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    Preparation of veratryl cyanide
    1.
    发明授权
    Preparation of veratryl cyanide 失效
    氰化镨的制备

    公开(公告)号：US4661610A

    公开(公告)日：1987-04-28

    申请号：US887940

    申请日：1986-07-22

    申请人： Josef Muller ,  Walter-Wielant Wiersdorff ,  Wolfram Burst ,  Heinz Dralle ,  Ernst Schaffner ,  Rolf Steinkamp

    发明人： Josef Muller ,  Walter-Wielant Wiersdorff ,  Wolfram Burst ,  Heinz Dralle ,  Ernst Schaffner ,  Rolf Steinkamp

    IPC分类号： C07C255/53 ,  C07C120/04

    CPC分类号： C07C255/00

    摘要： Veratryl cyanide is prepared by chloromethylating veratrol in solution in toluene and then reacting the resulting veratryl chloride with from 1 to 5 moles of an alkali metal cyanide, by a process in which the toluene from the chloromethylation is not removed for the reaction with cyanide, and from 3 to 25% by weight, based on veratryl chloride, of water, from 5 to 50% by weight, based on toluene, of a ketone of 3 to 6 carbon atoms and from 0.1 to 10% by weight, based on veratryl chloride, of a phase transfer catalyst are added before the reaction with cyanide.

    摘要翻译： 通过在甲苯溶液中氯甲基化藜芦醇，然后使得到的藜芦酰与1至5摩尔碱金属氰化物反应，其中氯甲基化的甲苯未被除去以与氰化物反应， 3至25重量％，基于藜芦醚，水，5至50重量％，基于甲苯，3至6个碳原子的酮和0.1至10重量％，基于藜芦 的相转移催化剂在与氰化物反应之前加入。

    Uniformly dyed water-swellable cellulosic fibers
    3.
    发明授权
    Uniformly dyed water-swellable cellulosic fibers 失效
    均匀染色的水溶胀纤维素纤维

    公开(公告)号：US4167394A

    公开(公告)日：1979-09-11

    申请号：US868213

    申请日：1978-01-09

    申请人： Johannes Dehnert ,  Guenter Hansen ,  Hermann Kaack ,  Wolf-Dieter Kermer ,  Walter Kurtz ,  Ernst Schaffner

    发明人： Johannes Dehnert ,  Guenter Hansen ,  Hermann Kaack ,  Wolf-Dieter Kermer ,  Walter Kurtz ,  Ernst Schaffner

    IPC分类号： C09B29/01 ,  C09B29/36 ,  D06P3/60 ,  D06P3/82 ,  C09B29/38 ,  D06M1/00 ,  D06P1/04

    CPC分类号： C09B29/0011 ,  C09B29/36 ,  D06P3/6041 ,  D06P3/8233

    摘要： Uniformly dyed water-swellable cellulosic fibers obtained by dyeing cellulosic fibers, in the swollen state, with a dye of the formula ##STR1## where X is hydrogen, chlorine, bromine, cyano, nitro, alkylsulfonyl of 1 to 4 carbon atoms, phenylsulfonyl, methoxy or ethoxy, Y is hydrogen, chlorine, bromine, cyano or nitro, Z is a radical of the formula ##STR2## Q is oxygen or sulfur, R.sup.1 is alkyl of 1 to 4 carbon atoms, methoxymethyl, phenoxymethyl or phenyl which is unsubstituted or substituted by chlorine, bromine, nitro, methyl, methoxy or ethoxy, R.sup.2 is hydrogen, methyl, ethyl, phenyl or phenyl substituted by chlorine, bromine or methyl, R.sup.3 is hydrogen, methyl or, if R.sup.2 is methyl, is C.sub.1 to C.sub.4 alkoxycarbonyl, R.sup.2 and R.sup.3 together with the linking carbon atoms are phenylene or phenylene substituted by chlorine, methyl, methoxy or ethoxy and K is a radical of a coupling component selected from the pyrazolone, pyrazole, indole, quinolone or homophthalimide series.

    摘要翻译： 通过染色纤维素纤维获得的均匀染色的水溶胀性纤维素纤维，其呈溶胀状态，其中X为氢，氯，溴，氰基，硝基，1至4个碳原子的烷基磺酰基，苯基磺酰基， 甲氧基或乙氧基，Y是氢，氯，溴，氰基或硝基，Z是下式的基团Q是氧或硫，R1是1至4个碳原子的烷基，甲氧基甲基，苯氧基甲基或苯基，其是未取代的 或被氯，溴，硝基，甲基，甲氧基或乙氧基取代，R 2为氢，甲基，乙基，苯基或被氯，溴或甲基取代的苯基，R 3为氢，甲基或如果R 2为甲基，则为C 1至C 4 烷氧基羰基，R2和R3与连接碳原子一起被亚甲基或亚苯取代，被氯，甲基，甲氧基或乙氧基取代，K是选自吡唑啉酮，吡唑，吲哚，喹诺酮或高邻苯二甲酰亚胺系列的偶联成分的基团。