Preparation of microcapsule with double layered structure
    1.
    发明授权
    Preparation of microcapsule with double layered structure 有权
    具有双层结构的微胶囊的制备

    公开(公告)号:US08808587B2

    公开(公告)日:2014-08-19

    申请号:US12675700

    申请日:2008-08-19

    IPC分类号: B01J13/02 B32B5/16

    摘要: The present invention relates to a method of preparing a microcapsule with a double-layered structure which comprises the steps of performing an interfacial polymerization of an amine-aldehyde prepolymer on droplets containing an inorganic metal precursor selected from carboxylate and alkoxide compounds, and hydrolyzing the including inorganic precursors for formation of inorganic inner layer. The method of the present invention can prepare a microcapsule with a double-layered structure of an inorganic inner layer and a polymer outer layer, which is effective for eluting and substituting a core material inside the capsule.

    摘要翻译: 本发明涉及一种制备具有双层结构的微胶囊的方法,其包括以下步骤:在含有选自羧酸盐和烷氧基化合物的无机金属前体的液滴上进行胺 - 醛预聚物的界面聚合,并水解包含 用于形成无机内层的无机前体。 本发明的方法可以制备具有无机内层和聚合物外层的双层结构的微胶囊,其对于在胶囊内部的芯材进行洗脱和取代是有效的。

    PREPARATION OF MICROCAPSULE WITH DOUBLE LAYERED STRUCTURE
    2.
    发明申请
    PREPARATION OF MICROCAPSULE WITH DOUBLE LAYERED STRUCTURE 有权
    具有双层结构的微孔的制备

    公开(公告)号:US20100237520A1

    公开(公告)日:2010-09-23

    申请号:US12675700

    申请日:2008-08-19

    IPC分类号: B01J13/02

    摘要: The present invention relates to a method of preparing a microcapsule with a double-layered structure which comprises the steps of performing an interfacial polymerization of an amine-aldehyde prepolymer on droplets containing an inorganic metal precursor selected from carboxylate and alkoxide compounds, and hydrolyzing the including inorganic precursors for formation of inorganic inner layer. The method of the present invention can prepare a microcapsule with a double-layered structure of an inorganic inner layer and a polymer outer layer, which is effective for eluting and substituting a core material inside the capsule.

    摘要翻译: 本发明涉及一种制备具有双层结构的微胶囊的方法,其包括以下步骤:在含有选自羧酸盐和烷氧基化合物的无机金属前体的液滴上进行胺 - 醛预聚物的界面聚合,并水解包含 用于形成无机内层的无机前体。 本发明的方法可以制备具有无机内层和聚合物外层的双层结构的微胶囊,其对于在胶囊内部的芯材进行洗脱和取代是有效的。

    Method for preparing a poly(ether sulfonimide or -amide) copolymer using cyclic oligomers
    4.
    发明授权
    Method for preparing a poly(ether sulfonimide or -amide) copolymer using cyclic oligomers 有权
    使用环状低聚物制备聚(醚磺酰亚胺或酰胺)共聚物的方法

    公开(公告)号:US08586700B2

    公开(公告)日:2013-11-19

    申请号:US13641585

    申请日:2010-10-07

    IPC分类号: C08G63/02

    摘要: Disclosed is a method for preparing a poly(ethersulfonimide or ethersulfonamide) copolymer using cyclic oligomers, and more particularly, to a method for preparing a poly(ethersulfonimide or ethersulfonamide) copolymer by preparing a cyclic ether sulfone oligomer and a cyclic imide or amide oligomer and subjecting the cyclic ether sulfone oligomer and the cyclic imide or amide oligomer to ring-opening copolymerization in the presence of an alkali metal fluoride catalyst.

