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1.发明授权公开(公告)号：US06590049B1
公开(公告)日：2003-07-08
申请号：US09687026
申请日：2000-10-13
IPC分类号： C08F200
CPC分类号： C09D17/001 , C08F4/00 , C09B67/009
摘要： The present invention is directed to novel compounds that can serve as highly efficient initiators for controlled radical (co)polymerization processes including atom transfer radical (co)polymerization processes. These compounds include di-(trimethylolpropane)-tetra-(2-haloisobutyrate) compounds. The present invention also is directed to controlled radical (co)polymerization processes in which novel (co)polymers are prepared using the novel compounds, as well as to the novel (co)polymer products of the process.
摘要翻译： 本发明涉及可用作用于受控自由基（共）聚合方法的高效引发剂的新型化合物，包括原子转移自由基（共）聚合方法。 这些化合物包括二（三羟甲基丙烷） - 四 - （2-卤代异丁酸酯）化合物。 本发明还涉及使用新化合物以及该方法的新型（共）聚合物产物制备新型（共）聚合物的受控自由基（共）聚合方法。
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2.发明授权Pigment dispersions containing dispersants prepared by controlled radical polymerization and having pendent hydrophilic polymeric segments 失效含有分散剂的颜料分散体，其通过可控自由基聚合制备并具有侧链亲水性聚合物链段公开(公告)号：US06294014B1
公开(公告)日：2001-09-25
申请号：US09464917
申请日：1999-12-16
IPC分类号： C08L5106
CPC分类号： C09B67/0085 , C09B67/0066
摘要： A pigment dispersion comprising pigment, an aqueous carrier selected from water and a mixture of water and at least one organic solvent, and a pigment dispersant is described. The pigment dispersant is prepared by controlled radical polymerization, e.g., atom transfer radical polymerization, of a radically polymerizable monomer in the presence of a polymeric initiator having at least one radically transferable group. The polymeric initiator forms the polymeric backbone segment of the pigment dispersant, and the monomer forms polymeric segments that are pendent to the polymeric backbone segment. The pigment dispersant has comb-like architecture in which the polymeric backbone segment is hydrophobic, and at least a portion of each pendent polymeric segment is hydrophilic.
摘要翻译： 描述了包含颜料，选自水和水与至少一种有机溶剂的混合物的水性载体和颜料分散剂的颜料分散体。 在具有至少一个可自由基转移基团的聚合物引发剂的存在下，通过可自由基聚合的单体的可控自由基聚合，例如原子转移自由基聚合制备颜料分散剂。 聚合引发剂形成颜料分散剂的聚合物主链段，并且单体形成与聚合物骨架链段相反的聚合链段。 颜料分散剂具有梳状结构，其中聚合物骨架链段是疏水性的，并且每个侧链聚合链段的至少一部分是亲水的。
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3.发明授权Pigment dispersions containing dispersants having pendent hydrophilic polymeric segments prepared by controlled radical polymerization 失效含有分散剂的颜料分散体，其具有通过受控自由基聚合制备的具有亲水性亲水性聚合物链段公开(公告)号：US06376597B1
公开(公告)日：2002-04-23
申请号：US09464915
申请日：1999-12-16
IPC分类号： C08L5100
CPC分类号： C09D17/001 , C09B67/0066 , C09B67/009
摘要： A pigment dispersion comprising pigment, an aqueous carrier selected from water and a mixture of water and at least one organic solvent, and a pigment dispersant is described. The pigment dispersant is prepared by polymerizing (i) at least one prepolymer having a radically polymerizable group, and (ii) at least one second monomer. The prepolymer is prepared by controlled radical polymerization, e.g., atom transfer radical polymerization, of at least one radically polymerizable first monomer. The second monomer forms a polymeric backbone segment of the pigment dispersant, and the prepolymer forms polymeric segments that are pendent to the backbone. The backbone segment of the pigment dispersant in hydrophobic, while at least a portion of each pendent polymeric segment is hydrophilic.
