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    Process for the production of triethylenediamine
    2.
    发明授权
    Process for the production of triethylenediamine 失效
    三亚乙基二胺生产工艺

    公开(公告)号：US5756741A

    公开(公告)日：1998-05-26

    申请号：US751142

    申请日：1996-11-15

    申请人： John Nelson Armor ,  Jose Guadalupe Santiesteban ,  Hong-Xin Li

    发明人： John Nelson Armor ,  Jose Guadalupe Santiesteban ,  Hong-Xin Li

    IPC分类号： B01J29/40 ,  C07B61/00 ,  C07C209/60 ,  C07C209/62 ,  C07C211/09 ,  C07D487/08

    CPC分类号： C07D487/08

    摘要： A process for preparing triethylenediamine by passing an amine compound over a catalyst at elevated temperature to afford a reaction product containing triethylenediamine and piperazine, the amine compound having, in the molecule, a moiety represented by the following general formula ##STR1## where R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are independently a hydrogen atom or an alkyl group having 1 to 4 carbon atoms and X is oxygen or nitrogen characterized by adding an ethylating compound containing at least one nitrogen and/or oxygen atom to the reaction product and contacting the reaction product, under conditions sufficient to produce triethylenediamine from the ethylating compound and piperazine, with a condensation/cyclization shape-selective zeolite catalyst demonstrating a triethylenediamine/piperazine weight ratio uptake value of at least 6:1.

    摘要翻译： 一种通过使胺化合物在升高的温度下通过催化剂制备三亚乙基二胺的方法，得到含有三亚乙基二胺和哌嗪的反应产物，所述胺化合物在分子中具有由以下通式表示的部分，其中R1，R2 R 3和R 4独立地是氢原子或具有1至4个碳原子的烷基，X是氧或氮，其特征在于向反应产物中加入含有至少一个氮原子和/或氧原子的乙基化合物，并使反应产物 在足以从乙基化合物和哌嗪产生三亚乙基二胺的条件下，使用缩合/环化形状选择性沸石催化剂，证明三亚乙基二胺/哌嗪的重量比吸收值至少为6:1。

    Metal exchanged zeolite catalysts for alcohol amination
    5.
    发明授权
    Metal exchanged zeolite catalysts for alcohol amination 失效
    用于醇胺化的金属交换沸石催化剂

    公开(公告)号：US5917092A

    公开(公告)日：1999-06-29

    申请号：US49540

    申请日：1998-03-27

    申请人： Gamini Ananda Vedage ,  Lenore Ann Emig ,  Hong-Xin Li ,  John Nelson Armor

    发明人： Gamini Ananda Vedage ,  Lenore Ann Emig ,  Hong-Xin Li ,  John Nelson Armor

    IPC分类号： C07C209/16 ,  C07C211/03 ,  C07C211/06 ,  C07C211/07 ,  C07C209/38

    CPC分类号： C07C209/16

    摘要： A process for the production of predominantly primary and secondary amines and little or no tertiary amines by the reductive amination of aliphatic alcohols using a metal exchanged crystalline aluminosilicate catalyst. The catalyst has a silica/alumina ratio ranging from about 10:1 to 40:1, contains about 1 to 10% by weight of cobalt or nickel and about 0.05 to 5% by weight of at least one other metal. High conversion rates are achieved at moderate temperatures and pressures.

    摘要翻译： 通过使用金属交换的结晶硅铝酸盐催化剂对脂族醇进行还原胺化，主要生产伯胺和仲胺以及很少或不含叔胺的方法。 催化剂的二氧化硅/氧化铝比例为约10:1至40:1，含约1至10重量％的钴或镍和约0.05至5重量％的至少一种其它金属。 在适度的温度和压力下实现高转化率。

    Fe-SAPO-34 CATALYST AND METHODS OF MAKING AND USING THE SAME
    9.
    发明申请
    Fe-SAPO-34 CATALYST AND METHODS OF MAKING AND USING THE SAME 审中-公开
    Fe-SAPO-34催化剂及其制备和使用方法

    公开(公告)号：US20120251422A1

    公开(公告)日：2012-10-04

    申请号：US13438365

    申请日：2012-04-03

    申请人： Hong-Xin Li ,  William E. Cormier ,  Bjorn Moden

    发明人： Hong-Xin Li ,  William E. Cormier ,  Bjorn Moden

    IPC分类号： B01J29/85 ,  B01D53/56

    CPC分类号： B01J29/85 ,  B01D53/9418 ,  B01D2251/2062 ,  B01D2251/2067 ,  B01D2255/20738 ,  B01D2255/50

    摘要： There is disclosed a method of making, through direct synthesis, a catalyst comprising an Fe-SAPO-34 molecular sieve. There is also disclosed an Fe-SAPO-34 molecular sieve made according to the disclosed method herein, wherein the molecular sieve contains both framework iron and iron cations at ion-exchange sites. In addition, there is disclosed a method of using the Fe-SAPO-34 disclosed herein in a selective catalytic reduction reaction, typically in the presence of ammonia or urea, to reduce or remove nitric oxides from exhaust emissions.

    摘要翻译： 公开了通过直接合成制备包含Fe-SAPO-34分子筛的催化剂的方法。 还公开了根据本文公开的方法制备的Fe-SAPO-34分子筛，其中分子筛在离子交换位点含有骨架铁和铁阳离子。 此外，公开了一种使用本文公开的Fe-SAPO-34在选择性催化还原反应中，通常在氨或脲存在下从废气排放物中还原或除去一氧化氮的方法。