Sato
发明人： Hiroshi Isa , Toshiyuki Ukigai , Anri Tominaga , Michito Sato
IPC分类号： C08F4/00 , B01J31/30 , C07B61/00 , C07C1/00 , C07C2/26 , C07C11/02 , C07C67/00 , C08F4/42 , C08F10/00 , C08F10/14 , C07C3/18
CPC分类号： B01J31/26 , B01J31/0202 , C07C2/26 , B01J21/02 , B01J2231/20 , B01J27/10 , B01J27/125 , C07C2521/02 , C07C2531/02 , C07C2531/26
摘要： A method of preparing an olefin oligomer by polymerizing an olefin having more than 6 carbon atoms, wherein said olefin is to be polymerized in the presence of a catalyst consisting of (a) polyhydric alcohol derivatives obtained by substituting hydrogen atoms of all the whole hydroxyl groups of polyhydric alcohol by either acyl group exclusively or acyl group and alkyl groups, both said acyl group and alkyl group having 1 - 20 carbon atoms, (b) aluminum halide in an amount of 0.7 - 1.0 mole per each ester bond and ether bond possessed by said polyhydric alcohol derivative and (c) metallic aluminum powder.
摘要翻译： 一种通过聚合具有多于6个碳原子的烯烃制备烯烃低聚物的方法，其中所述烯烃在催化剂存在下聚合，所述催化剂由（a）通过用全部羟基取代氢原子而获得的多元醇衍生物 的多元醇通过酰基或酰基和烷基，所述酰基和具有1-20个碳原子的烷基，（b）每个酯键和醚键具有0.7-1.0摩尔量的卤化铝 所述多元醇衍生物和（c）金属铝粉末。
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公开(公告)号：US3952071A
公开(公告)日：1976-04-20
申请号：US538965
申请日：1975-01-06
IPC分类号： C08F4/00 , A61K8/30 , A61K8/72 , A61K8/81 , A61K9/06 , B01J31/00 , C07B61/00 , C07C1/00 , C07C2/22 , C07C11/02 , C07C67/00 , C08F4/06 , C08F10/00 , C08F10/14 , C07C3/18
CPC分类号： C07C2/22 , C08F10/00 , C07C2527/125 , C07C2527/126 , C07C2531/02
摘要： An olefin oligomer having a low viscosity and a high viscosity index can be prepared by polymerizing an olefin having 6 or more carbon atoms in the presence of a mixture of a polyhydric alcohol derivative and an aluminum halide, said derivative being obtained by replacing the hydrogen atoms of all the hydroxyl groups of the polyhydric alcohol by either acyl groups exclusively or by acyl group and alkyl groups both of said groups having 1 - 20 carbon atoms. The thus prepared olefin oligomer scarcely contains halogen, and it has a wide range of uses such as, for instance, a lubricant, a cosmetic base, etc.
摘要翻译： 具有低粘度和高粘度指数的烯烃低聚物可以通过在多元醇衍生物和卤化铝的混合物存在下聚合具有6个或更多个碳原子的烯烃来制备，所述衍生物是通过将氢原子 的多羟基醇的所有羟基通过酰基独立地或通过酰基和烷基，所述基团都具有1-20个碳原子。 如此制备的烯烃低聚物几乎不含有卤素，并且具有广泛的用途，例如润滑剂，化妆品基料等。
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公开(公告)号：US3947509A
公开(公告)日：1976-03-30
申请号：US549864
申请日：1975-02-14
IPC分类号： C08F4/00 , A61K8/30 , B01J31/00 , C07B61/00 , C07C1/00 , C07C2/20 , C07C2/22 , C07C2/26 , C07C11/02 , C07C67/00 , C08F4/06 , C08F10/00 , C08F10/14 , C10M107/10 , C10M169/00 , C10N30/02 , C10N40/04 , C10N40/12 , C10N40/30 , C07C9/00 , C10M1/16
CPC分类号： C10M3/00 , C07C2/22 , C07C2527/126 , C07C2531/02 , C07C2531/26 , C10M2205/00 , C10M2205/028
摘要： A method of effecting polymerization of olefins having 6 or more carbon atoms or mixtures of such olefins (hereinafter referred to as the feed olefin), to produce a hydrocarbon liquid polymer which comprises mixing a catalyst composed of aluminum chloride, ketone having 4 or more carbon atoms and olefin catalyst constituent with 0.01 to 0.3 mole of ester, ether or alcohol per mole of said aluminum chloride and effecting the polymerization of the feed olefin at a reaction temperature of more than 60.degree.C.
摘要翻译： 一种使具有6个或更多个碳原子的烯烃或这种烯烃的混合物（以下称为进料烯烃）进行聚合的方法来制备烃液体聚合物，其包括将由氯化铝组成的催化剂，具有4个或更多个碳的酮 原子和烯烃催化剂组分，每摩尔所述氯化铝具有0.01至0.3摩尔的酯，醚或醇，并在大于60℃的反应温度下进行进料烯烃的聚合。
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公开(公告)号：US4066715A
公开(公告)日：1978-01-03
申请号：US675238
申请日：1976-04-08
申请人： Hiroshi Isa , Toshiyuki Ukigai , Anri Tominaga , Michito Sato
发明人： Hiroshi Isa , Toshiyuki Ukigai , Anri Tominaga , Michito Sato
IPC分类号： C08F4/00 , A61K8/30 , B01J31/00 , C07B61/00 , C07C1/00 , C07C2/22 , C07C2/24 , C07C2/26 , C07C11/02 , C07C67/00 , C08F4/42 , C08F10/00 , C08F10/14 , C10M143/08 , C10N30/02 , C10N40/08 , C10N40/12 , C10N40/16 , C07C3/18
CPC分类号： C08F10/14
摘要： A method of preparing an olefin oligomer by polymerizing an olefin having 6 or more carbon atoms, wherein said olefin is polymerized in the presence of a catalyst consisting of (a) a polyhydric alcohol derivative obtained by replacing the hydrogen atoms of all the hydroxyl groups of the polyhydric alcohol by either acyl groups exclusively or by acyl groups and alkyl groups, both of said groups having 1 - 20 carbon atoms, (b) an aluminum halide in an amount of 1.1 - 2.8 mole per one ester bond or ether bond possessed by said polyhydric alcohol derivative and (c) metallic aluminum powder.
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