    摘要翻译: 公开了使用环状低聚物制备聚(醚砜酰亚胺或醚磺酰胺)共聚物的方法,更具体地说,涉及通过制备环状醚砜低聚物和环状酰亚胺或酰胺低聚物制备聚(醚砜酰亚胺或醚磺酰胺)共聚物的方法, 在碱金属氟化物催化剂的存在下使环醚砜低聚物和环状酰亚胺或酰胺低聚物进行开环共聚。

    Aromatic polyether resins crosslinked by amic acid or imide side chain
    5.
    发明授权
    Aromatic polyether resins crosslinked by amic acid or imide side chain 有权
    通过酰胺酸或酰亚胺侧链交联的芳香族聚醚树脂

    公开(公告)号:US07662904B2

    公开(公告)日:2010-02-16

    申请号:US11352885

    申请日:2006-02-13

    IPC分类号: C08G75/00 C08G8/02 C08G14/00

    摘要: The present invention relates to aromatic polyether resins crosslinked with amic acid or imide side chain, and more particularly, to the aromatic polyether resin crosslinked by amic acid or imide side chain, which is produced by heat curing of amic acid, wherein introduction of imide groups to the basic backbone provides excellent chemical resistance as well as heat resistance and improves surface roughness when coated as a thin film so that it can be suitable for films and flexible display plate substrate.

    摘要翻译: 本发明涉及用酰胺酸或酰亚胺侧链交联的芳族聚醚树脂,更具体地说,涉及通过酰胺酸热固化生产的酰胺酸或酰亚胺侧链交联的芳香族聚醚树脂,其中引入酰亚胺基 到基本骨架提供优异的耐化学性以及耐热性,并且当涂覆为薄膜时改善表面粗糙度,使得其可适用于膜和柔性显示板基材。

    Method of surface modification of polyimide film using ethyleneimines coupling agent, manufacturing method of flexible copper clad laminate and its product thereby
    7.
    发明授权
    Method of surface modification of polyimide film using ethyleneimines coupling agent, manufacturing method of flexible copper clad laminate and its product thereby 有权
    使用乙烯亚胺偶联剂对聚酰亚胺膜进行表面改性的方法,由此形成柔性覆铜层压板及其制品的制造方法

    公开(公告)号:US08419918B2

    公开(公告)日:2013-04-16

    申请号:US11920492

    申请日:2006-05-18

    IPC分类号: C25D5/56 C25D5/34 C23C28/02

    摘要: A method of surface modifying a polyimide film, a method of manufacturing a flexible copper clad laminate using the same, and a flexible copper clad laminate (FCCL) having a two-layer structure manufactured thereby. The method of surface modifying a polyimide film is conducted by modifying the surface of a polyimide film through a first plasma treatment, dipping the polyimide film into a solution containing an ethyleneimine-based silane coupling agent prepared by mixing the compound of Formula 1 and the compound of Formula 2 at a molar ratio of with 0.25˜1, and then modifying the surface of the polyimide film through a second plasma treatment. The method of surface modifying a polyimide film is advantageous because it may be substituted for a conventional surface treatment processes using ion beams. Also, the FCCL having a two-layer structure, formed by conducting copper sputtering and electroplating on the surface modified polyimide film, has good adhesive strength between the polyimide film and the copper foil and can maintain such adhesive strength even at high temperatures for a long period of time. Further, it may be usefully applied to electronic parts, such as flexible printed circuit boards, TCP (Tape Carrier Package), COF (Chip On Film), etc.

    摘要翻译: 对聚酰亚胺膜进行表面改性的方法,使用该方法的柔性覆铜层压板的制造方法以及由此制造的具有两层结构的柔性覆铜层压板(FCCL)。 聚酰亚胺薄膜的表面改性方法是通过第一等离子体处理改性聚酰亚胺薄膜的表面,将聚酰亚胺薄膜浸入含有通过将式1化合物与化合物混合而制备的乙烯亚胺基硅烷偶联剂的溶液 的摩尔比为0.25〜1,然后通过第二等离子体处理改性聚酰亚胺膜的表面。 对聚酰亚胺膜进行表面改性的方法是有利的,因为它可以代替使用离子束的常规表面处理方法。 此外,具有通过在表面改性聚酰亚胺膜上进行铜溅射和电镀形成的双层结构的FCCL具有在聚酰亚胺膜和铜箔之间的良好的粘合强度,并且即使在高温下也能够保持这种粘合强度长时间 一段的时间。 此外,它可以有用地应用于诸如柔性印刷电路板,TCP(胶带载体封装),COF(片上胶片)等电子部件。

    Polyamide-imide having head-to-tail backbone
    8.
    发明授权
    Polyamide-imide having head-to-tail backbone 失效
    具有头对头骨架的聚酰胺酰亚胺