摘要翻译： 描述了包含颜料，选自水和水与至少一种有机溶剂的混合物的水性载体和颜料分散剂的颜料分散体。 通过聚合（i）至少一种具有自由基聚合性基团的预聚物和（ii）至少一种第二单体来制备颜料分散剂。 预聚物通过至少一种可自由基聚合的第一单体的受控自由基聚合，例如原子转移自由基聚合制备。 第二单体形成颜料分散剂的聚合物主链段，并且预聚物形成与主链相邻的聚合物链段。 疏水性的颜料分散剂的骨架部分，而每个侧链聚合物链段的至少一部分是亲水的。
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4.发明授权Thermosetting coating compositions comprising a copolymer formed from chlorotrifluoroethylene and methods of making copolymers formed from chlorotrifluoroethylene 失效包含由三氟氯乙烯形成的共聚物的热固性涂料组合物和由氯三氟乙烯形成的共聚物的方法公开(公告)号：US07335705B2
公开(公告)日：2008-02-26
申请号：US11241344
申请日：2005-09-30
IPC分类号： C08F114/18
CPC分类号： C08F8/00 , C08F214/18 , C08F214/24 , C08K5/0025 , C09D127/12 , D06M15/277 , C08L27/12
摘要： Fluoropolymers are disclosed. The fluoropolymers include (i) units derived from a fluoromonomer composition comprising chlorotrifluoroethylene, and (ii) units derived from at least one donor monomer composition. In the disclosed fluoropolymers, units (i) and (ii) are distributed along the fluoropolymer chain in a substantially alternating fashion. Also disclosed are thermosetting compositions containing such fluoropolymers, substrates coated with such compositions, methods for making such compositions, and methods for coating substrates with such compositions.
摘要翻译： 披露了含氟聚合物。 含氟聚合物包括（i）衍生自包含氯三氟乙烯的含氟单体组合物的单元，和（ii）衍生自至少一种供体单体组合物的单元。 在所公开的含氟聚合物中，单元（i）和（ii）以基本交替的方式沿着含氟聚合物链分布。 还公开了含有这样的含氟聚合物的热固性组合物，用这种组合物涂覆的基材，制备这种组合物的方法，以及用这种组合物涂覆基材的方法。
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5.发明授权Fluoropolymers, methods for their production, and thermosetting compositions containing them 失效含氟聚合物，它们的生产方法和含有它们的热固性组合物公开(公告)号：US07332545B2
公开(公告)日：2008-02-19
申请号：US11239777
申请日：2005-09-30
IPC分类号： C08F114/18
CPC分类号： C08F214/18 , C08F8/12 , C08F214/28 , C08F2800/10 , C08F2800/20 , C09D123/22 , C08L2666/28 , C08F218/08
摘要： Fluoropolymers are disclosed. The fluoropolymers include (i) units derived from a fluoromonomer having the formula F2C═CXY, where X is CF3 and Y is either F or CF3, and (ii) units derived from at least one donor monomer. In the disclosed fluoropolymers, units (i) and (ii) are distributed along the fluoropolymer chain in a substantially alternating fashion. Also disclosed are thermosetting compositions containing such fluoropolymers, substrates coated with such compositions, methods for making such compositions, and methods for coating substrates with such compositions.
摘要翻译： 公开了含氟聚合物。 含氟聚合物包括（i）衍生自具有式F 2 C-CXY的含氟单体的单元，其中X是CF 3，Y是F或CF 3 和（ii）衍生自至少一种供体单体的单元。 在所公开的含氟聚合物中，单元（i）和（ii）以基本交替的方式沿着含氟聚合物链分布。 还公开了含有这样的含氟聚合物的热固性组合物，用这种组合物涂覆的基材，制备这种组合物的方法，以及用这种组合物涂覆基材的方法。
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6.发明授权Pigment dispersions containing dispersants prepared by controlled radical polymerization and having pendent hydrophobic polymeric segments 失效含有分散剂的颜料分散体，其通过受控的自由基聚合制备并具有悬挂的疏水性聚合物链段公开(公告)号：US06441066B1
公开(公告)日：2002-08-27
申请号：US09464914
申请日：1999-12-16
IPC分类号： C08K548
CPC分类号： C09D17/001 , C08K5/0041 , C09B67/009 , C09D7/45
摘要： A pigment dispersion comprising pigment, an aqueous carrier selected from water and a mixture of water and at least one organic solvent, and a pigment dispersant is described. The pigment dispersant is prepared by controlled radical polymerization, e.g., atom transfer radical polymerization, of a radically polymerizable monomer in the presence of a polymeric initiator having at least one radically transferable group. The polymeric initiator forms the polymeric backbone segment of the pigment dispersant, and the monomer forms polymeric segments that are pendent to the polymeric backbone segment. The pigment dispersant has comb-like architecture in which the polymeric backbone segment is hydrophilic, and at least a portion of each pendent polymeric segment is hydrophobic.
