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    Process for producing phenol and methyl ethyl ketone
    3.
    发明授权
    Process for producing phenol and methyl ethyl ketone 失效
    苯酚和甲基乙基酮的制备方法

    公开(公告)号：US07834218B2

    公开(公告)日：2010-11-16

    申请号：US12162970

    申请日：2007-02-08

    申请人： Jihad M. Dakka ,  Jon E. Stanat ,  Francisco M. Benitez ,  John S. Buchanan ,  Jane C. Cheng ,  Jeffrey T. Elks

    发明人： Jihad M. Dakka ,  Jon E. Stanat ,  Francisco M. Benitez ,  John S. Buchanan ,  Jane C. Cheng ,  Jeffrey T. Elks

    IPC分类号： C07C45/53 ,  C07C37/08

    CPC分类号： C07C409/08 ,  C07C37/08 ,  C07C45/53 ,  C07C407/00 ,  C07C49/10 ,  C07C39/04

    摘要： A process for producing phenol and methyl ethyl ketone comprises contacting benzene and a C4 alkylating agent under alkylation conditions and in the presence of an alkylation catalyst comprising at least one molecular sieve of the MCM-22 family to produce an alkylation effluent comprising secbutylbenzene; wherein the contacting is conducted in a plurality of reaction zones and the C4 alkylating agent secbutylbenzene fraction is recovered from the alkylation effluent and comprises at least 95 wt % sec-butylbenzene, less than 100 wt ppm of C8+ olefins, and less than 0.5 wt % of isobutylbenzene and tert-butylbenzene. The sec-butylbenzene fraction is then oxidized to produce sec-butylbenzene hydroperoxide and the hydroperoxide is cleaved to produce phenol and methyl ethyl ketene.

    摘要翻译： 一种生产苯酚和甲基乙基酮的方法包括在烷基化条件下和在包含至少一种MCM-22族分子筛的烷基化催化剂的存在下使苯和C4烷基化剂接触以产生包含二丁基苯的烷基化流出物; 其中所述接触在多个反应区中进行，并且所述C4烷基化剂仲丁苯部分从烷基化流出物中回收，并且包含至少95重量％的仲丁基苯，小于100重量ppm的C 8+烯烃和小于0.5重量％ 的异丁基苯和叔丁基苯。 然后将仲丁基馏分氧化以产生仲丁基苯氢过氧化物，并将氢过氧化物裂解以产生苯酚和甲基乙基乙烯酮。

    PROCESS FOR PRODUCING PHENOL AND METHYL ETHYL KETONE
    5.
    发明申请
    PROCESS FOR PRODUCING PHENOL AND METHYL ETHYL KETONE 失效
    生产苯酚和甲基乙酮的方法

    公开(公告)号：US20090187047A1

    公开(公告)日：2009-07-23

    申请号：US12162970

    申请日：2007-02-08

    申请人： Jihad M. Dakka ,  Jon E. Stanat ,  Francisco M. Benitez ,  John S. Buchanan ,  Jane C. Cheng ,  Jeffrey T. Elks

    发明人： Jihad M. Dakka ,  Jon E. Stanat ,  Francisco M. Benitez ,  John S. Buchanan ,  Jane C. Cheng ,  Jeffrey T. Elks

    IPC分类号： C07C45/53 ,  C07C37/08

    CPC分类号： C07C409/08 ,  C07C37/08 ,  C07C45/53 ,  C07C407/00 ,  C07C49/10 ,  C07C39/04

    摘要： A process for producing phenol and methyl ethyl ketone comprises contacting benzene and a C4 alkylating agent under alkylation conditions and in the presence of an alkylation catalyst comprising at least one molecular sieve of the MCM-22 family to produce an alkylation effluent comprising secbutylbenzene; wherein the contacting is conducted in a plurality of reaction zones and the C4 alkylating agent secbutylbenzene fraction is recovered from the alkylation effluent and comprises at least 95 wt % sec-butylbenzene, less than 100 wt ppm of C8+ olefins, and less than 0.5 wt % of isobutylbenzene and tert-butylbenzene. The sec-butylbenzene fraction is then oxidized to produce sec-butylbenzene hydroperoxide and the hydroperoxide is cleaved to produce phenol and methyl ethyl ketone.

    摘要翻译： 一种生产苯酚和甲基乙基酮的方法包括在烷基化条件下和在包含至少一种MCM-22族分子筛的烷基化催化剂的存在下使苯和C4烷基化剂接触以产生包含二丁基苯的烷基化流出物; 其中所述接触在多个反应区中进行，并且所述C4烷基化剂仲丁苯部分从所述烷基化流出物中回收，并且包含至少95重量％的仲丁基苯，小于100重量ppm的C 8+烯烃和小于0.5重量％ 的异丁基苯和叔丁基苯。 然后将仲丁基馏分氧化以产生仲丁基苯氢过氧化物，并将氢过氧化物裂解以产生苯酚和甲基乙基酮。

    Process for producing sec-butylbenzene
    9.
    发明授权
    Process for producing sec-butylbenzene 失效
    仲丁基苯的制备方法

    公开(公告)号：US07939693B2

    公开(公告)日：2011-05-10

    申请号：US12666333

    申请日：2008-07-11

    申请人： Jane C. Cheng ,  Jihad M. Dakka ,  Travis A. Reine ,  Jon E. Stanat

    发明人： Jane C. Cheng ,  Jihad M. Dakka ,  Travis A. Reine ,  Jon E. Stanat

    IPC分类号： C07C45/00 ,  C07C37/08 ,  C07C15/067

    CPC分类号： C07C409/08 ,  C07C2/66 ,  C07C37/08 ,  C07C45/53 ,  C07C407/00 ,  Y02P20/127 ,  C07C15/02 ,  C07C49/10 ,  C07C39/04

    摘要： A process for producing sec-butylbenzene comprises feeding reactants comprising benzene and a C4 olefin to a distillation column reactor having a first reaction zone containing an alkylation catalyst and a second distillation zone, which is located below said first reaction zone and which is substantially free of alkylation catalyst, wherein the ratio of the number of distillation stages in said first reaction zone to the number of distillation stages in said second distillation zone is less than 1:1. Concurrently in the distillation reactor, the reactants are contacted with the alkylation catalyst in the first reaction zone under conditions such that the C4 olefin reacts with the benzene to produce sec-butylbenzene and the sec-butylbenzene is fractioned from the unreacted C4 olefin. The sec-butylbenzene thereby passes as a liquid phase stream from the first reaction zone to the second distillation zone and the liquid phase steam is withdrawn from the distillation column reactor as bottoms.

    摘要翻译： 一种生产仲丁基苯的方法包括将含有苯和C 4烯烃的反应物进料到具有含有烷基化催化剂和第二蒸馏区的第一反应区的蒸馏塔反应器中，所述第一反应区位于所述第一反应区之下且基本上不含 烷基化催化剂，其中所述第一反应区中的蒸馏级数与所述第二蒸馏区中的蒸馏级数之比小于1:1。 同时在蒸馏反应器中，使反应物与第一反应区中的烷基化催化剂接触，使得C 4烯烃与苯反应产生仲丁基苯，仲丁基苯从未反应的C 4烯烃中分馏。 因此，仲丁基苯作为液相物流从第一反应区流向第二蒸馏区，液相蒸汽作为底部从蒸馏塔反应器中排出。