    公开(公告)号:US06433184B1

    公开(公告)日:2002-08-13

    申请号:US09605026

    申请日:2000-06-28

    IPC分类号: C07D20948

    CPC分类号: C08G73/14

    摘要: The present invention relates to polyamide-imides having head-to-tail backbone and more particularly, to polyamide-imimdes having head-to-tail ragularity to provide excellent heat and chemical resistance, physical and mechanical properties, processability, and gas permeability and selectivity. The polyamide-imides represented in the following formula (1) are obtained by direct polymerization, in the presence of dehydrating catalyst, of alone or as a mixture of 2 or above of monomers prepared by condensation of an amine compound having a nitro group with a carboxylic acid anhydride,

    摘要翻译: 本发明涉及具有头 - 尾主链的聚酰胺 - 酰亚胺,更具体地说,涉及具有头对尾的粗糙度以提供优异的耐热和耐化学性,物理和机械性能,可加工性和气体渗透性和选择性的聚酰胺酰亚胺 。 在下式(1)中表示的聚酰胺 - 酰亚胺通过在脱水催化剂的存在下,单独或作为2种以上的单体的混合物直接聚合而获得,所述单体通过具有硝基的胺化合物与 羧酸酐,

    Process of preparing polycarbonates
    9.
    发明授权
    Process of preparing polycarbonates 有权
    制备聚碳酸酯的方法

    公开(公告)号:US06423812B1

    公开(公告)日:2002-07-23

    申请号:US09901727

    申请日:2001-07-11

    IPC分类号: C08G6400

    CPC分类号: C08G64/307

    摘要: The present invention relates to a process of preparing polycarbonates and more particularly, to the process of preparing polycarbonates through a melt polymerization reaction of dihydroxyaryl compounds with diarylcarbonate, wherein said melt polymerization is performed in the presence of a mixed catalyst composed of an oxygen (O) or sulfur (S) containing compound having lone-pair electrons and an alkali metal or alkaline earth metal salt in an appropriate ratio at a reduced temperature by accelerating a reaction rate to obtain high quality polycarbonates with higher than 15,000 g/mole of a viscosity average molecular weight and improved color.

    摘要翻译: 本发明涉及一种制备聚碳酸酯的方法,更具体地说,涉及通过二羟基芳基化合物与碳酸二芳基酯的熔融聚合反应制备聚碳酸酯的方法,其中所述熔融聚合在由氧(O )或含硫(S)的化合物,具有单对电子的碱金属或碱土金属盐,碱金属或碱土金属盐在降低的温度下通过加速反应速率以适当的比例获得高质量的聚碳酸酯,其粘度高于15,000g / 平均分子量和颜色改善。

    Quantitative evaluation of scratch-induced damages on polymeric and coating materials
    10.
    发明授权
    Quantitative evaluation of scratch-induced damages on polymeric and coating materials 有权
    对聚合物和涂层材料的划痕损伤的定量评估

    公开(公告)号:US08316689B2

    公开(公告)日:2012-11-27

    申请号:US12845388

    申请日:2010-07-28

    IPC分类号: G01N3/56

    CPC分类号: G01N3/46

    摘要: Provided is a method for quantitative evaluation of mar- and scratch-induced surface damage on polymeric and coating materials. The method for quantitative evaluation of scratch-induced damage on polymeric and coating materials includes: preparing a test specimen of polymeric and coating materials; inducing a scratch damage on the surface of the test specimen; representing the scratch damage formed on the test specimen as corresponding color coordinates; and calculating a quantitated scratch damage index from a combination of a load applied to the surface of the test specimen and the color coordinates corresponding to the scratch damage.

    摘要翻译: 提供了一种用于定量评估聚合物和涂层材料上的划痕和划痕表面损伤的方法。 用于定量评估聚合物和涂层材料上的划痕损伤的方法包括:制备聚合物和涂层材料的试样; 在试样的表面引起划痕损伤; 代表在试样上形成的划痕损伤作为相应的颜色坐标; 以及从施加到测试样本表面的负载和对应于划痕损伤的颜色坐标的组合计算定量的划痕损伤指数。