摘要翻译： 描述了包含颜料，选自水和水与至少一种有机溶剂的混合物的水性载体和颜料分散剂的颜料分散体。 在具有至少一个可自由基转移基团的聚合物引发剂的存在下，通过可自由基聚合的单体的可控自由基聚合，例如原子转移自由基聚合制备颜料分散剂。 聚合引发剂形成颜料分散剂的聚合物主链段，并且单体形成与聚合物骨架链段相反的聚合链段。 颜料分散剂具有梳状结构，其中聚合物主链段是亲水性的，并且每个侧链聚合物链段的至少一部分是疏水性的。
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7.发明授权Pigment dispersions containing dispersants having pendent hydrophobic polymeric segments prepared by controlled radical polymerization 失效含有分散剂的颜料分散体，其具有通过受控自由基聚合制备的具有疏水性聚合物链段公开(公告)号：US06306209B1
公开(公告)日：2001-10-23
申请号：US09464916
申请日：1999-12-16
IPC分类号： C09D1700
CPC分类号： C09D151/006 , C08F265/04 , C08F265/06 , C08F285/00 , C08F287/00 , C08F290/06 , C08F291/00 , C08F293/005 , C08F2438/01 , C09B67/009 , C09D17/001 , C09D151/003 , C09D153/005 , C08L2666/02
摘要： A pigment dispersion comprising pigment, an aqueous carrier selected from water and a mixture of water and at least one organic solvent, and a pigment dispersant is described. The pigment dispersant is prepared by polymerizing (i) at least one prepolymer having a radically polymerizable group, and (ii) at least one second monomer. The prepolymer is prepared by controlled radical polymerization, e.g., atom transfer radical polymerization, of at least one radically polymerizable first monomer. The second monomer forms a polymeric backbone segment of the pigment dispersant, and the prepolymer forms polymeric segments that are pendent to the backbone. The backbone segment of the pigment dispersant is hydrophilic, while at least a portion of each pendent polymeric segment is hydrophobic.
摘要翻译： 描述了包含颜料，选自水和水与至少一种有机溶剂的混合物的水性载体和颜料分散剂的颜料分散体。 通过聚合（i）至少一种具有自由基聚合性基团的预聚物和（ii）至少一种第二单体来制备颜料分散剂。 预聚物通过至少一种可自由基聚合的第一单体的受控自由基聚合，例如原子转移自由基聚合制备。 第二单体形成颜料分散剂的聚合物主链段，并且预聚物形成与主链相邻的聚合物链段。 颜料分散剂的主链段是亲水性的，而每个侧链聚合链段的至少一部分是疏水性的。
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公开(公告)号：US08129466B2
公开(公告)日：2012-03-06
申请号：US12054821
申请日：2008-03-25
IPC分类号： C08L31/00
CPC分类号： C09D17/003 , C08F293/00 , C08K3/013 , C08K5/0041 , C08L53/00 , C09D7/45
摘要： A pigment dispersant is disclosed comprising a tri-block copolymer having a first block comprising a glycidyl(meth)acrylate reacted with a napthoic acid, a second block comprising (meth)acrylic acid alkyl esters, and a third block comprising (meth)acrylic acid alkyl esters, wherein said third block is different from said second block. The dispersant is suited for use in a nanoparticulate dispersion comprising pigment particles having an average primary particle size of less than 100 nm.
摘要翻译： 公开了一种颜料分散剂，其包含具有第一嵌段的三嵌段共聚物，所述第一嵌段包含与萘甲酸反应的（甲基）丙烯酸缩水甘油酯，第二嵌段包含（甲基）丙烯酸烷基酯，和第三嵌段，其包含（甲基）丙烯酸 烷基酯，其中所述第三嵌段不同于所述第二嵌段。 分散剂适用于包含平均一次粒径小于100nm的颜料颗粒的纳米颗粒分散体。
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9.发明申请SULFONATION OF CONDUCTING POLYMERS AND OLED, PHOTOVOLTAIC, AND ESD DEVICES 有权导电聚合物和OLED，光伏和ESD器件的降解公开(公告)号：US20120037852A1
公开(公告)日：2012-02-16
申请号：US13209210
申请日：2011-08-12
申请人： Venkataramanan SESHADRI , Brian E. Woodworth , Christopher Greco , Darin Laird , Mathew K. Mathai
发明人： Venkataramanan SESHADRI , Brian E. Woodworth , Christopher Greco , Darin Laird , Mathew K. Mathai
CPC分类号： H01L51/0036 , C08G61/126 , C08G2261/1424 , C08G2261/1452 , C08G2261/18 , C08G2261/212 , C08G2261/3223 , C08G2261/43 , C08G2261/512 , C08G2261/722 , C08G2261/79 , C08G2261/95 , C08L65/00 , C09D165/00 , H01G9/028 , H01G11/48 , H01G11/56 , H01L51/006 , H01L51/0081 , H01L51/5048 , H01L51/5088 , Y02E10/549 , Y02E60/13 , Y10T428/31504 , Y10T428/31533 , Y10T428/31678 , C08L2666/02
摘要： Conducting polymer systems for hole injection or transport layer applications including a composition comprising: a water soluble or water dispersible regioregular polythiophene comprising (i) at least one organic substituent, and (ii) at least one sulfonate substituent comprising sulfonate sulfur bonding directly to the polythiophene backbone. The polythiophene can be water soluble, water dispersible, or water swellable. They can be self-doped. The organic substituent can be an alkoxy substituent, or an alkyl substituent. OLED, PLED, SMOLED, PV, and ESD applications can be used.
摘要翻译： 用于空穴注入或传输层应用的导电聚合物体系包括包含以下组合物的组合物：水溶性或水分散性区域性聚噻吩，其包含（i）至少一种有机取代基，和（ii）至少一种磺酸盐取代基，其包含与所述聚噻吩直接结合的磺酸盐 骨干。 聚噻吩可以是水溶性的，水分散的或水可溶胀的。 它们可以是自掺杂的。 有机取代基可以是烷氧基取代基或烷基取代基。 可以使用OLED，PLED，SMOLED，PV和ESD应用。
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10.发明授权Sulfonation of conducting polymers and OLED, photovoltaic, and ESD devices 有权导电聚合物和OLED，光伏和ESD器件的磺化公开(公告)号：US08017241B2
公开(公告)日：2011-09-13
申请号：US11826394
申请日：2007-07-13
申请人： Venkataramanan Seshadri , Brian E. Woodworth , Christopher Greco , Darin Laird , Mathew K. Mathai
发明人： Venkataramanan Seshadri , Brian E. Woodworth , Christopher Greco , Darin Laird , Mathew K. Mathai
CPC分类号： H01L51/0036 , C08G61/126 , C08G2261/1424 , C08G2261/1452 , C08G2261/18 , C08G2261/212 , C08G2261/3223 , C08G2261/43 , C08G2261/512 , C08G2261/722 , C08G2261/79 , C08G2261/95 , C08L65/00 , C09D165/00 , H01G9/028 , H01G11/48 , H01G11/56 , H01L51/006 , H01L51/0081 , H01L51/5048 , H01L51/5088 , Y02E10/549 , Y02E60/13 , Y10T428/31504 , Y10T428/31533 , Y10T428/31678 , C08L2666/02
摘要： Conducting polymer systems for hole injection or transport layer applications including a composition comprising: a water soluble or water dispersible regioregular polythiophene comprising (i) at least one organic substituent, and (ii) at least one sulfonate substituent comprising sulfonate sulfur bonding directly to the polythiophene backbone. The polythiophene can be water soluble, water dispersible, or water swellable. They can be self-doped. The organic substituent can be an alkoxy substituent, or an alkyl substituent. OLED, PLED, SMOLED, PV, and ESD applications can be used.
摘要翻译： 用于空穴注入或传输层应用的导电聚合物体系包括包含以下组合物的组合物：水溶性或水分散性区域性聚噻吩，其包含（i）至少一种有机取代基，和（ii）至少一种磺酸盐取代基，其包含与所述聚噻吩直接结合的磺酸盐 骨干。 聚噻吩可以是水溶性的，水分散的或水可溶胀的。 它们可以是自掺杂的。 有机取代基可以是烷氧基取代基或烷基取代基。 可以使用OLED，PLED，SMOLED，PV和ESD应用。
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